• Title/Summary/Keyword: 표준 시편

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Development of Coercivity Measuring System for Ferromagnetic Materials in Open Magnetic Circuit (개방자기회로에서 강자성재료의 보자력 측정장치 개발)

  • 유권상;박진습
    • Journal of the Korean Magnetics Society
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    • v.10 no.6
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    • pp.297-301
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    • 2000
  • Coercivity is defined as the magnetic field strength required to reduce the magnetic polarization to zero of magnetic specimen which has been previously magnetized to saturation. This quantity is a reference for classifying soft and hard magnetic materials. We have constructed the measuring system for measurement of coercivity of ferromagnetic materials in open magnetic circuit. The measurement range of the constructed system is from tens A/m to tens kA/m, the combined uncertainty is ${\pm}$0.22 kA/m as coercivity is 14.63 kA/m.

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Thermo-Oxidative Stability of Epoxy/Carbon Fiber Composites under Thermal Cycling Conditions (반복되는 열주기환경에 노출된 에폭시/탄소섬유 복합재료의 열산화 안정성 연구)

  • 남재도
    • The Korean Journal of Rheology
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    • v.10 no.2
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    • pp.106-112
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    • 1998
  • 항공기용 소재로 개발된 에폭시/탄소섬유 복합재료가 매트릭스의 유리전이온도에 육 박하는 온도주기를 경험할 때 발생하는 복합재료의 구조 및 물성변화를 실험과 모델링을 통 하여 연구하였다. 복합재료의 표준 경화온도인 177$^{\circ}C$에서 2시간 체류시킨후 냉각시키는 바 복 열주기는 복합재료를 취약하게 하여 결국 표면에서부터 미세크랙이발생한다는 것을 알수 있었다. 이러한 열주기에 따른 미세크랙 현상은 매트릭스의 분해반응이 발생할수 있는 유효 표면적을 증가시키고 크랙을 통하여 산소의투과를 용이하게 함으로서 산화반응을 가속화하 여 복합재료시편의 무게감소를 가속화시키는 것으로 판단된다. 특히 본 연구에서는 등온과 등속도 승온조건을 주기적으로 반복하는 열주기 조건을 해석하기 위하여 열주기 조건을 특 정온도에서의 등오시간으로 전환할 수 있는 e-quivalent cycle time(ECT)를 제안하였고 이 를 이용하여 열주기에 의한 복합재료 손상의 가속/감속 현상을 규명할수있었다.

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Dielectric passivation effects on the electromigration phenomena in Al-1%Si thin film interconnections (A1-1%Si 박막배선에서 엘렉트로마이그레이션 현상에 미치는 절연보호막 효과)

  • 김경수;김진영
    • Journal of the Korean Vacuum Society
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    • v.10 no.1
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    • pp.27-30
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    • 2001
  • Electromigration Phenomena in Al-1%Si thin film interconnections under DC and PDC conditions were investigated. Thin film interconnections with $SiO_2$ and PSG/$SiO_2$ dielectric passivation layer were formed by a standard photolithography process method and test line lengths were 100, 400, 800, 1200, and 1600 $\mu\textrm{m}$. The current density of $1.19\times10^7\textrm{A/cm}^2$ was stressed in Al-1%Si thin film interconnections under DC condition. The current density of $1.19\times10^7\textrm{A/cm}^2$ was also applied under PDC condition at the frequency of 1 Hz with the duty factor of 0.5. The electromigration resistance of PSG/SiO2 dielectric passivation test line was stronger than $SiO_2$ dielectric passivation test line. The lifetime under PDC was 2-4 times longer than DC condition. As the thin film interconnection line increased, the lifetime decreased and saturated over the critical length. Failure patterns by an electromigration were dominated by void-induced electrical open and hillock-induced electrical short.

