• 제목/요약/키워드: 03-03

검색결과 11,389건 처리시간 0.043초

Glass 첨가량에 따른 ZnO 바리스터의 전기적 특성 (Electrical Properties of ZnO Varistors with Variation of Glass Addition)

  • 조현무;이종덕;박상만;이성갑
    • 한국전기전자재료학회논문지
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    • 제18권9호
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    • pp.815-820
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    • 2005
  • ZnO varistor ceramics were fabricated with variation of addition of glass-frit amount and the sintering temperature was $1100^{\circ}C$. The average grain sizes were showed increased from $8.6{\mu}m\;to\;10{\mu}m$, and varistor voltages were decreased from 506V to 460V by added amount of glass-frit. Nonlinear coefficient $\alpha$, of all were with increasing the amount of glass-frit more than 70, in case of added on $0.03wt\%$ glass-frit was 83. And leakage current were less than $1{\mu}A$ with applied at $82\%$ of varistor voltage. The clamping voltage ratio of the specimens added $0.03wt\%$ glass-frit was 1.41 at applied 25A $[8/20\;{\mu}s]$. In the specimen added $0.03wt\%$ glass-frit, endurance of surge current and deviation of varistor voltage were $6200A/cm^2,\;\Delta-1.67\%$, respectively and clamping voltage ratio was 2.33. In the Specimen added $0.03wt\%$ glass-frit were superior to any other compositions on High Temperature Load Test(HTLT) for 1000 hr at $85^{\circ}C$, and deviation of the varistor voltage were $\Delta-1.29\%$.

다결정${(Fe,In,Eu)}_2O_3$계의 자기적 성질에 관한 연구 (A Study on the Magnetic Properties of Polycrystailine${(Fe,In,Eu)}_2O_3$)

  • 김정기;서정철;한은주;홍양기
    • 한국자기학회지
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    • 제1권1호
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    • pp.1-5
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    • 1991
  • 다결정${(Fe_{2}O_{3})}_{1-x-y}{(In_{2}O_{3})}_{x}{(Eu_{2}O_{3})}_{y}$(x=0.01, y=0.02과 x=0.02, y=0.03)의 자기적 성질을 X선 회절, $M\"{o}ssbauer$ 효과 방법과 자기이력 측정에 의해서 연구하였다. X선 회절결과는 이들 시료의 결정구조는 $\alpha-Fe_{2}O_{3}$와 같음을 보인다. 사중극자 분열과 평균 반폭치 분석으로부터 x=0.01과 y=0.02인 시료는 Morin 전이를 보이며, x=0.02와 y=0.03시료에서 반 강자성 벡타와 결정축[111]사이의 각은 온도의 증가에 따라 약 $35^{\circ}$로부터 (111) 평면에 놓이기 까지 변한다. 초미세 자기장의 온도 의존성은 스핀파 이론을 써서 분석하였다. 상온에서의 이성질체 이동값은 약 0.35mm/s로 이는 시료내의 철의 이온값은 $3^{+}$임을 의미하는 것이다. 이성질체 이동의 온도의존성은 Delbye모형을 써서 분석하였다.

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Co-Doped Willemite 파란색 안료의 합성과 생성기구 (Synthesis and Formation Mechanism of Cobalt Doped Willemite Blue Pigments)

  • 황동하;한경섭;이병하
    • 한국세라믹학회지
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    • 제47권6호
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    • pp.603-607
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    • 2010
  • Turquoise blue pigment of Vanadium-zircon blue (DCMA number 14-42-2), which was already commercialized, was stable to be reproduced but insufficient to give strong blue. However, it possible to obtain more intense blue by partially substituting cobalt ions into the willemite($Zn_2SiO_4$) lattice classified into DCMA number 7-10-2 for blue ceramic pigment. By the composition of willemite $Co_xZn_{2-x}SiO_4$(X=0.01, 0.03, 0.05, 0.07, 0.09 mole), this study used reagent grade zinc oxide, cobalt oxide and silicon dioxide as starting materials, carrying out the synthesis with solid reaction method by adding $H_3BO_3$ as a mineralizer. The firing temperature was between $1200^{\circ}C$ and $1400^{\circ}C$. The characteristics of synthesized pigment were analyzed by X-ray diffraction, Raman spectroscopy and SEM and the characteristics of color tones were analyzed by UV-Vis spectroscopy and CIE-$L^*a^*b^*$ measurement. As a result, the optimal composition was $Zn_{1.95}Co_{0.05}$ with 1wt% of $H_3BO_3$ as a mineralizer and firing condition was $1350^{\circ}C$/3 h. $L^*a^*b^*$ value was 29.25, 41.03, -59.93 for on glaze pigment and 37.03, 36.41, -60.03 for under glaze pigment.

