• Journal of Korean Society of Environmental Engineers
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• v.32 no.6
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• pp.581-586
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• 2010

Generally, electrokinetic potential has been considered as an intensive property. In other words, electrokinetic potential is not affected by the amount of particulate matter. Montmorillonite, one of essential inorganic matter, was chosen to measure electrokinetic potential. The result of electrokinetic potential measuring experiment showed that the value observed to decrease as the amount of montmorillonite clay increased. This is due to the fact that total ions that adsorbed per unit mass were decreased as the amount of montmorillonite was increased. As a result, electrokinetic potential is considered as an extensive property. By using these results, total interaction energy of suspension was also checked, and revealed that total interaction energy was decreased as the amount of montmorillonite increased.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 1999.10a
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• pp.103-107
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• 1999

가속기 질량분광분석법(Accelerator Mass Spectrometry; AMS)은 동위원소 분석에 있어 초정밀 질량 분석 기술에 속한다. 시료(Samples)의 원자를 이온화 시켜 가속시키고, 에너지, 운동량 그리고 전하 상태를 분석하여 최종 얻고자 하는 원자핵의 동위원소, 예를 들어 탄소-14$^{14)C$),의 수를 정확하게 측정하는 분광분석 기술이다. 본 논문을 통하여 AMS를 소개하고 대기 환경 연구에 AMS가 어떻게 응용될 수 있는지 살펴 보기로 한다.(중략)

• Proceedings of the Optical Society of Korea Conference
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• 1991.06a
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• pp.199-202
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• 1991

기체 시로의 정밀한 분석이 가능한 공명이온화 질량분석장치(Resonance lonization Mass Spectrometor)를 설계, 제작하고 그 특성을 분석하였다. 두 개의 터보펌프(turbo-molecular pump)로 차등펌핑하여 1*10-7Torr 의 진공도를 얻었으며, Nd:YAG 레이저로 광펌핑되는 색소레이저를 분자빔에 조사하여 공명다광자 이온화현상에 의해 발생되는 이온들을 가속시켜 질량을 측정하였다. 아닐린을 시료로 사용하여 분석한 결과 최대 분해능 200을 얻었다.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.6
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• pp.3442-3447
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• 2014

A simple method to evaluate the hygroscopic characteristics of polymer of microelectronic plastic package is suggested. To evaluate the characteristics, specimens were prepared, and the internally absorbed moisture masses were measured as a function of the absorbing time and calculated numerically. The hygroscopic pressure ratio was calculated by heat transfer analysis supported by commercial FEM code because the hygroscopic diffusion equation has the same form as the heat transfer equation. The moisture masses were then summed by the self developed code. The nonconductive polymers had quite different characteristics for the different lots, even though they were the same products. The absorbed moisture mass variations were calculated for several different characteristics, and the optimal curve of the mass variation close to experimental data was selected, whose solubility and diffusivity were affected by the hygroscopic characteristics of the material. The method can be useful in the industrial fields to quickly characterize the polymer material of the semiconductor package because the fast correspondence is normally required in industry. The weight changes in the aluminum-nonconductive-polymer joint due to moisture absorption were measured. The deformed system was also measured using the Moire Interferometry system and compared with the results of finite element analysis.

• Resources Recycling
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• v.32 no.6
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• pp.25-33
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• 2023

With the growth of the battery industry, a rapid increase in the production and usage of lithium-ion batteries is expected, and in line with this, much interest and effort is being paid to recycle waste batteries, including production scrap. Although much effort has been made to recycle cathode material, much attention has begun to recycle anode material to secure the supply chain of critical minerals and improve recycling rates. The proximate analysis that measures the content of coal can be used to analyze graphite in anode material, but it cannot accurately analyze due to the interaction between the components of the black mass. Therefore, in this study, thermogravimetric analysis of each component of black mass was measured as the temperature increased up to 950℃ in an oxygen atmosphere. As a result, in the case of cathode material, no change in mass was measured other than a mass reduction of about 5% due to oxidation of the binder and conductive material. In the case of anode material, except for a mass reduction of about 2% due to the binder, all mass reduction were due to the graphite(fixed carbon). In addition, metal conductors (Al, Cu) were oxidized and their mass increased as the temperature increased. Thermal analysis results of mixed samples of cathode/anode show similar results to the predictive values that can be calculated through each cathode and anode analysis results.

