• Analytical Science and Technology
• /
• v.7 no.2
• /
• pp.233-236
• /
• 1994

To evaluate the emulsion stability indices of W/O emulsion system, we developed the simple and sensitive "VOLUMETRIC METHOD". This technique involved the first step of homogenizing the milk fat-water system with Ultra-turrax T25, then the volume of the added water phase was measured immediately. After quiescent incubation in test tubes at room temperature for a desired storage time, the bottom volume of the separated water layer was measured. And then "emulsion stability index(ESI)" was calculated by the following equation : $ESI=(1-V_s/V_a){\times}100$, where $V_a$ means the volume of the added water in the W/O emulsion and $V_s$ represents the volume of the separated water in the W/O emulsion for a desired storage time. The emulsion stability indices of W/O emulsion system at sorbitan trioleate, span 60, and tween 20 were $95.4{\pm}1.8$, $56.1{\pm}2.8$, and $41.6{\pm}2.2$ respectively. Furthermore, the differences between "VOLUMETRIC METHOD" and "Titus et al method" were less than 5.0 of ESI Value.

• Analytical Science and Technology
• /
• v.7 no.2
• /
• pp.225-232
• /
• 1994

The podands I-VII, acyclic polyethers, expected high extractability for $Ag^+$ against $Pb^{2+}$ were designed and synthesized with high yields. Using podands I-VII as extractants, the %extraction(%Ex) of $Ag^+$ and $Pb^{2+}$ as picrates were determined in water/chloroform systems. The stability constants(log K) for the complexation of $Ag^+$ with podands I-VII were also determined by potentiometry. %Ex($Ag^+$) were proportional to the numbers of substituted sulfur donor atoms. Podand VI(log K : 7.65) having 3 substituted sulfur and podand VII(log K : 9.15) having 4 substituted sulfur, however, exhibited almost 100% of extractability, respectively. In %Ex($Ag^+/Pb^{2+}$, oxygen-sulfur mixed donor podands(IV-VII) showed the higher values. Otherwise, the values of log K and %Ex($Ag^+$) largely depended on the variation of donor-site of sulfur. From the results of NMR experiments, it seems that it is due to the ${\pi}-{\pi}$ stacking interaction between the aromatic end-groups.

• The Korean Journal of Pesticide Science
• /
• v.8 no.2
• /
• pp.137-144
• /
• 2004

[ $\beta$ ]-Ketoacetoanilide chloride derivatives containing a substituent at 4 in phenyl group (para) reduced specifically the development of tomato late blight caused by Phytophthora infestans. Among $\beta$ketoacetoanilide chloride derivatives, five (KIST163, KIST170, KIST260, KIST263, and KIST267) were selected and tested for their protective, curative, systemic, persistent activities, and disease control efficacy against tomato late blight on adult plants. They exhibited a strong l-day protective activity and $EC_{50}$ of KIST163 and KIST170 were 21.9 and $14.5{\mu}g/mL$, respectively. However, they had little curative and systemic activities. Good persistence of KIST163 and KIST170 on tomato plants were observed against P. infestans; both KIST163 and KIST170 at $100{\mu}g/mL$ showed control values more than 75% in a 7-day protective applications. In addition, the two chemicals effectively controlled the occurrence of P. infestans on adult tomato plants. These results indicate that five $\beta$-ketoacetoanilide chloride derivatives are foliar fungicides with a preventive action and KIST163 and KIST170 have a potential for the control of tomato late blight in the fields.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
• /
• v.11 no.4
• /
• pp.259-269
• /
• 2013

