• Proceedings of the Korea Institute of Fire Science and Engineering Conference
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• 2009.04a
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• pp.129-138
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• 2009

화재발생시 가장 주요한 사망원인인 유독가스의 제어와, 소방관의 소화활동을 돕기 위한 제연설비는 각 구성품이 유기적으로 동작하는 시스템을 이루기 때문에 전체의 조화도 중요하지만, 기본적으로 각 설비요소가 제 기능을 발휘할 때 전체 시스템의 제연성능을 확보할 수 있게 된다. 그러나 현재 법으로 규정된 국내기준은 주요 구성품별 성능을 제대로 평가할 수 있는 방법 및 기준이 없어 본 연구를 통하여 배연창의 성능평가기술을 개발하고 항목별 성능시험을 실시하여 평가방법의 적합성을 검토하고 국가표준을 만들기 위한 기초 자료로 제공하고자 한다.

• Korean Journal of Food Science and Technology
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• v.43 no.5
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• pp.532-536
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• 2011

The internal standard method using ion chromatography combined with tandem mass spectrometry (IC-MS/MS) for quantifying perchlorate in different types of food was established. Because the presence of ions and other biomolecules in matrices usually interrupts accurate determination of perchlorate, it is necessary to develop efficient, reproducible method to determine perchlorate concentrations in food. In this study, the internal standard method was compared with the external standard method to determine perchlorate concentrations in standard samples. The obtained method detection limit (MDL) for perchlorate was 0.005 ${\mu}g/L$ for bottled water, 0.12 ${\mu}g/L$ for milk, 0.27 ${\mu}g/kg$ for rice, 0.16 ${\mu}g/kg$ for vegetables, and 0.07 ${\mu}g/kg$ for seaweed, respectively. The limit of quantitation (LOQ) was calculated by multiplying the MDL by 7. The recoveries of perchlorate from food samples spiked with perchlorate ranged from 98 to 105% and their percent relative standard deviation (%RSD) levels were <20%. This method was successfully applied for the quantitative determination of perchlorate in various kinds of food.

• The Korean Journal of Pesticide Science
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• v.10 no.3
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• pp.189-195
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• 2006

The purpose of the current study was to develop a standard method to assess the ecological effect of pesticides using the representative Korean freshwater cladocerans. The indigenous cladocerans, Daphnia obtusa, Daphnia sp., Moina macrocopa, Simocephalus vetulus and Daphnia magna formally endorsed by the major international organizations were tested to select optimal culture media in laboratory condition. All of the Korean water flea tested showed good growth and fecundity in the moderately hard water ($CaCO_3$ ranged 80 to 100 mg $L^{-1}$) and soft water ($CaCO_3$ ranged 40 to 48 mg $L^{-1}$). However, considering that the total hardness of fresh water collected from 5 rivers ranged from 60.2 to 127.2 mg $L^{-1}$ ($CaCO_3$) and Ca deficiency could be a major determinant of species success and community structure among crustacean zooplankton, the present study suggests that the optimal water hardness for growing Daphnia sp., Daphnia obtusa, Moina macrocopa and Simocephalus vetulus is $80{\sim}100$ mg $L^{-1}$ of $CaCO_3$.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.1
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• pp.310-315
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• 2017

Although studies evaluating the effects of the blasting vibration on the adjacent structures from various angles have continued, cases of securing the safety of the adjacent buildings and researching the proper blasting method for the field condition by analyzing the vibration waveform of the measuring field while performing the open pit blasting are poor. Therefore, it is necessary to present a remedy for blasting pattern selection through test blasting that is appropriate for field conditions, and is economical and efficient. In this study, open pit blasting work was conducted based on the separation distance applied according to the standard blasting method by test blasting and the vibration regulation standard in the road expansion construction site to measure the blasting vibration value, and the vibration prediction equation by blasting methods was examined using a regression analysis computer program to calculate K, N, and R of the confidence level 95%. By setting the blasting allowed vibration standard of the test blasting target area to 0.3cm/sec, and the charring weight and blasting method by the separation distances according to the blasting vibration estimation equation of the open pit blasting guideline and the blasting vibration estimation equation of the test blasting were compared/analyzed, it was possible to identify the factors that increased the working expenses. In addition, the measurement and analysis of the adjacent structures during open pit blasting and the blasting vibration were performed after selecting the most adjacent structure to the open pit blasting spot to analyze the problems on the test blasting procedure and analysis method in the open pit blasting design/construction guidelines, which appeared in the process of completing open pit blasting construction, and a remedy is presented.

• Journal of the Korea Institute of Information and Communication Engineering
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• v.23 no.1
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• pp.7-12
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• 2019

Variety of companies which carry out R&D projects supported by government are proposing quantitative evaluation index business plans. However, Many companies have difficulties in aspects of selecting quantitative evaluation index and in some cases they have troubles to get results from selecting unsuitable evaluation index. First of all, both methods of gathering the data to be analyzed and the products which are tested by the accredited testing institutes classifying by industrial sectors are classified as the quantitative evaluation index selected by the company according to the eight quality characteristics of ISO/IEC 25023 Standard. Secondly, based on the results of the quantitative evaluation indexes classified into eight quality characteristics of the ISO/IEC 25023 standard, the tendency of the quality characteristics of the quantitative evaluation indexes selected mainly by the companies will be understandable. It is hopefully expected that this research will be helpful to select a quantitative evaluation index to evaluate the quality of software products.