X-선 조사된 Beta-eucryptite의 열자극 발광 (Thermoluminescence from X-Ray Irradiated Beta-Eucryptite)

  • 김태규;이병용;최범식;강현식;추성실;황정남
    • 한국의학물리학회지:의학물리
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    • 제3권1호
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    • pp.9-18
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    • 1992
  • 4MeV X-선을 제조된 beta-eucryptite 에 조사시 킨 후, 300K-600K 온도 구간에서 열자극 방광을 측정하였다. 혼합되어 측정된 열자극발광 스펙트럼은 342K, 392K, 438K, 474K 과 572K 에서 열자극발광 peak가 나타난다. 527K 의 열자극방광 스펙트럼은 retrapping이 일어나는 2nd kinetic order 임을 알았다. Peak shape 법의 활성화에너지는 1.03eV이었고 이탈진 동수는 3.9$\times$$10^{8}$sec$^{-1}$이었다. 또한 initial rise법과 온도 상승률에 따른 활성화 에너지는 각각 1.19$\pm$0.03eV, 1.02$\pm$0.05eV로 나타났다. 최고의 열자극발광 세기를 갖는 온도 527K를 유지하고 측정한 isothermal decay 스펙트럼에 의한 이탈진동수는 heating rate법의 결과와 유사한 2.8$\times$$10^{8}$sec$^{-1}$이었다. 50Gy의 조사선량 범위까지는 조사선량에 따른 열자극발광 세기의 선형성이 유지되었지만, 그 이상의 영역에서는 supralinearity가 나타난 후 saturation되었다.

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미세단층촬영기(Micro-CT)를 이용한 전자 근관장 측정기의 정확성에 관한 연구 (A Study on the Accuracy of the Electronic Apex Locator Using a Micro-Computed Tomography)

  • 전경진;김양수;남태계
    • 한국정밀공학회지
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    • 제24권8호통권197호
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    • pp.116-121
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    • 2007
  • The length of root canal has to be measured for endodontic treatment. Several electronic apex locators were developed to measure the length of root canal by other researchers. And their accuracies were verified by X-ray or micrometer method. But these methods did not consider the non-linear bends of pulp and had ${\pm}0.5mm$ error which was large enough to measure the length of root canal. The purpose of this study is the introduction of a new method to measure the length of root canal and the verification of the accuracy of an electronic apex locator using a Micro-CT. The length of root canal of 6 teeth were measured with the electronic apex locator. When the electronic apex locator reads 0.5, 0.6, 0.7, 0.8, 0.9 and 1.0 mm length of the file which was inserted in the hole of the tooth to measure the length of root canal. The average (${\pm}$Standard deviation) length of root canal of 6 teeth measured by the Micro-CT was $0.49{\pm}0.03,\;0.59{\pm}0.04,\;0.68{\pm}0.03,\;0.78{\pm}0.03,\;0.90{\pm}0.04\;and\;1.01{\pm}0.03mm$, respectively. The maximum error of the electronic apex locator was 0.06 mm.