• Proceedings of the Korea Institute of Fire Science and Engineering Conference
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• 2013.11a
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• pp.49-49
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• 2013

실규모급 화재 실험의 신뢰성 있는 발열량 측정을 위해서 흡입 배관의 직경 1.6 m, 직선길이 26m, 후드 직경 10 m 그리고 흡입용량 $2,000m^3/min$ 이상의 대형 콘 칼로리미터를 구성하여 헵탄의 화재 크기별 연소 실험을 진행하였다. 발열량 측정을 비교 분석하기 위해서 산소 소모 지수법, 질량 소모법, 복사열 그리고 대류열 측정 기법에 따라서 각각의 발열량을 산출하고 크기를 비교하였다. 그 결과 대형 콘 칼로리미터에 의해서 측정한 산소 소모 지수법은 이론 발열량에 해당하는 질량 소모법과 최대 약 2.3 % 정도, 복사열에 의한 발열량 산출법은 12.2 % 정도, 연소면적에 의한 이상적인 발열량과는 최대 30 % 정도, 그리고 대류열만 고려한 경우 약 50 % 정도 차이가 나는 것을 확인하였다.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.92-92
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• 2016

전기방전의 기본적인 특성을 가지고 있는 플라즈마를 이용하여 재료를 가공하는 증착, 식각, 표면처리 공정에 있어서 플라즈마 내의 전자 충돌 반응에 의한 이온, 라디칼의 생성과 재료 표면의 반응을 분석하는 도구로써 분압 측정은 일반적인 화학 조성 분석에 기원한 오랜 역사를 가지고 있다. 1 amu 정도의 분해능을 가지고 있고 크기가 30 cm 정도에 불과한 사중극자 질량 분석기는 적절한 질량 스캔 시간과 넓은 이온 전류 측정 범위를 가지므로 소형 차등 배기 시스템과 조합하면 1 mTorr 영역의 스퍼터링 시스템에서 1 Torr 영역의 PECVD/PEALD 시스템 진단에도 쉽게 적용이 가능하다. Inficon사의 CPM-300과 Pfeiffer사의 Prisma80을 이용한 플라즈마 식각 공정 분석 결과를 보면 동위원소까지 분석이 가능하다. 또한 전자충돌 이온화 에너지를 조절하여 m/q(질량전하비율)가 중첩되는 경우의 해석도 가능하다. 다중 오리피스를 갖는 compact design의 밸브 블록을 이용한 설계에서는 line-of-sight 입사가 불가능하여 이온 전류를 분석할 수 없다는 단점이 있으나 표준 가스를 이용한 정량화 등의 큰 장점들이 있다. 최근 이루어진 연구의 내용으로는 유도 결합 플라즈마 장치에서 전도성 메쉬를 이용한 라디칼 거동 관찰을 위해서 두 대의 CPM-300을 메쉬 전 후에 설치하여 라디칼의 양 변화를 전류 프로브와 같이 사용하여 조사하였다.

• The Bulletin of The Korean Astronomical Society
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• v.28 no.2
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• pp.45-45
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• 2003

• The monthly packaging world
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• s.91
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• pp.148-157
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• 2000

• Analytical Science and Technology
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• v.24 no.1
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• pp.1-9
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• 2011

We described an estimation of measurement uncertainty in quantitative analysis of 11-nor-9-carboxy-${\Delta}^9$-tetrahydrocannabinol (THC-COOH), the metabolite of ${\Delta}^9$-tetrahydrocannabinol, in hair samples by using the bead-assisted liquid-liquid extraction and gas chromatography-tandem mass spectrometric (GC-NCI-MS/MS) detection. Traceability of measurement was established through the use of reference materials, calibrated volumetric tubes, volume measuring devices, and measuring instruments. The analytical results were compared and the different contributions to the uncertainty were evaluated. Inter-day variation was performed by using statistical analysis of several indicative factors. Measurement uncertainty associated with the analyte in real forensic hair samples were estimated using QC data. The major factor of contribution to combined standard uncertainty was inter-day repeatability, while those associated with preparation of analytical standard and also sample of weight were insignificant considering the degree of contribution. Relative uncertainty of relative extended standard uncertainty divided into the measured concentration of the analyte was 17% in a hair sample. The uncertainty of result evaluation will be invaluable to improve quality of the analysis.