• Title/Summary/Keyword: -energy-dispersive x-ray-

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Formation Characteristics of Environment Friendly Electrodeposit Films Formed in Natural and Synthetic Seawater Conditions (천연 및 인공해수를 이용하여 제작한 환경친화적인 전착코팅막의 형성 특성)

  • 이명훈;이찬식
    • Journal of Advanced Marine Engineering and Technology
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    • v.28 no.6
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    • pp.1000-1009
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    • 2004
  • The environment friendly calcareous deposit films were formed on steel plates by electrodeposition technique in natural seawater and synthetic solutions such as dissolved $\textrm{Mg}^{2+}$ and $\textrm{Ca}^{2+}$ ions at various potential conditions. The influence of potential conditions on composition ratio, structure and morphology of the electrodeposited films were investigated by scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS) and X-ray diffractor (XRD). Accordingly, this study was provided a better understanding of the composition between the growth of $\textrm{Mg(OH)}_2$ and that of $\textrm{CaCO}_3$ during the formation of calcareous deposit films on steel substrate under cathodically electrodeposition in synthetic and natural seawater. The results showed that the formation of good overall calcareous deposited film in seawater can be achieved by controlling the Ca/Mg ratio according to interfacial pH with the effective use of the electro deposition technique.

Electrical discharge machining of $TiC/Al_2O_3$ Ceramic Composite (탄화티탄/알루미나 세라믹 복합체의 방전가공)

  • Wang, D.H.;Woo, J.Y.;Ahn, Y.C.
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.9
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    • pp.80-89
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    • 1997
  • Die sinking electrical discharge machining(EDM) was conducted for ceramic composite of 33 weight percent TiC based on AI$_{2}$O$_{3}$ ceramic matrix according to the change of current and duty factor(DF). Material removal rate(MRR) was increased as the current and the duty factor increased, but better surface mor-pholoty was obtained in the region of lower current and duty factor. From the scanning electron microscopy(SEM) photographs and the energy dispersive X-ray spectroscopy(EDX) of the EDMed surface, EDM trace formed by one discharge spark was analyzed. Although the bending strength after EDM was highly decreased, reliability obtained by weibull analysis was increased twice. The bending strength was recovered or more by barrel polishing after EDM. From the FEM analysis of temperature for one spark, the possible melting region of AI$_{2}$O$_{3}$and TiC was obtained.

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A Study on Electrically Assisted Solid State Joining of Aluminum and Copper (알루미늄과 구리 간 통전고상접합 연구)

  • Park, J.W.;Choi, H.;Lee, S.;Jeong, H.J.;Hong, S.T.;Han, H.N.
    • Transactions of Materials Processing
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    • v.29 no.1
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    • pp.49-54
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    • 2020
  • The influence of electric current on the joining properties of aluminum and copper was investigated. Various pulsed electric current conditions were set to the joining specimens followed by pressure. The shear strength of the joint area between aluminum and copper was measured by the lab shear test. In addition, the microstructures of the joint area were observed through a field emission scanning electron microscope, energy dispersive X-ray, and electron backscatter diffraction. The mechanical properties of each phase in the joint region were measured by nano-indentation. As a result, it was confirmed that electrically assisted solid state joining of copper and aluminum could be applied in various industrial fields.

The Variation of Sedimentary Rock Strength due to Weathering (풍화에 따른 퇴적암의 강도 변화)

  • 배우석;이봉직;오세욱;이종규
    • Journal of the Korean Society of Safety
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    • v.18 no.1
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    • pp.89-93
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    • 2003
  • The failure of rock slopes were influenced by weathering, which causes change in the shear strength. The weathering is also directly related to slaking and swelling characteristics. In the paper, the core of diameter loom was obtained by digging on rock slope of Kong-ju in Korea and then EDX(Energy Dispersive X-ray spectrometer) analysis was carried out to verified element of chief rock-forming minerals. Uniaxial compression tests, slaking tests, and point load test are performed to study engineering characteristics of conglomerate and red shale. As a results of slaking test, slaking index of conglomerate indicate range of 85.11-99.58 and shale indicate 58.37-99.23. Therefore, it is recognized that the resistance of shale to weathering decreases in shallow depth and it greatly influences the strength of rock. The result of uniaxial compression test and Point load test show that the strength of sedimentary such as conglomerate and red shale has an influence on both weathering and saturation.

