• Title/Summary/Keyword: 주사형 전자 현미경

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Creep Behaviours of Duplex Stainless Steel (2상 스테인리스강(STS 329J1)의 크리프 특성)

  • Hwang Kyung Choong;Kwon Jong Wan;Yoon Jong Ho
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.14 no.2
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    • pp.42-47
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    • 2005
  • Micro duplex stainless steel is used to denote a fine scale two-phase micro structure consisting austenite and firrite. The development of this structure was done by proper thermo-mechanical processing. The objective of present investigation is to study creep characteristics of this alloy. Since we have little design data about the W behaviors of the alloy. An apparatus has been designed and built fir conducting creep tests under constant load conditions. A series of creep tests on them have been performed to get the basic design data and life prediction of micro duplex stainless steel products and we have gotten the 1311owing results. First the stress exponents decrease as the test temperatures increase. Secondly, the creep activation energy Gradually decreases as the stresses become higher. Thirdly, the constant of Larson-Miller Parameters on this alloy is estimated as about 5. Last, the fiactographs at the creep rupture show both the ductile and brittle fracture modes according to the creep conditions.

Creep Behaviours of Inconel 690 Alloy (인코넬 690 합금의 크리프거동)

  • 황경충;윤종호;최재하;김성청
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.11 no.4
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    • pp.54-61
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    • 2002
  • Inconel 690 alloy has widely been used in power plant and high temperature facilities because it has high thermal resistance and toughness. But we have little design data about the creep behaviors of the alloy. Therefore, in this study, an apparatus has been designed and built for conducting creep tests under constant load conditions. A series of creep tests on Inconel 690 alloy have been performed to get the basic design data and life prediction of inconel products and we have gotten the following results. First, the stress exponents decrease as the test temperatures increase. Secondly, the creep activation energy gradually decreases as the stresses become bigger. thirdly, the constant of Larson-Miller Parameters on this alloy is estimated about 10. And last the fractographs at the creep rupture show both the ductile and the brittle fracture according to the creep conditions.

Preparation of Oriented MFI Zeolite Membranes (배향된 MFI 제올라이트 박막의 제조)

  • Song, Kyeong-Keun;Ha, Kwang
    • Korean Chemical Engineering Research
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    • v.44 no.3
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    • pp.243-247
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    • 2006
  • MFI zeolite membranes were prepared on anodic alumina (Anodisc) as support. First, silicalite-1(${\approx}1.2{\mu}m$) seed crystals were attached to the surface of the support via chemical bonding, and the a- and b-axis oriented zeolite membranes could be synthesized on the support coated with the monolayer of the seed crystals by secondary growth hydrothermal synthesis. The zeolite membranes prepared were characterized using scanning electron microscope and analyzed by X-ray diffraction.

Creep Behaviours of Glasses Rim Material Alloy (안경테소재 합금(Ti-6AI-4V)의 크리프 특성)

  • 황경충;윤종호
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2003.10a
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    • pp.248-253
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    • 2003
  • Titanium alloy has widely been used as glasses rim material because it has high specific strength and also is light, harmless to men. But, we have little design data about the creep behaviors of the alloy. Therefore, in this study, an apparatus has been designed and built for conducting creep tests under constant load conditions. A series of creep tests on them have been performed to get the basic design data and life prediction of titanium products and we have gotten the following results. First, the stress exponents decrease as the test temperatures increase. Secondly, the creep activation energy gradually decreases as the stresses become bigger. Thirdly, the constant of Larson-Miller parameters on this alloy is estimated about 13. And last, the fractographs at the creep rupture show both the ductile and the brittle fracture according to the creep conditions.

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Study on Cutting Characteristics of WC-Co with Micro Cutting in SEM (SEM 내 마이크로 절삭에 의한 초경합금재의 절삭 특성에 관한 연구)

  • 허성중
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.10
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    • pp.74-81
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    • 2003
  • This paper describes that the micro-cutting of WC-Co using PCD (Polycrystalline Diamond) and PcBN (Polycrystalline Cubic Boron Nitride) cutting tools are performed with SEM(Scanning Electron Microscope) direct observation method. The purpose of this study is to present reasonable cutting conditions to obtain precise finished surface and machining efficiency. Summary of the results are shown below: (1) The thrust cutting forces tend to increase more than the principal forces as the depth of cut and the cuttlllg speed are increased preferably on orthogonal microcutting. (2) The tool wear in the flank face was formed larger than that in the rake face on orthogonal micro cutting. (3) The wear appearance for PCD tools is abraded by hard WC particles of the work materials, which lead diamond grain to be detached from the bond.

