• Title/Summary/Keyword: 화학적 성분 분석

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Effect of Proline on First Polar Body Formation in Porcine Primary Oocyte

  • Oh, H. J.;Lee, E. J.;B. C. Yang;W. K. Chang;Kim, J. S.;J. K. Lim;Y. K. Yeo;M. A. Della-Fera;Park, Y. S.
    • Korean Journal of Animal Reproduction
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    • v.26 no.2
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    • pp.165-171
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    • 2002
  • Follicular fluid (FF) contains an oocyte maturation inhibitor with unknown chemical properties. This study was carried out to chemically define the factor(s) inhibiting cumulus cell denudation (CD) and first polar body formation (PBF). Porcine FF (PFF) was extracted with methanol and the extract was serially separated using gel filtration on Superose 12 and Superdex columns. A Superdex fraction was derived with PITC and analyzed with an amino acid analysis column. The results obtained are as follows; PFF had an activity inhibiting both CD and PBF of porcine primary oocytes. Superdex fractions RV2.11 prepared from PFF exhibited an activity inhibiting CD and PBF. By amino acid analysis, the fraction RV2.11 appeared to be proline having the same activity inhibiting CD and PBF. In conclusion, PFF had oocyte maturation inhibitors, of which proline should inhibit CD and PBF.

Chitin 및 Chitosan의 탈단백 및 탈아세틸화도 측정과 지방흡착특성의 확인을 위한 근적외선 분석법의 이용

  • 송호수;김경태;황선영;박성민;이근태
    • Proceedings of the Korean Society of Fisheries Technology Conference
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    • 2001.10a
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    • pp.95-96
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    • 2001
  • 수산식품의 품질검사를 위한 기존의 분석법들은 대부분 각종 무기 및 유기 시약을 이용한화학적 분석이 주로 이용되어지고 있으며, 이와 같은 화학적 분석 방법들은 시료의 전처리부터 최종 결과를 도출하기까지 상당한 시간이 소요되며, 분석자의 숙련도에 따라 결과의 재현성이 달라지는 단점들을 지니고 있다. 이에 비해 분광학적 분석 방법중의 하나인 근적외선(Near-Infrared) 분광분석법은 식품의 구성성분을 분석하는 비파과 측정법 중에서 가장 발전된 방법이라 할 수 있다. (중략)

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The Composition and Physico-chemical Characteristics of Municipal Solid Waste in National park area of Kyungnam-do (경남국립공원지역 폐기물의 성상 및 물리·화학적 특성연구)

  • Lee, Keon-Joo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.14 no.3
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    • pp.138-147
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    • 2006
  • In this study, the composition and physico-chemical characteristics of municipal solid waste (MWS) which was treated in national park area kyungnam-do landfill were investigated. It is necessary to measure the characteristics of MSW and sludge to build a waste treatment facility, the data-base and total managing of the landfill. This MSW was composed of 34.62% of food wastes, 36.05% of papers, 15.37% of plastics & vinyls, 2.28% of textiles, 3.33% of wood, 0.49% of rubber & leathers and others, respectively. Most of MSW are composed of food, paper and plastic waste and more than 90% was combustible waste. For three components, moisture is 29.84%, combustible component is 62.30% and ash is 7.86%. The chemical element has the high order of carbon, oxygen, hydrogen on the dry basis of wastes. Also, the low heating value of the MSW which is measured by calorimeter is calculated as 2377.8kcal/kg. low heating value of the sludge is calculated as 338.06kcal/kg.

