• Title/Summary/Keyword: 03-03

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Synthesis and Electrochemical Behavior of Rare Earths Metal Complexes (희토류금속 착물의 합성과 전기화학적 거동 (제 2 보))

  • Choe, Chil Nam;Jeong, O Jin;Yun, Seok Jin;Kim, Jun Tae
    • Journal of the Korean Chemical Society
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    • v.34 no.3
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    • pp.280-287
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    • 1990
  • The electrochemical behavir of trivalent lanthanides [Sm(Ⅲ), Tb(Ⅲ), and Yb(Ⅲ)) complexes were investigated by the use of direct current, differential pulse polarography and cyclic voltammetry in aprotic media. These reduction peak were irreversible one-electron processes at $E_{pc}$ = -0.16 V, -0.35 V, -0.14 V, and -0.03 V of trivalent lanthanide complexes vs. Ag/AgCl electrode and the behavior of heavier lanthanides were decreased Sm > Tb > Ho > Yb order of the stability constant with decreasing atomic number.

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Stability of 0ndansetron and Fluconazole in 5% Dextrose Injection and Normal Saline during Y-Site Administration

  • Burm, Jin-Pil
    • Archives of Pharmacal Research
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    • v.20 no.2
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    • pp.171-175
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    • 1997
  • The stability of ondansetron and fluconazole in 5% dextrose injection and normal saline during simulated Y-site injection at room temperature was studied. Ondansetron 0.03, 0.1 and 0.3 mg/ml were admixed 1:1 with fluconazole 2 mg/ml. The solutions were stored at room temperature and samples were retrieved at time 0, 1, 2, 4 and 12 hr for immediate assay. At the time of the assay and before any dilution, each sample was visually inspected for clarity, color, precipitation, and the pH was determined. Drug concentrations were measured by a stability-indicating high performance liquid chromatograph. Ondansetron 0.03, 0.1 and 0.3 mg/ml were stable when mixed with concentration of fluconazole 2 mg/ml. There were no change in clarity and color and no precipitates in any admixture for 12 hr of inspection. The pH measurements did not have a particular trend in any direction over time.

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Status of Studies on Regulatory Provisions for HAPS (성층권 통신 시스템(HAPS) 규정 연구 현황)

  • Lee, S.M.;Park, J.M.;Ku, B.J.;Ahn, D.S.
    • Electronics and Telecommunications Trends
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    • v.22 no.3 s.105
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    • pp.166-173
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    • 2007
  • WRC-97에서 HAPS 개념이 도입된 후, HAPS 이용 주파수 대역으로 IMT-2000 대역과 Ka 및 V 대역이 지정되었다. IMT-2000 대역에 대한 공유 및 규정 연구는 WRC-03에서 종료되었으나, Ka 및 V 대역에서 타 무선업무와 HAPS를 이용한 고정업무 간의 기술적, 운용적 그리고 규정에 관한 연구를 지속하고 WRC-07에서 연구결과를 검토하기로 하였다. 본 고에서는 WRC-03 회의에서 결의한 IMT-2000 서비스를 제공하는 HAPS 시스템의 이용에 관한 규정 현황을 알아보고, 현재 ITU-R에서 논의중인 Ka및 V 대역에서 HAPS 시스템 활용을 위한 규정 연구 현황을 살펴보고자 한다.

UBV CCD PHOTOMETRY OF OPEN CLUSTER NGC 1907 AND NGC 1912

  • Lee, Sang-Hyeon;Lee, Si-Woo
    • Publications of The Korean Astronomical Society
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    • v.11 no.1
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    • pp.139-146
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    • 1996
  • Galactic open clusters NGC 1907 and NGC 1912 are known as a binary cluster candidate by Subramaniam et al.(1995). With the SNUO 0.6m telescope, UBV CCD photometric observations were performed for 62 stars in NGC 1907 within the area of $8'{\times}8'$ and 203 stars in NGC 1912 within the area of $15'{\times}15'$ area. We obtained C-M and C-C diagrams. Their mean reddenings are E(B-V) = $0.50{\pm}0.03$ for NGC 1907 and $0.27{\pm}0.03$ for NGC 1912. The distance moduli are estimated as $10.9{\pm}0.15$ and $10.4{\pm}0.10$ for NGC 1907 and NGC 1912, respectively. The ages for these clusters are $400{\pm}50Myr$ for NGC 1907 and $150{\pm}30Myr$ for NGC 1912. The distance difference of the two clusters is 300pc and the age difference is 150Myr. These results imply that the two clusters are not physically connected.

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Variation of the Electrophoretic Mobility of Acid Mucopolysaccharides in Polyacrylamide Gel Electrophoresis (Polyacrylamide Gel Electrophoresis에 있어서 酸性 Mucopolysaccharide의 移動度의 變化)

  • Geum, Gi-Chang;Ru Do Wi Keu Jul, Ri O
    • Journal of the Korean Chemical Society
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    • v.18 no.2
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    • pp.132-137
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    • 1974
  • Acid mucopolysaccharides were isolated from nucleus pulposus of whale embryo. The separation of acid mucopolysaccharides was most excellent in $0.03{\%}$ hexamine cobaltic chloride in 0.05 M-sodium acetate buffer solution at pH 4.8. Changes in electrophoretic mobility of acid mucopolysaccharides were observed when the sample solution on top of spacer gel were covered with $40{\%}$ sucrose solution. This effect was not observed by the addition of hexamine cobaltic chloride to the buffer solution.