Correlations of Physical Fitness Factors, Antioxidant Enzymes, Lipid Peroxidation, Lipid Profiles, Lactate Levels and Cardiovascular Variables in an Exercising Group and Controls

  • Yu, Jae-Ho;Lee, Suk-Min
    • The Journal of Korean Physical Therapy
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    • 제22권3호
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    • pp.61-69
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    • 2010
  • Purpose: This study was designed to investigate correlations between physical fitness, antioxidant enzymes (SOD, CAT, GPX), lipid peroxidation levels (MDA), lipid profiles, lactate levels and cardiovascular variables in an exercising group and a control group. Methods: Twelve healthy young males (Exercise group: 6, Controls: 6). All subjects took physical fitness tests and blood samples were collected while subjects were resting. Results: In the exercise group, there were several significant correlations: between back strength and SOD enzyme levels (r=0.82, p=0.04), back strength and MDA (r=0.94, p=0.00), agility and GPX (r=0.81, p=0.04), and balance and GPX (r=0.81, p=0.04). In the control group, there were significant correlations between: dominant grip strength and MDA (r=-0.84, p=0.03), and agility and GPX (r= -0.82, p=0.04). In the exercise group, there were no significant correlations between physical fitness factors, TC, TG, HDL-C and lactate levels. In the control group, there were significant correlations between: back strength and TG (r=0.88, p=0.01), and agility and HDL-C (r= -0.84, p=0.03). In the exercise group, there were significant correlations between: non-dominant grip strength and SBP (r=0.94, p=0.00), dominant grip strength and SBP (r=0.85, p=0.03), and power and SBP (r=0.82, p=0.04). In controls, there were significant correlations between: dominant grip strength and DBP (r=-0.85, p=0.03), muscular endurance and ST level (r=-0.93, p=0.00), and muscular endurance and HR (r=-0.88, p=0.01). Conclusion: That cardiovascular patients and controls who participated in regular exercise maintained their antioxidant capacity suggests that long-term physical activity can counteract the negative dysfunction that characterizes sedentary lifestyle, probably by maintaining plasma antioxidant defenses and thereby preventing oxidative stress.

Negative Association of the HLA-DQB1*02 Allele with Breast Cancer Development among Jordanians

  • Atoum, Manar Fayiz;Tanashat, Reem Qasem;Mahmoud, Sameer Al Haj
    • Asian Pacific Journal of Cancer Prevention
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    • 제14권11호
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    • pp.7007-7010
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    • 2013
  • Background: In the literature, data concerning the relationship between breast cancer and HLA class II gene polymorphisms are limited, so the aim of this study was to determine if HLA-DQB1 and HLA-DRB1 MHC class-II alleles may confer susceptibility or resistance to the disease among Jordanian females. Materials and Methods: This case control study enrolled 56 Royal Hospital breast cancer patients and 60 age matched healthy controls, all of whom provided blood samples (2011-2013). A questionnaire was filled after signing a consent form and DNA was extracted, nucleic acids being amplified for assessment of HLA-DQB1 and HLA-DRB1 alleles by muliplex INNO-LiPA and allele typing carried out by reverse hybridization. Comparison of HLA-DQB1 and HLA-DRB1 allele distributions was carried out with paired t-test and chi-square statistics. Risk factors were assessed by odd ratios with 95% confidence intervals. Results: A significant negative correlation was observed between $HLADQB1^*$ 02 alleles and breast cancers (p=0.013). No significant associations were observed among $HLADQB1^*$ 03, 04, 05 and 06 or among $HLA-DRB1^*$ 01, 03, 04, 07, 08, 10, 11, 13, 14 and 15. Conclusions: $HLADQB1^*$ 02 alleles may provide positive protection against breast tumor risk among Jordanians, but not $HLADQB1^*$ 03, 04, 05 and 06 or $HLA-DRB1^*$ 01, 03, 04, 07, 08, 10, 11, 13, 14 and 15 alleles.

Fe(III)와 Xylenol Orange의 착물형성에 대한 분광광도법적 연구 (Spectrophotometric Study of the Complex Formation of Ferric Ion with Xylenol Orange)

  • 오대섭;이선행;박정학
    • 대한화학회지
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    • 제22권5호
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    • pp.311-316
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    • 1978
  • Fe(III)과 Xylenol Orange (XO 또는 $H_6A$)의 반응을 분광광도법으로 연구하였다. Fe(III)과 XO는 조성이 Fe(III) : XO = 2 : 1 및 1 : 1 인 두가지 착물을 형성함을 확인하였다. 2 : 1 착물은 XO보다 Fe(III)를 많이 포함한 산성에서 안정하고, 1 : 1 착물은 XO가 많이 포함된 약산성용액에서 안정하다. 흡수극대는 590nm(2 : 1)와 500nm(1 : 1)이고 몰흡광계수는 각각 $3.18{\pm}0.04{\times}10^4,\;1.32{\pm}0.03{\times}10^4$이다. pH값을 변화시키면서 측정한 두 착물의 안정도상수는 $log{\beta}_{21}=18.69{\pm}0.03,\;log{\beta}_{212}=42.08{\pm}0.09,\;log{\beta}_{11}=4.17{\pm}0.04,\;and\;log{\beta}_{113}=34.47{\pm}0.07$이었다.

