• Proceedings of the Korea Crystallographic Association Conference
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• 2002.11a
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• pp.35-35
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• 2002

나노미터 표준을 확립하기 위하여 일체식 엑스선 간섭계에 광간섭계를 결합시킨 복합간섭계를 구성하였다. 복합간섭계는 광간섭계의 Zero crossing 지점부터 표준시편이 올려진 미소이동대의 이동거리를 변화된 위상값으로 읽고 그 변화량을 고분해능 변위 측정기인 엑스선 간섭계로 읽어들이는 구조로 구성된다. 본 연구에서는 미소이동대의 위치 변화와 관련된 광간섭계의 위상 안정도, 엑스선 간섭계 및 미소이동대의 위치 안정도 등이 나노미터 영역의 길이 측정에 매우 중요한 요인이 되므로, 미소이동대의 위치 변화시 정지상태에서의 위상 잠김 (phase locking) 안정도를 측정하였다. 마이켈슨 레이저간섭계의 한쪽 팔을 고정시키고 다른 한 팔은 미소이동대 위에 반사거울을 설치하여 미소이동대의 움직임을 측정하였다. 보다 안정된 위상잠김 상태를 확보하기 위하여 PID feedback loop controller를 사용하였다. 측정 결과 위상 변동폭이 0.022 degree 이하의 높은 위상잠김 안정도를 확보하였으며, 이를 길이단위로 환산하면 정지상태에서 약 0.02 nm 이하의 위치 안정도를 나타낸다.

• Journal of the Korean Chemical Society
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• v.28 no.5
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• pp.293-301
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• 1984

-ray fluorescence analysis of $Ta_2O_5$, $Nb_2O_5$ and $ZrO_2$ in tin-slag samples using the simple dilution method was studied. The method is to correct mathematically the calibration curve to the linear line by the dilution. One synthesized standard having similar composition to the sample and tin slag samples were diluted with anhydrous $Li_2B_4O_7$ at the level of 1%, 2% and 3% of the sample content respectively. The diluted samples were fused at $1150^{\circ}C$ for 30 minutes and these glass beads were finely ground and pelletized. Measuring the X-ray intensities with these pellets, analytical results were calculated by the equation derived from J. Scherman's equation for the characteristic X-ray intensity of an element. Analytical results agreed with the reference values obtained by the standard calibration method within allowable error range and were reproducible.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1416-1419
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• 2005

Design and manufacturing of plastic injection mold with cavity pressure/temperature sensors were performed in the present study for tensile test specimen. Standards of mold-base and tensile test specimen were used to design an injection molding system. Cavity pressure and temperature sensors were placed on the side of fixed platen of injection mold machine to prevent them from external impact damage. Injection molding experiments with variations of injection speed and melt temperature were performed and polycarbonate tensile specimens were prepared for the tensile test. It was shown that injection molding processing parameters can have effect on the mechanical properties of the plastic injection molded part.

• Journal of the Korean Society for Precision Engineering
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• v.24 no.11
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• pp.84-90
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• 2007

In this study, design and manufacturing of plastic injection mold with cavity pressure/temperature sensors were performed fur tensile test specimen. International standard system for plastic tensile specimen was applied to design an injection molding system. Cavity pressure and temperature sensors were placed on the side of fixed platen of the injection mold to prevent them from external impact damage. Injection molding experiments with variations of injection speed and melt temperature were performed and then tensile test of the manufactured polycarbonate specimens was also performed. It was shown that injection molding processing parameters can have effect on the mechanical properties of the plastic injection molded part.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.05a
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• pp.579-580
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• 2006

In this study, an injection mold of tensile test specimen was manufactured by international standard. Pressure and temperature in the cavity of the injection mold was measured by sensors. Simulation of injection molding process was performed with the same condition of experiment and linear structural tensile analysis was also performed with the initial condition of the residual stress induced by injection molding analysis. Normalized elastic coefficient of tensile test was compared with that of structural analysis. It was shown that the residual stress induced by injection molding has an effect on both the experiment of tensile test and linear structural analysis.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2016.11a
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• pp.103.2-103.2
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• 2016