Applicability of ammonium molybdophosphate/iron oxides-polyacrylonitrile (AMP/IO-PAN) composites on the removal of radionuclides in the radioactive wastewater generated from nuclear power plants was investigated. The composites were characterized using the following analytical techniques: X-ray diffraction (XRD), Fourior transform-infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), particle size analyzer (PSA), nitrogen adsorption-desorption and magnetic property measurement system (MPMS). 10wt% of AMP/IO-PAN composite has a saturation magnetization of 2.038 emu/g. Single-solute sorptions of Co, Sr and Cs onto 10wt% of AMP/IO-PAN composite were investigated. The maximum sorption capacities ($Q^0$) predicted by the Langmuir model on 10wt% of AMP/IO-PAN composite were 0.097, 0.086 and 0.66 mmol/g for Co, Sr and Cs, respectively. The maximum sorption capacities ($Q^0$) of Cs predicted by Langmuir model on 0, 10, 20 and 30wt% of AMP/IO-PAN composites were 0.702, 0.655, 0.602 and 0.559 mmol/g, respectively. The maximum sorption capacities ($Q^0$) of Cs decreased with increasing the iron oxide content in the AMP/IO-PAN composites.

• Journal of Animal Science and Technology
• /
• v.44 no.4
• /
• pp.483-490
• /
• 2002

The aim of this study was to determine if a low-molecular weight casein hydrolysate has an anti- hypertensive effect in spontaneously hypertensive rats (SHR). Prior to the in vivo experiment, the casein hydrolysate was confirmed to be resistant to gastrointestinal digestion by confirming the retention of its potency as an inhibitor of angiotensin I-concerting enzyme after incubation with pepsin, trypsin, or chymotrypsin. The in vivo anti-hypertensive effect of the hydrolysate was determined by the tail cuff method. Following an oral administration of the hydrolysate solution, the systolic blood pressure (SBP) decreased by 12.9% (－28.9mmHg; P<0.05) at 3 h after the administration at a dose of 500mg/kg body weight. When the hydrolysate was administered as an emulsion with 30% egg yolk, its anti-hypertensive effect was even more greater at the same dose(－30.8mmHg or －15.9%; P<0.01). In a 50-day long-term trial where the casein hydrolysate was administered once a day, the SBP-lowering effect of the hydrolysate was apparent (P<0.05) from day 35 through the end. Moreover, organ weights and plasma glutamate oxaloacetate transaminase and glutamate pyruvate transaminase activities of the administered SHR were not significantly different from those of controls at the end of the long-term trial.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
• /
• v.3 no.3
• /
• pp.193-200
• /
• 2005

[ $^{14}C$ ] and $^{3}H$ in the evaporator bottom (EB) discharged from the Nuclear power plant (NPP) were extracted simultaneously into a gaseous $^{14}CO_{2}$ and liquefied HTO by using the chemical oxidation, which is the method to oxidize samples completely using potassium persulfate and sulfuric acid. The extracted $^{14}C$ and $^{3}H$ were counted by the liquid scintillation counter (LSC) after the quench correction. To examine the recovery of $^{14}C$ using the radioactive standards, $Na_{2}^{14}CO_{3}$, $^{14}C-alcohol$, and $^{14}C-toluene$ as $^{14}C$, and HTO as $^{3}H$ were used. Also, the most suitable method for oxidizing $^{14}C-toluene$, which is difficult to be oxidized, was investigated through FT-IR spectra according to the concentration of sulfuric acid. With the identical method, $^{14}C$ and $^{3}H$ in the EB generated in the NPP were assayed in the range of $8.35{\sim}l.38{\times}10^3$ Bq/g and $2.46{\times}10^2{\sim}1.40{\times}10^4$ Bq/g, respectively.

• Applied Biological Chemistry
• /
• v.13 no.3
• /
• pp.187-191
• /
• 1970

This experiment was carried out to isolate osmophilic yeasts for higher concentration of NaCl than 20 per cent may affect greatly the fermentation of soy sauce. 6 strains of yeasts were selected from the soy sauce mashes at the fermentating periods and identified observing their morphological characteristics. Their salt-resistance and effects upon the flavor of soy sauce were examined. The results obtained were as follows: (1) The strain $T_3,T_5,$ and $T_{11},\;T_8,\;T_9,\;and\; T_{10},$ selected were identified Saccharomyces cerevisiae group II, Debaryomyces nicotianae, Saccharomyces chevalieri, Saccharomyces rouxii and Saccharomyces rosei, respectively. (2) They were more salt-resistant on the liquid media than on the solid media in the case of cultures on the media containing more than 26 per cent of NaCl. (3) They were grown on the media containing 5-23 per cent of NaCl better than containing none of NaCl. (4) The strain $T_3,\;T_8,\;T_9,\;and\; T_{10}$ were grown on the media containing up to 28 per cent of NaCl, and $T_5\;and\;T_{11}$ up to 32 per cent of NaCl is the case of liquid cultures. (5) Among them, the strain $T_9$ showed the best alcohol fermentation ability and the best fermentative flavor, and $T_5\;and\;T_{11}$ formed moldy smell and pellicle.