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Comparison Between ELISA and Gel-filtration Assay for the Guantitation of Airway Mucins

  • Shin, Chan-Young;Kang, Suk-Jo;Kim, Kwang-Chul;Ko, Kwang-Ho
    • Archives of Pharmacal Research
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    • 제21권3호
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    • pp.253-259
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    • 1998
  • In this study, we developed immunoassay methods for the more convenient and effective detection of rat tracheal mucin and the results were compared with those of [$3^H$]glucosamine based gel-filtratioh method. A monoclonal anti-rat tracheal mucin antibody, mAbRT03, which specifically recognizes rat tracheal mucins, was used throughout in this study. To induce mucin secretion, varying concentrations of ATP (0-2 mM) were applied to the primary rat tracheal surface epithelial (RTSE) cell culture which had been metabolically radiolabeled with [$3^H$]glucosamine and the secretion of mucin was analyzed both by the immunoassay and the gel-filtration chromatography methods. For the immunoassay, the following two procedures were employed. 1) Simple ELISA; the culture spent media were directly coated onto the assay plate and the immunoreactivity with mAbRT03 was assessed from the standard curve generated with the purified rat mucin. 2) Inhibition ELISA; A known amount of the purified rat mucin was coated onto the assay plate and then ATP-stimulated culture spent media were added to inhibit the immunorelitivity with mAbRT03. The contents of mucin in the sample were calculated from the standard inhibition curve which was generated with the purified rat mucin. The assay results obtained from the immunoassays were identical with those from the gel-filtration methods. The present result indicates that ELISA can be substituted for the laborious, time-consuming gel-filtration assay in studying the regulation of airway mucin release from cultured airway epithelial cells.

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추출 방식의 차이에 따른 주목약침이 Formalin 유도 통증 모델의 진통에 미치는 영향 (Analgesic Effects of Taxus cuspidata Pharmacopuncture Using Different Extraction Methods on the Formalin-Induced Pain Model)

  • 신유빈;이현종;김재수;이윤규
    • Journal of Acupuncture Research
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    • 제33권3호
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    • pp.17-28
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    • 2016
  • Objectives : This study was designed to investigate the analgesic effects of Taxus cuspidata pharmacopuncture(TCP) at KI03 on formalin-induced pain in rats and to evaluate the efficiency of different extraction methods of Taxus cuspidata(TC). Methods : 30 rats were divided into 5 groups, each consisting of 6 rats. Each of the groups was treated two times. The first treatment for its right KI03 was as follows: rats were treated with normal saline(NOR), normal saline(CON), hot-water extraction of TC(W), ethanol extraction of TC(E), and ultrasonification extraction of TC(U). The second treatment was given 35 mins after the first one. Rats in NOR were treated with normal saline at their hind-paw. All groups, except NOR, were treated with formalin(5 %, $40{\mu}{\ell}$) at their hind-paw. To evaluate pain behavior, Ultrasonic vocalization(USV) was examined to be around 18~30 kHz. After analysis of USV, blood samples were taken from the rats for analysis of Substance P, aspartate aminotransferase(AST) and alanine aminotransferase(ALT). Results : In the experimental groups, USV was significantly decreased compared with CON and similar to that of NOR in the early phase. But there were no significant differences among the three extraction methods of TC. In addition, Substance P of W was significantly decreased. AST and ALT activation showed no significant differences among the 5 groups. Conclusion : These results show that regardless of extraction methods of TC, TCP at KI03 has analgesic effects in the early phase on formalin-induced pain in rats. In particular, hot-water extraction of TC significantly reduces Substance P activation.