금속질화물 박막은 대표적인 고경도, 고내열성 박막이다. 박막의 두께는 기계적물성과 밀접한 상관관계가 있으며, 두께의 관리와 제어는 매우 중요하다. 3조 2배열의 증발원을 이용하여 Cathodic vacuum arc deposition(CVAD)법으로써 금속질화물 박막을 제조하였으며, 평균 두께 $4.38{\mu}m$, 표준편차 ${\pm}11.5%$ 박막들을 제조할 수 있었다. 증발원과 증발원 사이의 중첩이 되는 지점에 장착된 시편보다 각각의 증발원에서 평행한 위치에 장착된 시편에 코팅된 박막이 두꺼웠다.

• Journal of the Korean Vacuum Society
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• v.11 no.4
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• pp.218-224
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• 2002

A domestic round robin test(RRT) for the quantitative analysis of minor impurities was performed by a standard procedure and standard reference material. The certified reference material(CRM)s for B-doped Si thin film and analysis specimens and the analysis specimens were prepared by an ion beam sputter deposition method. These samples were certified by inductively coupled plasma mass spectrometry(ICP-MS) with isotope dilution method which il one of the most quantitative methods in chemical analysis. By using an international standard procedure(ISO/DIS-l4237) for the quantitative analysis of B in Si by SIMS, a domestic RRT was performed for these specimens. Although only a few laboratories participated in this RRT, the average B concentration well agreed with the certified value within 2% error.

• Analytical Science and Technology
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• v.17 no.4
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• pp.355-362
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• 2004

Fission products and Inter reaction layer of $U_3Si-Al$ dispersion fuel, irradiated in HANARO research reactor with 121 kW/m of maximum liner power and 63 at% of average burn-up, was characterization by EPMA (Electron Probe Micro Analyzer). The fuel punching system developed by Irradiated Materials Examination Facility (IMEF) has used to make these samples for the EPMA. With this system a very small and thin specimen which is 1.57 mm in diameter and 2 mm in thickness respectively has been fabricated to protect the EPMA operator from high radioactive fuel and to mini-mize the equivalent dose rate less than 150 mSv/h. EPMA was performed to observe layers of sectional, Inter-reaction and oxide with specimens of cutting and polished. Stoichiometry in the Inter-reaction layer with $16{\mu}m$ of thickness was $U_{2.84}$ Si $Al_{14}$ with calibration of $UO_2$ and $U_{3.24}$ Si $Al_{14.1}$ with calibration of standard specimen. metallic precipitates in this layer were not observed using fission products examination.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.2
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• pp.187-192
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• 2013

Fatigue crack was detected from a temperature change around surface crack using the thermographic technique. Thermal gradient across the crack decreased very much due to thermal resistance of contact surface in the crack. Heat diffusion flow passing through the discontinuity was visualized in temperature by infrared camera to find and locate the crack. A fatigue crack specimen(SM-45C), which was prepared according to KS specification and notched in its center to initiate fatigue crack from the notch tip, was heated by halogen lamp at the end of one side to generate a heat diffusion flow in lateral direction. A abrupt jump in temperature across the fatigue crack was observed in thermographic image, by which the crack could be located and sized from temperature distribution.

• Composites Research
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• v.28 no.5
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• pp.285-290
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• 2015

Multiscale multiphysics in structural batteries make mechanical property testing difficult. In this research, the effect of electrolyte-coating on the mechanical performance of carbon fabric was studied using a suitable mechanical test method for structural batteries. For this experiment, two types of specimens were determined their dimension according to ASTM. One type of specimen was smaller than the standard dimension. The specimens were coated by spreading the electrolyte material on carbon fabric, hardened using epoxy, and tested for tensile properties using universal testing machine. As a result, it was found that the mechanical properties of carbon fabric were not influenced by electrolyte coating. In addition, the small-scale specimen used in this experiment was determined to be sufficiently reliable.