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Bond Strength Properties of Latex Modified Concrete (라텍스 개질 콘크리트의 부착강도 특성)

  • 윤경구;이주형;최상릉;김기헌
    • Journal of the Korea Concrete Institute
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    • v.13 no.5
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    • pp.507-515
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    • 2001
  • Significant improvements in bond strength between new and existing concrete can be achieved through the modification of the new concrete by latex. This study focuses on the investigation of bond strength of latex modified concrete. Pull-out bond test and uniaxial direct tensile bond test are adopted for evaluating the adhesion characteristics of latex modified concrete to conventional concrete substrate. The main experimental variables are test methods, latex-cement ratio, surface preparations and moisture levels. The results are as follows; The increase of latex-cement ratio substantially improves the adhesion between latex modified concrete and substrate. The effects of surface preparation at substrate into the bonding of latex modified concrete are quite different according to the conditions of surfaces. Thus, an adequate surface preparations are essential for good bond strength. Because the moisture level of the substrate may be critical to achieving bond, optimum moisture condition for a conventional concrete has evaluated in this study. The saturated condition of surface is the most appropriate moisture level among the considered, followed by dry condition and wet condition.

A Study on the Performance Assessment of Nuclear Fuel Debris Filtration Using the Weighted Mean (가중평균을 이용한 핵연료 이물질 여과성능 평가에 관한 연구)

  • Park, Joon Kyoo;Lee, Seong Ki;Kim, Jae Hoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.2
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    • pp.149-156
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    • 2017
  • Nuclear fuel requires high reliability and safety and therefore contains debris filtering devices to prevent failure-inducing debris from entering it. The debris filtering performance of nuclear fuel is one of the most important factors for fuel integrity. Therefore, the performance must be evaluated and the measurement must be reasonable. In this study, a calculation method of the comprehensive filtering efficiency using the weighted mean was proposed to establish a standard filtering efficiency index. To confirm the suitability of the proposed method, representative debris specimens were selected and the filtering efficiency with the weighted mean was compared with the efficiency of the arithmetic mean. The weighting factor of the weighted mean was introduced to produce a fair evaluation. In addition, the analysis of the debris filtering mechanism was performed according to the size of debris specimens, and the main dimensions of the filtering feature for commercial nuclear fuel.

Evaluation of Fracture Toughness Using Small Punch Test for Aluminum 6061-T6 Type-3 Cylinder Liner (소형펀치시험법을 이용한 알루미늄 6061-T6 Type-3 용기 라이너의 파괴인성 평가)

  • Ma, Young-Wha;Lee, Seong-Hoon;Yoon, Kee-Bong
    • Journal of the Korean Institute of Gas
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    • v.15 no.4
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    • pp.21-26
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    • 2011
  • Type-3 cylinder liner has a limitation of machining the standard specimen for fracture toughness test because it has approximately 5 mm in thickness as well as a curvature. Hence, it needs to be employed a miniature specimen test technique to evaluate fracture toughness of the cylinder liner. In this study, small punch (SP) test method was employed to evaluate fracture toughness of the cylinder liner. Load-displacement curve result measured from the SP test showed that the liner material was failed during membrane stretching in the general SP load-displacement curve. Additionally, it was shown that liner material was isotropic although the amount of plastic deformation was different depending on the direction due to manufacturing process characteristics. Fracture toughness, $J_{Ic}$, was evaluated using the SP test data. The value of fracture toughness obtained was $13.0kJ/m^2$. This value was similar to that of the same kind of materials. Therefore, the fracture toughness evaluated using the SP test data was reasonable.

Study on Soft Conversion from ASD to RBD Code in Larch (국산 낙엽송 부재에 대한 ASD에서 RBD로의 코드 전환에 관한 연구)

  • Park, Chun-Young;Kim, Ho-Ki;Lee, Jun-Jae
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.5
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    • pp.45-50
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    • 2004
  • Currently, structural design of wood structure has been based on ASD (Allowable Structural Design) in Korea. However, the results from this method was known as greater than real value because variations of materials and various conditions were not considered sufficiently. So the study about the design method with probabilistic approach is being performed to overcome this problem. And the standard design method of RBD (Reliability Based Design) has been established and applied. In this study, to apply this method on the domestic wood, the distribution property of the lumber and Glulam was analyzed from the previous report and the basis of the standardized design method was established as soft conversion method from allowable stress used in ASD into reference resistance used in RBD. And through the additional study about the sample size as a important factor to effect on soft conversion, condition to be required in more accurate conversion was evaluated.

