• Title/Summary/Keyword: 질량 보존

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Analysis of characteristics of natural resins using organic residue analysis organic materials attached on wooden coffins from Singok-dong Site, Uijeongbu (유기잔존물 분석을 활용한 천연 수지 특성 분석 - 의정부 신곡동 유적 출토 목관 부착 유기물을 중심으로 -)

  • YUN, Eunyoung
    • Korean Journal of Heritage: History & Science
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    • v.54 no.4
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    • pp.78-89
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    • 2021
  • Organic residues analysis is an analysis method that reveals the types of organic material samples by using the characteristic that main components constituting substances are different depending on the species of animals and plants. In this study, scientific analysis of the organic residues attached to wood coffins in the Joseon Dynasty Hoemyo excavated from the site of Singok-dong, Uijeongbu was used to identify the types of remnants and to use them as information to restore the uses of organic materials and the way they lived in the past. As a result of FT-IR analysis of the residue attached to the inside of the wood, it was estimated to be a natural plant resin material. In addition, as a result of analysis by GC-MS to confirm the characteristic factors of natural resins, diterpenoids (abietane) and pimaran (pimarane), such as dehydroabietic acid and pimaric acid (diterpenoid) compounds, and saturated and unsaturated fatty acid components were detected together. Diterpenoid compounds are components mainly found in Pinaceae resins. It is confirmed in the literature that rosin, a representative material of Pinaceae resin, was used as an adhesive material. Considering the situation where an organic material remained at the joint of the wood, the organic material attached to the wood is judged to be an adhesive material made of Pinaceae resin. In addition, the fatty acid component detected together is a component derived from plant oil, and it is presumed to be made by mixing rosin and oil as recorded in previous studies. This study confirms that organic residues remain in the burial environment without losing their characteristics. It is expected that scientific analysis of organic residues will be conducted in the future to accumulate information necessary for the interpretation of past living culture.

Material Characteristics of White Wares from Yeongdong Province, Gangwon-do: Gangneung and Donghae Kiln Sites (강원 영동지역 백자의 재료과학적 특성 연구: 강릉 남양리 백자가마터와 동해 발한동2(사문동) 가마터를 중심으로)

  • Lee, Byeong Hoon;So, Myoung-Gi
    • Journal of Conservation Science
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    • v.31 no.3
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    • pp.181-192
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    • 2015
  • This study aims to examine production technique of twelve white wares from the Gangneung Namyang-ri and Donghae Balhan-dong2(Samun-dong) kiln sites, Kangwon Province and characteristics of the used materials, and to find a correlation among materials of the excavated white wares. X-ray fluorescence sequential spectroscopy(XRF), X-ray diffraction(XRD), Dilatometer and Inductively coupled plasma mass spectrometry(ICP-MS), Inductively coupled plasma automic emission spectrometer(ICP-AES) were applied to determine the chemical composition, crystalline phase of samples, firing temperatures, trace elements and rare earth elements. When analyzing body crystalline phases of the white wares using the XRD method, quartz and mullite were extracted from all the samples. Though firing temperature of each sample was different, they were mostly fired at a temperature below $1200^{\circ}C$. Analyzing the excavated white wares using the Seger formula, compositional properties of white wares in Gangneung Namyang-ri kiln showed diffrently from the Donghae Balhan-dong2(Samun-dong) kiln. The body of white wares from Gangneung Namyang-ri kiln have higher raito of $RO_2$ and $RO+R_2O$ than of white wares from Donghae Balhan-dong2(Samun-dong) kiln site. The white wares from Gangneung Namyang-ri kiln and Donghae Balhan-dong2(Samun-dong) kiln were made of host rocks of the different geological origin, according to the result of rare earth elements analysis.

The Study of Sediment Volume Concentration in Liquefied-Layer of Debris Flow (토석류 유동층에서 토사체적 농도 특성에 관한 연구)

  • Kim, Sungduk
    • Journal of the Korean GEO-environmental Society
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    • v.15 no.12
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    • pp.109-115
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    • 2014
  • The purpose of this study is to estimate the sediment volume concentration of the liquified-solid mixture which is included fine sediment fractions, according to the variance of the channel slope and the water supply. The numerical model was performed by using the Finite Differential Element Method (FDM) based on the equation for the mass conservation, momentum conservation and the equation of coarse sediment an fine sediment. In comparison of varying the channel slope, the deeper the channel slope, the inflection point of the sediment concentration was occurred rapidly. In comparison of variance of the water supply, as the water supply increases fluctuation with high sediment concentration. In this situation, debris flow changes to the turbulent flow and the sediment becomes to be floated. In comparison varying the length paved saturated sediment, the longer the length, the high concentration of sediment occurred, for the safety of the slope it is needed to check the possibility of the erosion in the slope by debris flow. The results of this study will provide useful information in predicting of the disaster by the liquified-solid mixture and in prevention of the debris flow with various the slope in the mountain side.

