• Title/Summary/Keyword: 질량분석

Search Result 2,064, Processing Time 0.031 seconds

Additive Noise Reduction Algorithm for Mass Spectrum Analyzer (질량 스펙트럼 분석기를 위한 부가잡음제거 알고리즘)

  • Choi, Hun;Lee, Imgeun
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.22 no.1
    • /
    • pp.33-39
    • /
    • 2018
  • An additive noise reduction algorithm for a mass spectrum analyzer is proposed. From the measured ion signal, we first used an estimated threshold from the mode of the measured signal to eliminate background noises with the white Gaussian characteristics. Also, a signal block corresponding to each mass index is constructed to perform a second order curve fitting and a linear approximation to signal block. In this process, the effective signal block composed of only the ion signal can be reconstructed by removing the impulsive noises and the sample signals which are insufficient to be viewed as normal ion signals. By performing curve fitting on the effective signal block, the noise-free mass spectrum can be obtained. To evaluate the performance of the proposed method, a simulation was performed using the signals acquired from the development equipment. Simulation results show the validity of the threshold setting from the mode and the superiority of the proposed curve fitting and linear approximation based noise canceling algorithm.

An Analysis of Elementary Mathematics and Science Textbooks for Grades 3 and 4: Focused on Capacity, Volume, Weight, and Mass (초등학교 3~4학년군 수학·과학 교과서 비교 분석: 들이, 부피, 무게, 질량을 중심으로)

  • Pang, JeongSuk;Kwon, MiSun
    • School Mathematics
    • /
    • v.19 no.3
    • /
    • pp.617-638
    • /
    • 2017
  • In order to make a connection in teaching similar concepts between mathematics and science in teaching similar concepts, this paper analyzed the contents related to capacity, volume, weight, and mass in the mathematics and science textbooks aligned with the national elementary curriculum. We first explored when to present such topics in both textbooks, and then analyzed in what ways the topics were addressed in terms of quantitative comparison, vocabulary, units of measurement, measurement, tools for measurement, estimation, and connections to real life. The results of this study showed that there were some aspects emphasized in common both in mathematics and science textbooks. The analysis of this study also demonstrated subtle but considerable differences according to the characteristics of two subject matters. Based on these results, this paper provides implications for elementary school teachers to consider in teaching capacity, volume, weight, and mass through mathematics and science lessons.

Nano-Bio Surface Analysis

  • Lee, Tae-Geol
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2013.02a
    • /
    • pp.88-88
    • /
    • 2013
  • 최근 각광을 받고있는 나노바이오 질량이미징 분석법의 측정원리를 이해하고, 세포/생체조직/생체샘플/바이오칩의 측정결과를 바탕으로 핵심측정 능력을 파악하여 각자의 연구에 적용 가능성을 탐색할 수 있는 역량을 배양하고자 한다.

  • PDF

Determination of Plutonium in HANARO Irradiated Fuel by IDMS (동위원소희석 질량분석법에 의한 조사 후 하나로 핵연료 중 Pu 정량)

  • Jeon, Young Shin;Son, Sae Chul;Kim, Jung Suk
    • Analytical Science and Technology
    • /
    • v.16 no.3
    • /
    • pp.191-197
    • /
    • 2003
  • Two methods, IDMS (Isotope Dilution Mass Spectrometry) and controlled potential coulometry are compared by the determination of Pu for the NBL, CRM No.122, $PuO_2$. The recovery of Pu was found to be $1.002176{\pm}0.000452$ within the relative standard deviation of 0.045% (95% conf. level) although a small size of sample ($0.9{\mu}g$-Pu) was used in IDMS. The recovery using controlled potential coulometry were obtained in the range of 0.9923~0.9960. The analytical results of IDMS and controlled potential coulometry were good agreement within 0.6~1%. Base on these experiment results, The plutonium in HANARO irradiated fuel rod that separated portion of top, middle, and bottom were determined. The measured values of Pu are 1.155 mg, 2.483 mg and 1.920 mg in one gram of sample(fuel+clad), respectively.