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Changes of Free Sugars & Free Sugar Alcohols in Lentinus edodes during Storage. (표고버섯(Lentinus edodes) 저장중의 유리당과 당알콜성분의 변화)

  • 이가순;이주찬
    • Food Science and Preservation
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    • v.5 no.2
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    • pp.154-161
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    • 1998
  • Changes of free sugars and sugar alcohols of fresh shiitake were measured during storage. Shiitake were stored at 1$^{\circ}C$ and -4$^{\circ}C$, with non-packaging, wrapping, 0.03mm polyethylene(PE)film packaging(unpunched and punched, unprecooled and precooled before storage), 0.05mm PE film (vacuum packaging). Chanties of glycerol, arabitol and arabinose contents were not marked during storage. The content chanties of $\beta$-rhamnose, fructose, glucose, mannitol, sucrose and maltose were the smallest until 40days storage and were increased significantly after 40 days and then decreased significantly after 50days. Content of $\beta$-rhamnose during storage when was treated unprecooling, 0.03mm PE film punched and unpunched at -4$^{\circ}C$ was the highest 25.08% and 34.86%, respectively in 50~60days. Content of mannitol was not changed at -4$^{\circ}C$.

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The Microwave Dielectric Properties of $BiNbO_4$ as The Addition of $MoO_3$ ($MoO_3$첨가에 따른 $BiNbO_4$의 마이크로파 유전특성)

  • 박영순;김덕규;김규도;박춘배
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.11a
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    • pp.232-235
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    • 1999
  • In this paper, We described the effect of $MoO_3$ Addition and firing temperature on the microwave dielectric properties of $BiNb0_4$ ceramics. The specimens prepared by conventional mixed method was addicted by 0 - 0.03 wt% $MoO_3$ and fired at 860 - $950^{\circ}$ for 3hr. Density increased when $MoO_3$ is below O.Olwt% but decreased when over O.Olwt%. $BiNb0_4$ ceramics addicted with CuO 0.03wt % and $MoO_3$ 0.01 wt% showed microwave dielectric properties, Dielectric constant 37.5, Quality factor[Qx$f_0$]5500, Temperature coefficient of resonance frequency 15ppm/$^{\circ}$

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Effects of A-Site and B-Site Vacancies on Structural and Dielectric Properties of PLZT Ceramics

  • Jeong, Cheol-Su;Park, Hyu-Bum;Hong, Young-Sik;Kim, Si-Joong
    • The Korean Journal of Ceramics
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    • v.2 no.2
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    • pp.76-82
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    • 1996
  • PLZT ceramics having two nominal compositions, $Pb_{1-3x/2}La_xV_{x/2}(Zr_{03}Ti_{03})O_3$ and $Pb_{1-x}La_x(Zr_{0.2}Ti_{0.5})_{1-x/4}V_{x/4}O_3$ (V: vacancy) with x=0.00~0.30, were prepared. The physical, structural, and dielectric properties were investigated by X-ray diffraction, scanning electron microscopy, Raman spectroscopy, and measurements of bulk density and dielectric constant. The two series with A-stie and B-site vacancies showed different physical, structural, dielectric properties, and, specially, Curie temperature. In comparison to PLZT with B-site vacancies, PLZT with A-site vacancies showed high Curie temperatures and low maxima of dielectric constant. Consequently, it is evident that the properties of PLZT ceramics depend on the vacancy formula adopted as a batch composition in preparation.

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Pilot Scale Experiments on the Oxidation of $TiCl_4$ ($TiCl_4$의 산화반응에 대한 파이롯트 규모 실험)

  • 박균영;이익형;양현수
    • Journal of the Korean Ceramic Society
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    • v.27 no.6
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    • pp.817-823
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    • 1990
  • Pilot-scale experiments on the oxidation of TiCl4 to produce TiO2 were carried out in a verical reactor of 20cm in inside diameter and 140cm in length ; LPG burning was used as a heating means to maintain the reaciton temperature. The effects of reaction temperature and excess oxygen content on the conversion of TiCl4 and on the particle size of produced TiO2 were investigated. The ranges of operating conditions varied were 900 to TiO2 was 0.45-0.57${\mu}{\textrm}{m}$, TiCl4 conversion was 82-96%, the rutile content was 33-57% and the contents of impurities were 0.03% of Fe, 0.03% of SiO2 and 62ppm of Cl. These experimental results were compared with those of other investigators.

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Thermoelectric Properties of N-type 90% $Bi_2Te_3+10%Bi_2Se_3$ Thermoelectric Materials Produced by Melt Spinning Method and Sintering

  • Kim, Taek-Soo;Chun, Byong-Sun
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.459-460
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    • 2006
  • N-type $Bi_2Te_3-Sb_2Te_3$ solid solutions doped with 1$CdCl_2$ was prepared by melt spinning, crushing and vacuum sintering processes. Microstructure, bending strength and thermoelectric property were investigated as a function of the doping quantity from 0.03wt.% to 0.10wt.% and sintering temperature from $400^{\circ}C$ to $500^{\circ}C$, and finally compared with those of conventionally fabricated alloys. The alloy showed a good structural homogeneity as well as bending strength of $3.88Kgf/mm^2$. The highest thermoelectric figure of merit was obtained by doping 0.03wt.% and sintering at $500^{\circ}C$.

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