Tightness of specimen sealing box in 20 L test chamber to evaluate building materials emitting pollutants (건축자재에서 방출되는 오염물질 평가 시 사용되는 20 L 시험챔버 시편홀더의 기밀성 개선)

  • Shin, Woo Jin;Lee, Chul Won;Kim, Man Goo
    • Analytical Science and Technology
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    • v.20 no.4
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    • pp.261-267
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    • 2007
  • The 20 L small chamber test method is to evaluate pollutants such as TVOC, formaldehyde emitted from building materials. This method was only designed to evaluate the surface emission of sample exposed in the chamber. In this method, building materials cut with a fixed standard size are fixed in a sample sealing box. The sample sealing box is put into the 20 L test chamber. This chamber is ventilated at a standard air change rate with purified air for 7 days then the sample from the chamber is collected and analyzed to measure the emission rate of TVOC and formaldehyde. In this method, however, if the sealing box does not guarantee airtightness, accurate evaluation for the building materials can not be achieved due to the pollutants emitted from edge of the sample so called, edge effect. This edge effect can be much greater when evaluating panels such as plywood, flooring due to their surface treatment. In this study, flooring was tested to check airtightness of the sample sealing box with analytic results between 1L and 20 L test chamber. Furniture materials like LPM coated one side surface treatment and MDF coated both sides surface treatment with LPM were tested to identify whether the improvement of the sample sealing box airtightness is possible with the comparison between existing and improved test method that low VOC emission tape was used to seal the sample edge. After 7 days, MDF TVOC emission rate was different according to the existence and nonexistence of tape. The emission rate of the existing test method was $0.009mg/m^2h$ and that of improved test method was $0.003mg/m^2h$. Relative standard deviation for the existing test method was $0.004mg/m^2h$ and relative standard deviation for the improved test method was $0.002mg/m^2h$ when the same sample was analyzed three times. The improved test method in this study using low VOC emission tape was effective and able to reduce the heterogeneous effect of the edge from the sample sealing box.

The Study of Fast X-ray Fluorescence Analysis Using a SSQ Program (SSQ 프로그램을 이용한 빠른 X-선형광분석법 고찰)

  • Park, Yong Joon
    • Analytical Science and Technology
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    • v.11 no.2
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    • pp.112-119
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    • 1998
  • A Siemens SemiQuant (SSQ) 3000 program, a precalibrated 'standardless' analytical program handling up to 90 elements, was evaluated for the fast analysis of various types of reference materials using a wavelength dispersive X-ray spectrometer. Various types of standard reference materials such as metal discs, metal chips, and geological materials in powder form were analysed and it took 23 minutes of measuring time for 75 elements. Measurements of geological reference materials using different sampling methods were carried out and their data were interactively evaluated. The analysis of materials of a known matrix concentration such as stainless steels provided higher precision value compared to totally unknown samples. The analyses of materials prepared as pressed pellets or fused glass beads provided higher precision values compared to the measurement of loose powders with a foil on the sample surface and helium operation, though their sampling procedures were more complicate and took more time. Since very light elements such as boron, carbon, and oxygen have a strong influence on the matrix effects and also on the calculation of effective matrix corrections, the rhodium Compton check was applied to verify the reliability of the defined light element concentrations of light matrix materials and the defined major sample compounds. Failure of defining correct matrix resulted in an unoptimized matrix correction and therefore in the wrong calculation of the element concentration.

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Study on the Prediction of Surface Color Change of Cultural Properties Materials by Fog Occurrence (안개 발생에 따른 문화재 표면의 색 변화 예측 연구)

  • Han, Ye Bin;Park, Sang Hyeon;Yu, Ji A;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.32 no.4
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    • pp.491-500
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    • 2016
  • Fog is atmospheric in which tiny drops of water vapor are suspended in the air near the ground. Its form, occurrence, etc., change according to the temperature, relative humidity, wind and geographical features of the space around it. In particular, fog tends to occur near a source of water because of temperature and relative humidity difference. These days, climate change is increasingly affecting the occurrence of fog. Therefore the purpose of this study was to investigate how fog affects materials that are part of our cultural properties through outdoor exposure tests and artificial degradation. The degradation evaluation of materials as a function of fog occurrence frequency, showed that the color of metals changed noticeably, whereas dyed silk and Dancheong showed degradation on the surface and color differences but no particular tendencies. Therefore, damage prediction by color differences as a function of fog occurrence frequency was based on metal samples, which showed constant color differences. Through a comparison of the predictive value and color difference by outdoor exposure, the accuracy and applicability of the damage prediction formula was confirmed. If a more complex damage prediction formula is created, it is expected that prediction of the degree of material damage in the field would be possible.