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The Study of Two-dimensional Chemical Distribution about Soil using Laser Spectroscopy (레이저 분광법을 활용한 토양 2차원 화학적 분포도 검출 연구)

  • Yang, Jun-Ho;Yoh, Jai-Ick
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.45 no.6
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    • pp.523-530
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    • 2017
  • Laser-Induced Breakdown Spectroscopy (LIBS) which a plasma is irradiated at a specific wavelength depending on the material when a high-energy laser is irradiated, and a Raman spectroscopy which measures rotation and vibration in molecules as light-scattering phenomenon occurs, are attracting attention as a space exploration technology because of the advantages of high accuracy and real-time analysis, and the ability to perform long-range detection. In this study, the tendency of the laser spectrum according to the change of the soil component was analyzed by laser spectroscopy and the two - dimensional chemical distribution was conducted based on the trend of laser spectrum. We have also established the environment of Mars (4-7 torr) and lunar atmosphere (<1 torr) in experimental setup, to prove that it is possible to measure by difference of soil chemical composition using LIBS and Raman spectroscopy even in artificial space environment.

Chemical Characterization of Commercial Vinegars (식초의 종류별 화학성분의 특징)

  • Yoon, Hee-Nam
    • Korean Journal of Food Science and Technology
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    • v.31 no.6
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    • pp.1440-1446
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    • 1999
  • Fourty-two commercial vinegars were analyzed for their non-volatile organic acids, free sugars. amino acids, and volatile compounds. A study was made to characterize commercial vinegars chemically into three kinds of vinegars such as spirit, cider, and brown rice vinegars. Sixteen chemical components were significantly effective for the chemical characterization of commercial vinegars by stepwise discriminant analysis. Those were malic, succinic and lactic acids from the non-volatile organic acids; fructose and glucose from the free sugars; lysine, serine, leucine, valine and alanine from the amino acids; 1-hexanol, acetaldehyde, 3-methyl-1-butanol, 2-methylpropanoic acid, isopropyl butanoate and ethanol from the volatile compounds. Six components including malic acid, lysine, succinic acid, glucose, lactic acid and 1-hexanol were the most significant contributors to the differentiation of commercial vinegars into spirit, cider, and brown rice vinegars. In particular, cider vinegars could be characterized to be abundant in amounts of malic acid and 1-hexanol, whereas brown rice vinegars in amounts of lysine and lactic acid compared to spirit vinegars.

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Physical and Chemical Properties of Waste Glass as Feed Materials for the Production of Foamed Glass (발포유리 원료로서 폐 유리의 물리 화학적 특성)

  • Lee, Chul-Tae
    • Applied Chemistry for Engineering
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    • v.16 no.3
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    • pp.440-448
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    • 2005
  • Physical and chemical properties of waste glass, such as bottle glass, plate glass, and LCD glass were investigated to test the feasibility of starting materials for the production of high quality foamed glass for insulating grade construction material without pre-treatments such as cleaning, and waste removals. For this purpose, chemical analysis, thermal analysis, crystalline analysis, and rheological analysis including viscosity were proceeded and the preparation of foamed glass under the qualitative conditions obtained from these various analysis was also attempted. Overall results of various analysis and investigations for these waste glass showed that waste bottle glass and plate glass have high possivility of use as feed materials for the production of foamed glass.

A TECHNIQUE TO OPTICALLY DETERMINE THE STOICHIOMETRY OF $C_2$ GROWN LITHIUM NIOBATE CRYSTALS (Czochralski법으로 성장시킨 $LiNbO_3$단결정의 화학양론(Stoichiometry)을 결정하기 위한 광학적 방법)

  • Kim, You-Song
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.1 no.2
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    • pp.1-14
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    • 1991
  • In growing single crystals, which exhibit incongruent melting behavor, it is extremely difficult to maintain the stoichiometry of its chemical compositions for given crystals. For instance, $LiNbO_3$ is a typical one which exhibits such incongruent melt, especially with a large solid solution region that makes it difficult to maintain the chemical compositions. Such a variation can then cause a serious problem for the practical applications in designing a precision electro /optic device. Of the known methods of determining its composition and quality, an optical technique of measuring refractive index of the crystals has been implemented. This technique is also capable of determining optical uniformity of the grown crystals and the chemical compositions. The technique used for such characterizations is herein described and some of results are discussed.