• Polymer(Korea)
• /
• v.38 no.4
• /
• pp.550-556
• /
• 2014

Recently, the peptide(or protein)-polymer hybrid materials (PPs) were sought in many research areas as potential building blocks for assembling nanostructures in selective solvents. In PPs, the facile routes of preparing well-defined peptide-polymer bio-conjugates and their specific activities in various applications are important issues. Our strategy to prepare the peptide-polymer hybrid materials was to combine atom transfer radical polymerization (ATRP) method with solid phase peptide synthesis. The standard solid phase peptide synthesis method was employed to prepare the PYGK (proline-tyrosine-glycine-lysine) peptide. PYGK is an analogue peptide, PFGK (proline-phenylalanine-glycine-lysine), which interacted with plasminogen in fibrinolysis. The peptide and the peptide-initiator were characterized with MALDI-TOF mass spectrometry and $^1H$ NMR spectrometer. The peptide-polymer, pSt-PYGK was characterized by GPC, IR, $^1H$ NMR spectrometer and TLC. Spherical micellar aggregates were determined by TEM and SEM. Current synthesis methodology suggested opportunities to create the well-defined peptide-polymer hybrid materials with specific binding activity.

• Journal of agricultural medicine and community health
• /
• v.42 no.2
• /
• pp.79-86
• /
• 2017

Objectives: Metabolic syndrome and depression are interconnected disorders. Although many studies have assessed the association between dietary intake and each disorder independently, few studies have examined the association between depression and dietary intake in patients with metabolic syndrome. Our study examined the association between depression and dietary intake in adults with metabolic syndrome. Methods: We analyzed the second data set (2014) from the sixth KNHNES. Of the patients with metabolic syndrome, the final study population comprised 1,334 patients, aged 20 to 60 years, with metabolic syndrome as defined by KNHNES and depression diagnosed by a physician. We examined the patients' dietary intake obtained using the 24-h recollection method in KNHNES. Results: Depression group had a lower niacin dietary intake than those without depression in both male and female (male P=0.047, female P=0.025). None of the other components had any association between depression group and those without depression group in both male and female. Conclusions: This study demonstrates that a low dietary intake of niacin may be related to the depression in patients with metabolic syndrome. The results indicate that it is worthwhile to evaluate the nutritional status in patients who have been diagnosed with both metabolic syndrome and depression.

• Journal of Digital Convergence
• /
• v.12 no.12
• /
• pp.633-641
• /
• 2014

The purpose of this study was to grasp relationship between obesity and dental caries. A research was performed by utilizing raw data of the 3rd year(2009) in the 4th term for Korean National Health and Nutrition Examination Survey, which is a survey of health and nutrition in the national unit for the Republic of Korea. The research subjects are finally 7,393 people except the subjects with missing of variables relevant to obesity and dental caries among adults aged over fully 19 years old. Data analysis was used SPSS 18.0 program. As a result of analyzing with significant level in 0.05, the following conclusions were obtained. 1. Overweight(${\beta}$ = -0.12, p = .02) was indicated to be low in number of DT pieces compared to normality. 2. Obesity(OR = 0.69, 95% CI: 0.57, 0.84) was indicated to be low in possibility of having DMFT compared to normality. 3. Overweight(${\beta}$ = -0.39, p = .02) and obesity(${\beta}$ = -0.70, p<.0001) was indicated to be low in number of DMFT pieces compared to normality. And to conclude, obesity(body mass index) and dental caries(DT, DMFT) were found to have negative correlation. A significant result was indicated even after adjusting confounding variables.