An experimental study on the effect of mass injection location and flow rate for tip vortex cavitation of 3D hydrofoil (수중익 날개 끝 보텍스 캐비테이션 제어를 위한 질량분사 위치 및 분사량 영향에 대한 실험적 연구)

  • Eunsue Hwang;So-Won Jeong;Hongseok Jeong;Hanshin Seol
    • The Journal of the Acoustical Society of Korea
    • /
    • v.42 no.3
    • /
    • pp.233-242
    • /
    • 2023
  • In this paper, the effect of mass injection on the control of tip vortex cavitation was studied experimentally. A mass injection system for a 3D hydrofoil was designed to control the location of injection as well as the injection rate. A series of cavitation tests were carried out in a cavitation tunnel for different injection locations and rates. The cavitation behaviour was observed using a high-speed camera and the corresponding noise was measured using a hydrophone installed in the observation window. The results showed that the tip vortex cavitation was suppressed under certain conditions and the noise was reduced in some frequency bands. It was also found that there is a location where the effect of mass injection could be maximized and hence the noise reduction.

Proteome Data Analysis of Hairy Root of Panax ginseng : Use of Expressed Sequence Tag Data of Ginseng for the Protein Identification (인삼 모상근 프로테옴 데이터 분석 : 인삼 EST database와의 통합 분석에 의한 단백질 동정)

  • Kwon, Kyung-Hoon;Kim, Seung-Il;Kim, Kyung-Wook;Kim, Eun-A;Cho, Kun;Kim, Jin-Young;Kim, Young-Hwan;Yang, Deok-Chun;Hur, Cheol-Goo;Yoo, Jong-Shin;Park, Young-Mok
    • Journal of Plant Biotechnology
    • /
    • v.29 no.3
    • /
    • pp.161-170
    • /
    • 2002
  • For the hairy root of Panax ginseng, we have got mass spectrums from MALDI/TOF/MS analysis and Tandem mass spectrums from ESI/Q-TOF/MS analysis. While mass spectrum provides the molecular weights of peptide fragments digested by protease such as trypsin, tandem mass spectrum produces amino acid sequence of digested peptides. Each amino acid sequences can be a query sequence in BLAST search to identify proteins. For the specimens of animals or plants of which genome sequences were known, we can easily identify expressed proteins from mass spectrums with high accuracy. However, for the other specimens such as ginseng, it is difficult to identify proteins with accuracy since all the protein sequences are not available yet. Here we compared the mass spectrums and the peptide amino acid sequences with ginseng expressed sequence tag (EST) DB. The matched EST sequence was used as a query in BLAST search for protein identification. They could offer the correct protein information by the sequence alignment with EST sequences. 90% of peptide sequences of ESI/Q-TOF/MS are matched with EST sequences. Comparing 68% matches of the same sequences with the nr database of NCBI, we got more matches by 22% from ginseng EST sequence search. In case of peptide mass fingerprinting from MALDI/TOF/MS, only about 19% (9 proteins of 47 spots) among peptide matches from nr DB were correlated with ginseng EST DB. From these results, we suggest that amino acid sequencing using tandem mass spectrum analysis may be necessary for protein identification in ginseng proteome analysis.

The Observations of Water, Carbon Dioxide, Hydrgen, Nitrogen, Oxygen, Carbon Monoxide and Methane as Impurities in Natural Garnets (석류석의 불순물인 물, 이산화탄소, 수소, 질소, 산소, 일산화탄소 및 메탄의 고찰)

  • R. Everett Langford;A. A. Giardini;Charles E. Melton
    • Journal of the Korean Chemical Society
    • /
    • v.17 no.5
    • /
    • pp.353-356
    • /
    • 1973
  • A unique method of destructive analysis has been developed for the study of gaseous impurities in minerals. Samples are crushed in a high vacuum sample system of a research mass spectrometer. This is done by means of a suitably designed crusher which is incorporated in the inlet system of the instrument. Crusher elements are constructed of tungsten carbide. The mass spectrometer used for this preliminary study has a detection sensitivity of about $10^{-10}cc$at STP. In a study of rhodolite garnets obtained from near Lavonia, Georgia, U.S.A., the gases$H_2$, $O_2$, $H_{2}O$, $CO_2$, CO, and $CH_4$have been identified and their composition determined.