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Physical and Chemical Variation of Sedimentary Rocks due to Weathering (풍화에 의한 퇴적암의 물리-화학적 변화)

  • Kim, Young-Su;Heo, No-Young;Jeong, Woo-Seob;Rui, Da-Hu;Lee, Jea-Ho
    • Journal of the Korean GEO-environmental Society
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    • v.3 no.2
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    • pp.49-60
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    • 2002
  • A study on mineral composition and chemical component governing of weathering process is necessary to know the weathering characteristics of sedimentary rocks. In this study, a mineral and chemical component analysis, and physical and engineering characteristic tests were conducted to find out the characteristics of sedimentary rocks in Daegu, according to the weathering degree of sedimentary rock. Test results show that the mineral composition of rock, such as Albite (Ab), Muscovite (Ms), Magenetite (Mt) and the chemical composition of $A_2O_3$, CaO, $Na_2O$, $K_2O$, MgO and so on are closely related to the weathering. Based on the test results, we illustrated the quantitative application of weathering decision for the sedimentary rocks.

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Petrography and Mineral Chemistry of Some Deep Sea Basaltic Rocks from the Western Caroline Ridge and Yap Trench-Arc System (서부 캐롤라인 해령과 얍 해구-열도계의 해저 현무암질암에 대한 암석 기재 및 광물화학)

  • Park Jun-Beom;Kwon Sung-Tack;Ahn Jung-Ho;Kang Jung-Keuk
    • The Journal of the Petrological Society of Korea
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    • v.1 no.1
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    • pp.71-84
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    • 1992
  • This paper reports the results about the petrography and mineral chemistry of 13 representative dredged basaltic rocks from the western Caroline Ridge (WCR) and Yap Trench-Arc system, and provides the chemical and tectonic informations based on the compositions of clinopyroxene phenocrysts. Compositions of olivine phenocrysts in some analyzed samples are Fo$_{86-80}$. Plagioclase phenocrysts have variable compositions ranging from An$_{90}$ to An$_{55}$. The compositions of clinopyroxene phenocrysts vary according to geological environments; titansalite in atoll and guyot of WCR, diopside-augite in trough and bank of WCR, and endiopside in Yap Trench-Arc system. Application of the discrimination schemes proposed by Leterrier et al. (1982) suggests: (1) the samples from atoll-guyot belong to within plate alkali basalt, implying that western CR could be the continuation of eastern CR formed by hot spot magmatism, (2) the samples from the Yap Trench-Arc system with no present-day magmatism clearly indicate the occurrence of orogenic tholeiites presumably related to early island arc magmatisms in this area, however, (3) the samples from the bank and trough do not provide definitive informations, which might indicate the complexity of their origins.

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Thermal Changes of Aroma Components in Soybean Pastes (Doenjang) (된장 가열조리 시 생성되는 향기성분 변화)

  • Lee, Seung-Joo;Ahn, Bo-Mi
    • Korean Journal of Food Science and Technology
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    • v.40 no.3
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    • pp.271-276
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    • 2008
  • In this study, volatile compounds were isolated from traditional and commercial fermented soybean pastes according to different heating temperatures (room temperature, $50^{\circ}C$, $100^{\circ}C$) using headspace-solid phase microextraction (HS-SPME). The compounds were then analyzed by gas chromatography-mass spectrometry (GC-MS). A total of 51 volatile components, including 18 esters, 3 alcohols, 6 acids, 8 pyrazines, 5 volatile phenols, 6 aldehydes, and 5 miscellaneous compounds, were identified. Esters and acids such as ethyl hexadecanoate, acetic acid, and 2/3-methyl butanoic acid were the largest groups among the quantified volatiles. By applying principal component analyses to the GCMS data sets, differences were observed in the volatile components of the soybean pastes as to the different heating temperatures. A large variation was shown between the volatile components of the traditional and commercial soybean pastes by increasing the heating temperature. Commercial samples had significantly higher levels of longer chain ethyl esters, aldehydes, and thermal degradation products such as maltol and 2-acetyl pyrrole, while traditional samples showed higher concentrations of acids and pyrazines.