One-dimensional Hydraulic Modeling of Open Channel Flow Using the Riemann Approximate Solver I : Model Development (Riemann 해법을 이용한 1차원 개수로 수리해석Ⅰ: 모형 개발)

  • Kim, Ji-Sung;Han, Kun-Yeun
    • Journal of Korea Water Resources Association
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    • v.41 no.8
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    • pp.761-772
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    • 2008
  • The object of this study is to develop the model that solves the numerically difficult problems in hydraulic engineering and to demonstrate the applicability of this model by means of various test examples, such as, verification in the gradually varied unsteady condition, three steady flow problems with the change of bottom slope with exact solution, and frictional bed with analytical solution. The governing equation of this model is the integral form of the Saint-Venant equation satisfying the conservation laws, and finite volume method with the Riemann solver is used. The evaluation of the mass and momentum flux with the HLL Riemann approximate solver is executed. MUSCL-Hancock scheme is used to achieve the second order accuracy in space and time. This study introduce the new and simple technique to discretize the source terms of gravity and hydrostatic pressure force due to longitudinal width variation for the balance of quantity between nonlinear flux and source terms. The results show that the developed model's implementation is accurate, robust and highly stable in various flow conditions with source terms, and this model is reliable for one-dimensional applications in hydraulic engineering.

Organic Analysis of Charred Residues on the Pottery in the Proto-Three Kingdom from Joong-do Site, Chuncheon (춘천 중도 유적에서 출토된 원삼국시대 토기 탄착물에 대한 화학적 분석)

  • Kang, Soyeong;Jee, Sanghyun;Kim, Yun Ji;Chang, Hong Sun
    • Journal of Conservation Science
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    • v.29 no.4
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    • pp.437-444
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    • 2013
  • We studied for the chemical characterizations of the charred residues obtained from the ancient potteries in the Proto-Three Kingdom period from archaeological sites in Joong-do, Chuncheon. Organic components of the charred residues were extracted and analysed using mass spectrometry and infrared spectroscopy. Lipid profiles from these samples were not identified in gas chromatography-mass spectrometry. Bulk stable isotope analyses of charred residues was used to infer an average values of the foods prepared. The average carbon isotope values (${\delta}^{13}C$) of the residues are $-14.7{\pm}2.8$‰ (ranging from -8.7‰ to -18.4‰, n=9), and nitrogen isotope values (${\delta}^{15}N$) are $6.2{\pm}1.1$‰ (ranging from -4.4‰ to -7.6‰, n=9). This is the first approach to analyse charred residues using stable isotopic method in Korea. Charred food residues on the interior surface of archaeological pottery can provide valuable information about pottery use and dietary habits of its population.

A Comparative Study on the Metallurgical Characteristics of the Iron Knife Using Traditional Iron-Making Method (전통 제철법을 적용하여 제작한 철제 칼의 금속학적 특성에 관한 비교 연구)

  • Cho, Sung Mo;Cho, Nam Chul;Han, Jung Uk
    • Journal of Conservation Science
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    • v.34 no.5
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    • pp.433-442
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    • 2018
  • In this study, metal properties were compared by preparingthree iron knives from steel ingots produced via traditional iron-making, and ingot which jointed the steel of modern times. Metal microscope and SEM-EDS analysis revealed fine ferrite and pearlite structures of the hypo-eutectoid steel of Fe-C alloys. All samples also exhibited martensite on the blade of the knife. By Vicker's hardness analysis, the hardness of the sand iron knife (K1) was 533.38 HV, sand iron-nickel steel knife (K3) was 514.8 HV, and sand iron-carbon steel knife (K2) was 477.02 HV. The mass reduction due to wear was 0.058% for K1, 0.059% for K3, and 0.144% for K2. EPMA(Electron probe micro-analyzer) analysis of the surface pattern of the specimens confirmed that the patterns were exposed due to differences in the content of C or the chemical composition. Additional research on heat treatment processes is needed to increase the abrasion resistance of blades. Traditional steel ingots could produce high-quality steel if combined with nickel steel.

A Study on Chemical Composition and Firing Temperature of White Wares from the Guyre-2ri Kiln Sites, Wonju (원주 귀래2리 가마터 출토 백자의 화학조성과 소성온도 연구)

  • Lee, Byeong Hoon;So, Myoung-Gi
    • Journal of Conservation Science
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    • v.30 no.3
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    • pp.249-261
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    • 2014
  • This study aims to examine production technique of white wares from the Guyre-2ri 1st and 2nd kiln sites, Wonju, Gangwon Province and characteristics of the used materials, and to find a correlation among materials of the excavated white wares. X-ray fluorescence sequential spectroscopy(XRF), X-ray diffraction(XRD), Dilatometer and Inductively coupled plasma mass spectrometry(ICP-MS), Inductively coupled plasma automic emission spectrometer(ICP-AES) were applied to determine the chemical composition, crystalline phase of samples, firing temperatures, trace elements and rare earth elements. White wares from the Guyre-2ri kiln sites contained high contents of coloring oxides and fluxes. Though firing temperature of each sample was different, they were mostly fired at a temperature below $1200^{\circ}C$ and some of them experienced a low temperature of $1000^{\circ}C{\pm}20^{\circ}C$ and a high temperature above $1200^{\circ}C$. When analyzing body crystalline phases of the white wares using the XRD method, quartz and mullite were extracted from all the samples, and the proportions were similar to each other. When analyzing the excavated white wares using the Seger formula, also, all the samples showed similar clay sources and production techniques. Moreover, the white wares were made of host rocks of the same geological origin, according to the result of rare earth elements analysis.