  • PDF

BIACORE 바이오센서를 이용한 B형 간염 표면항원 정량분석의 기초연구

  • Yu, Chang-Hun;Ryu, Gang;Jeon, Jun-Yeong;Lee, Hyeon-Ik;Choe, Seong-Cheol;Lee, Eun-Gyu
    • 한국생물공학회:학술대회논문집
    • /
    • 2001.11a
    • /
    • pp.231-234
    • /
    • 2001
  • We performed a basic experiment for rapid. on-line, real-time measurement of HBsAg by using a BIACORE biosensor, a chip-based sensor utilizing surface plasmon resonance technology to quantify the recognition and interaction of biomolecules. We immobilized an a -HBsAg antibody on a CM5 chip surface which was activated by N-hydroxysuccinimide for amine coupling with HBsAg, and measured the mass increase from the coupling. This study showed the potential of this biosensor-based method as a rapid, multi-sample, on-line assay. Once properly validated, it can serve as a more powerful method for HBsAg quantification.

  • PDF

저진공, 고진공, 초고진공 영역에서의 잔류가스질량분석기 설계특성

  • Park, Chang-Jun;An, Jong-Rok;Jo, Bok-Rae;Han, Cheol-Su;An, Sang-Jeong
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2014.02a
    • /
    • pp.108.2-108.2
    • /
    • 2014
  • 잔류가스측정 질량분석기(RGA)는 진공챔버 내부의 진공상태 이상유무, 공정상태 확인 및 주입가스 농도제어 등 여러 종류의 작업에 응용되고 있다. 반도체용 박막 제조공정(PVD, CVD)에서 챔버 내의 수분 혹은 불순물 가스의 정확한 모니터링은 반도체 품질향상에 매우 중요하다. 1 Pascal 진공도의 증착용 챔버에 RGA를 직접 장착하여 작동시키기 위해서는 저진공용 RGA가 사용되어야 한다. 10-3 Pascal에서 6m 자유운동거리를 갖는 질소분자는 1 Pascal에서는 6 mm로 짧은 자유운동거리를 갖는다. 따라서 1 Pascal 저진공영역에서 이온을 생성시키고 mass filter를 사용하여 질량분석을 하기 위해서는 이온원과 mass filter 길이가 자유운동거리 수준으로 작아져야한다. 저 진공영역에서는 검출기와 전자방출용 필라멘트가 저진공에서 작동되도록 일반고진공용 RGA와는 완전히 다르게 소형으로 설계 제작되어야 한다. 10-7 Pascal 이상의 초고진공에서 사용되는 RGA는 이온원이 작동할 때 발생하는 outgassing을 낮추도록 설계가 되어야 초고진공의 유지가 가능하다. 한국표준과학연구원에서 현재 개발 중인 일반고진공용 RGA를 소개하고 저진공용과 초고진공용 RGA의 설계특성을 발표한다.

  • PDF

A Real Vehicle Tracking Acceleration Using A Tire-Wheel-Tracking Machine (제작차륜이동 시험기의 실동주행 가속도측정)

  • Sung, Ikhyun;Seung, Seoungyoul
    • Journal of the Society of Disaster Information
    • /
    • v.7 no.3
    • /
    • pp.190-197
    • /
    • 2011
  • In this paper, an analytical and experimental study is performed in order to determine the effects of interaction between a vehicle and a structure. For this purpose, a wheel tracking machine and an adequate single span bridge are designed. Results presented in the paper show that the real vehicle tracking accelerations including the interaction between the vehicle and the structure produce additional effects on the dynamic behavior of the structure including reversal and contrary behavior. Also, the interaction between the vehicle and the bridge is reproduced by applying the identified real vehicle tracking accelerations to a general finite element analysis program.