Behavior of the Temperature Coefficient of Resistance at Parallelly Connected Resistors (병렬로 접속된 저항체에서 저항온도계수의 거동)

  • Lee, Sunwoo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.31 no.2
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    • pp.98-101
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    • 2018
  • In this paper, we discuss the fabrication of metal alloy resistors. We connected them in parallel to estimate their resistance and temperature coefficient of resistance (TCR). The fabricated resistors have different resistances, 5 and $10{\Omega}$ and different TCRs, 50 and $200ppm/^{\circ}C$. Each resistor was confirmed to have the correct atomic composition through the use of energy dispersive X-ray (EDX). The resistors' electrical properties were confirmed by measuring resistance and TCR. The resistance and TCR of the resistors connected in parallel were estimated through the increase in resistance due to the increase in temperature, and were compared with the measured values. We are confident that this TCR estimation technique, which uses the increase in resistance due to temperature, will be very useful in designing and fabricating resistors with low and stable TCR.

On the Surface Defect Analysis of an Aluminum Tube for an OPC Drum using n SEM and EDX (SEM/EDX를 이용한 OPC 드럼용 Al 튜브의 표면결함 분석에 관한 연구)

  • Kim, Chung-Kyun
    • Tribology and Lubricants
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    • v.23 no.4
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    • pp.143-148
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    • 2007
  • The surface defects of an aluminum tube for an OPC drum have been analyzed using a scanning microscopy(SEM) and an energy dispersive X-ray analyze.(EDX). The SEM/EDX system, which may provide good information on the surface defects and their distributions, provides an optical diameter of an impurity and a chemical composition. These are strongly related on the coated film thickness and quality of an OPC drum, which is a key element of a toner cartridge for a laser printer. The experimental results show that the local deformations, scratch wear, and flaws are produce the non-uniform coating layers, which may be removed by a manufacturing process of an aluminum tube. The major parameters on the coating quality of an OPC drum are the impurities of an aluminum tube such as silicon, oxygen, calcium, carbon, sulphur, chlorine, and others. These impurities may be removed by an ingot molding, extrusion and drawing, quality control, and packing processes with a strict manufacturing technology.

Evaluation in Performance of High Voltage Cable for BLU of TFT-LCD by Improvement for Material and Manufactured Process (TFT-LCD BLU용 고압 케이블의 재료특성 및 제조공정 개선을 통한 성능 향상)

  • Chung, Jin-Do;Kim, Jae-Hoon;Koo, Kyung-Wan;Hwang, Seung-Min
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.58 no.4
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    • pp.495-498
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    • 2009
  • To improve the efficiency of the high voltage cable for BLU(backlight unit) of TFT-LCD(Thin Film Transistor-Liquid Crystal Display), the analysis for the trial products(UL3239, UL3633) is conducted by using SEM(scanning electron microscope) and EDX(Energy Dispersive X-ray Spectroscopy). The result that it is possible to accumulate the know-how to about stranding pitch through effective improvement of stranding process. The troubles which are the badness of withstanding voltage and tensile strength etc. are solved by development of excellent material. Furthermore, phenomenon of conductor unfasten in the harness work is solved by improvement of the stranding wire process.

Investigation About Surface Microstructure of Aluminum with Change of Voltage, a Period of Treatment and Density of Electrolyte in Micro-Arc Oxidation Treatment (MAO(Micro-Arc Oxidation) 공정 중 인가 전압, 반응 시간, 전해액 농도에 따른 알루미늄의 표면 미세조직 평가)

  • Yeo, In-Chul;Kang, In-Cheol
    • Journal of Powder Materials
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    • v.18 no.6
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    • pp.575-582
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    • 2011
  • MAO(Micro-Arc Oxidation) method was used to make $Al_2O_3$ surface on 6063 Al specimen. This study was focused on an influence of voltage, density of electrolyte and a period of treatment on the change of surface microstructure by using SEM(Scanning Electron Microscope), EDS(Energy Dispersive X-ray Spectroscopy). The microstructure shows higher roughness and thicker oxidized layer with increase of voltage and maintaining period of treatment. The density of electrolyte affected a formation of more dense surface and increase of a oxidized layer.

A Study on individual Diesel Particles by SEM/EDX (SEM/EDX를 이용한 디젤 분진의 입자별 분석)

  • 김혜진;이종태;김동술
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.2
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    • pp.175-182
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    • 1999
  • Scanning electron microscopy (SEM) has played an important role in receptor modeling area because it is a powerful tool for characterizing individual particles. The purpose of the study was to classify individual diesel particles base on statistical analysis and image analysis by SEM/EDX (energy dispersive x-ray analyser). The diesel particles were sampled by both a modified CVS 75 mode and a high speed mode with a chassis dynamometer. The SEM/EDX system provides various physical parameters including particle's particle diameter and chemical information. Thus density and mass of the diesel particle were estimated cased on its chemical composition and further fractal dimensions of the diesel particle were obtained by the Hurst exponent method. The fractal dimension in the sample of modified CVS 75 mode was higher than the high speed mode. Finally, mass fractions for a diesel vehicle as a source profile were estimated cased on a particle class concept.

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