The Study for Analysis of Impact Force of Debris Flow According to the Location of Check Dam (사방댐 위치변화에 따른 토석류의 충격력 해석에 관한 연구)

  • Kim, Sung-Duk;Lee, Ho-Jin;Chang, Hyung-Joon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.1
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    • pp.409-418
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    • 2019
  • Debris flows occur in mountainous areas due to heavy rains resulting from climate change and result in disasters in the downstream area. The purpose of this study is to estimate the impact force of a debris flow when a check dam according is installed in various locations in the channel of a highly mountainous area. A Finite Differential Element Method (FDM) model was used to simulate the erosion and deposition based on the equation for the mass conservation and momentum conservation while considering the continuity of the fluid. The peak impact force from the debris flow occurred at 0 to 5 sec and 15 to 20 sec. When the supplied water discharge was increased, greater peak impact force was generated at 16 to 19 sec. This means that when increasing the water supply, the velocity of the debris flow became faster, which results in increased energy of the consolidation between the particles of the water and the sediment made. If a number of check dams were to be set up, it would be necessary to investigate the impact force at each location of the check dam. The results of this study could provide useful information in predicting the impact force of the debris flow and in installing the check dams in appropriate locations.

The Study for Reduction Effect of Riverbed Scour due to Shape of Vanes (베인 형태에 따른 하상세굴 저감 효과에 관한 연구)

  • Hae Min Noh;Ho Jin Lee;Sung Duk Kim
    • Journal of Korean Society of Disaster and Security
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    • v.16 no.2
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    • pp.57-63
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    • 2023
  • Recently, Heavy rains and super typhoons occurred by climate change cause a lot of damage in Korea. In order to reduce such damage, various types of river maintenance projects are being promoted, but it is difficult to maintain the balance of rivers in Korea with distinct flood and dry seasons. In particular, river structures installed as a river maintenance project cause various problems such as scouring of structures and their foundations during floods and river bed changes. In order to reduce such bed scour, various vanes are installed in the bend of the river, and various bed scour reduction effects appear depending on the size, arrangement, and shape of the vanes. The vane regenerates the secondary flow in the opposite direction to the secondary flow generated by the centrifugal force, thereby reducing scour around the outer bed and promoting deposition. The theory of this study uses the governing equation applying the continuity equation that satisfies the law of conservation of mass and the momentum equation that satisfies the conservation of momentum, and measures the overall average flow velocity change rate according to design factors to investigate the effect of vanes under various conditions. Both the average and cross-sectional flow velocities decreased in both the trapezoidal vane and the square vane. In addition, vanes installed perpendicularly or inclined to the direction of river flow generate a secondary flow in the opposite direction to the secondary flow generated by centrifugal force, thereby canceling the secondary flow of centrifugal force, so the effect of the vane appears.

Skin permeability of the biosynthetic galactosylated 2-phenoxyethanol (생합성된 galactosylated 2-phenoxyethanol의 피부 투과도)

  • Su-Hong Kim;Sun-Beom Kwon;Jun-Sub Kim;Gi-Seong Moon;Kyung-hwan Jung;Hyang-Yeol Lee
    • Journal of the Korean Applied Science and Technology
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    • v.41 no.1
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    • pp.1-8
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    • 2024
  • The safety of cosmetic ingredients is considered paramount. In order to enhance safety, a novel preservative, PE-gal, was bio-synthesized by utilizing the Escherichia coli enzyme 𝛽-galactosidase on the conventional preservative 2-phenoxyethanold (PE). The skin absorption of the bio-synthesized product, PE-gal, intended for use in cosmetics, was evaluated for permeability using the Franz Diffusion Cell Assay system, comparing it with the conventinal preservative PE. When using samples of the same mass concentration, the Flux and Kp values of PE increased over time, indicating a gradual increase in permeability. However, PE-gal did not exhibit sufficient permeability to measure. This suggests that the skin permeability of PE is higher than that of the PE-gal saccharide. According to Marzulli et al., when confirming the degree of permeation using Kp values, the permeation rate of PE was measured as "slow" at a concentration of 1mg/mL. Thus, the transdermal permeability of the divedened form of PE-gal was significantly lower compared to PE.