• Journal of the Society of Cosmetic Scientists of Korea
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• v.38 no.1
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• pp.33-41
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• 2012

An effective, environmentally friendly analytic methods using gas chromatography with mass spectrometric detector (GC-MSD) have been developed for the quantitative analysis of trace phthalate levels in cosmetics such as nail lacquer and hair spray. Since such cosmetics are largely comprised of organic solvents, conventional clean-up methods that have been widely used for phthalate analyses are in adequate. In addition, analysis of trace phthalate levels is notorious for its sensitivity to contamination, which causes high analytical values. A direct sample dilution method using an organic solvent was adopted to the sample preparation process to determine the exact amounts of phthalates and simultaneously avoid the high risk of secondary contamination. The method has many advantages including high accuracy, sensitivity, and simplicity in sample preparation. Dibutyl phthalate (DBP) and di (2-ethylhexyl) phthalate (DEHP) were selected for analysis because they have been frequently detected in cosmetics and consistently reported as endocrine disruptors in humans and animals. Internal standard method using two deuterium substitutes (DBP-$d_4$, DEHP-$d_4$) as the internal standard was also used. The results of 'Method validation' showed the capabilities of this method for the routine analysis of phthalates at the ppm level. The recovery ranges were between 95 % and 106.1 %, and relative standards deviations (RSD) were less than 3.9 % in fortified nail lacquer and hair spray samples at the concentration of $25{\mu}g/g$.

• Journal of Korean Society of Transportation
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• v.20 no.7
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• pp.205-211
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• 2002

본고에서는 최근 논의되고 있는 ATP 도입의 필요성 및 시스템 선정의 적절성을 검토하는데 있어서 철도신호 분야 뿐만이 아닌 우리의 환경변화 여건 등을 종합적으로 고려하여 철도의 장기 발전전략에 부합하는 APT 도입 방안을 제시하였다. ATP 도입시 고려해야 할 주요 환경변화로는 고속철도개통, 기존철도시스템과의 조화와 관련한 기술발전 측면, 틸팅차량 등 기존선 속도향상, 전철화, 복선화 등 철도영업거리 확장 및 남북철도연결 등을 고려해야 할 것이다. 즉, 바람직한 차상신호장치 도입을 위해서는 차량과의 적합성에 있어서는 기존차량, 특히 속도계장치와의 호환성, 시설분야에 있어서는 설치작업 및 향후 유지보수의 용이성과 국산화 가능성, 향후 남북철도 연결과 고속 철도의 기존선 연계운행 등을 종합적으로 고려하고 장기적인 철도발전에 도움이 되는 방향으로 추진되어야 할 것이다. 결론적으로, 우리철도의 기반시설과 차량 등의 현황과 향후 변동요인을 반영하여 가장 바람직한 ATP 표준기준을 용역 등을 통해 설정하고, 업체선정, 적어도 1년 정도의 시험기간을 거쳐 실용화 단계로 접근해야 할 것이다.

• The Transactions of the Korea Information Processing Society
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• v.5 no.1
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• pp.128-136
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• 1998

TTCN(Tree and Tabular Combined Notation), as an international standard, provides a concept and notation to describe a protocol test specification. In this paper, we explain some considerations on each components of Abstract Test Suite and propose naming conventions for Constraints and Test Cases based on the experience of describing Test Suite for real protocol. We also analyze some problems on real application of Test Suite and propose an approach to avoiding such problems in the stage of Test Suite specification. In this paper, we use the SSCOP(Service Specific Connection Oriented Protocol) protocol, that is a sub-layer of ATM Forum UNI 3.1 protocol stack, as an example to proposals on naming conventions on Constraints and Test Cases.

• Journal of Food Hygiene and Safety
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• v.34 no.1
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• pp.52-57
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• 2019

Method development and validation of decursin for the standardization of Angelica gigas Nakai as a functional ingredient and health food were accomplished. The quantitative determination method of decursin as a marker compound of aerial parts of Angelica gigas Nakai extract (AAGE) was optimized by HPLC analysis using a C18 column ($3{\times}150mm$, $3{\mu}m$) with 0.1% TFA in water and acetonitrile as the mobile phase at a flow rate of 0.5 mL/min and detection wavelength of 330 nm. The HPLC/PDA method was applied successfully to quantification of the marker compound in AAGE after validation of the method with linearity, accuracy, and precision. The method showed high linearity in the calibration curve at a coefficient of correlation ($R^2$) of 0.9994 and the limit of detection and limit of quantitation were $0.011{\mu}g/mL$ and $0.033{\mu}g/mL$, respectively. Relative standard deviation (RSD) values of data from intra- and inter-day precision were less than 1.10% and 1.13%, respectively. Recovery of decursin at 0.5, 1, 5 and $10{\mu}g/mL$ were 92.38 ~ 104.11%. These results suggest that the developed HPLC method is very useful for the determination of marker compound in AAGE to develop a health functional material.

• Analytical Science and Technology
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• v.27 no.6
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• pp.339-346
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• 2014

The author assessed the availability of urine reference material for proficiency test provided for laboratories in occupational health. N-methylacetamide is the biomarker of exposure to N,N-dimethyl acetamide, which was used as the substitute for hepatotoxic N,N-dimethylformamide (DMF). N-methylacetamide (NMAC) urine samples of 3 different levels covering the 0.2~2 times of the exposure limit were tested. Stability test up to 180 days (0, 7, 30, 60, 180 days) at 4 different temperatures (-60, -20, 5, $25^{\circ}C$) and homogeneity test were performed for these samples. New analytical condition by GC/MSD using SIM mode (m/z 58, 59) and DB-624 column was investigated for better selectivity, sensitivity and resolution. Urinary NMAC samples showed good homogeneity for 3 levels. These samples also showed good stability up to 180 days. The data of stability and homogeneity of urinary DMAC confirmed the basis of including this item into Korean proficiency test for occupational health laboratories since 2008.