Creep Behaviour of Al-Zn-Mg Ternary Aluminum Alloy (Al-Zn-Mg 3원계 알루미늄 합금의 크리프 거동)

  • 윤종호;황경충
    • Transactions of the Korean Society of Automotive Engineers
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    • v.12 no.1
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    • pp.203-208
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    • 2004
  • To make practical applications of Al-Zn-Mg ternary aluminum alloy effectively in various field, a series of static creep tests under the 16 temperature-stress combination conditions had been performed. The creep tester with constant stress loading was designed and made by the authors and used in this study. The higher the creep temperature rose, the less the stress exponents became. The bigger the applied stresses became, the less values the creep strain activation energy showed. The life prediction constant of Larson-Miller parameter was calculated as about 2.3. In the fractography, the ductile fracture with dimples by intergranular breakage was primarily observed. We can make practical use of these test data in the design, the life prediction and the prevention of the accidents of the thermal facilities, etc.

A Study on Fracture Characteristics of Woven Carbon Fiber Reinforced Composite Material (직물탄소 섬유강화 복합재료의 파괴특성에 관한 연구)

  • 김광수;김상태
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.16 no.3
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    • pp.497-505
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    • 1992
  • 본 연구에서는 최근에 개발된 직물 탄소섬유강화 복합재료의 파괴인성치를 정 량적으로 결정하고 파괴거동을 조사하고자 한다. 본 연구의 목적은 이 재료에 선형 탄성파괴역학의 적용여부를 알아보고, R곡선을 이용하여 균열의 생성점 및 불안정 파 괴점의 파괴인성치를 정확히 구하며, 주사형 전자현미경을 통해 파단면 및 균열 성장 시점을 관찰하여 파괴거동을 조사하는데 있다.

Catchodoluminescence Study of GaN Films Grown by Low-Pressure Metalorganic Chemical Vapor Deposition (저압 유기 금속 화학 증착법으로 성장시킨 GaN박막의 캐소드루미네슨스에 대한 연구)

  • 홍창희
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.36D no.5
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    • pp.63-68
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    • 1999
  • In this paper, the correlation between the growth mechanism and the optical property in GaN films grown by low-pressure metalorganic chemical vapor deposition was characterized using room temperature cathodoluminescence spectroscopy. An intense near band-edge emission, 364nm, and deep-level emission, 550nm, were observed. The intensity of 364nm peak was increased with increasing the beam current. Also the peak position of 364nm emission was red-shifted and the intensity of 550nm peak was increased with increasing the accelerating voltage. It shows that the deep-level emission is strongly associated with crystalline defects in the GaN at early stage. The relationship between the microstructure and the deep level emission observed by scanning electron microscope images and cathodoluminescence spectra was carefully analyzed.

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Fabrication of the photon scanning tunneling microscope with constant intensity mode (일정광량 방식의 광자주사현미경 제작)

  • Kim, Ji-Taek;Choi, Wan-Hae;Jo, Jae-Heung;Chang, Soo;Kim, Dal-Hyun;Koo, Ja-Yong;Chung, Seung-Tae
    • Korean Journal of Optics and Photonics
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    • v.10 no.3
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    • pp.195-200
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    • 1999
  • We made sharp optical fiber tips with less than 100 nm diameter by using the heating and pulling method with a good repetition and fabricated the photon scanning tunneling microscope (PSTM) using constant intensity mode. The 3-dimensional PZT (Piezoelctric transducer) scanner made of a long PZT tube is consisted of three divided parts, that is, a pair of $\pm$ x and a pair of $\pm$y scanning parts and a z scanning part for the fine approach and scanning. The scanning dimension is 1.43 $\mu\textrm{m}$$\times$1.76 $\mu\textrm{m}$. The height of a optical tip to maintain a constant height within $1/{\lambda}_0$ (${\lambda}_0$ is the incident wavelength) from surface of a specimen to a optical tip is controlled automatically by using the electric feedback circuit. The 3-dimensional shape of standing evanescent waves generated on the surface of a dove prism was measured successfully by using the constant intensity mode PSTM.

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Surface ultrastnlcture of metacercaria and adult of Gymnophalloides seoi (Digenea: Gymnnophallidae) (참굴큰입흡충의 피낭유충 및 성충의 표피 미세구조)

  • 최민호;박원진
    • Parasites, Hosts and Diseases
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    • v.33 no.4
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    • pp.289-296
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    • 1995
  • The surface ultrastructure of metacercariae and adults of Gymnophallokles seoi, the only known gymnophallid infecting humans, was observed by scanning electron microscopy. Metacercariae were ovoid or pyriform in shape and slightly concave ventrally. The oral sucker had two sizes of type I papillae, small and large, encircling its lip. Type I papillae were arranged in a row on both side oi the body. The ventral pit had several type I papillae on its inner surface. The ventral sucker was covered with cobble-stone like cytoplasmic processes and had 6 type I papillae on its lip. The surface of the body was covered with the tegumental spines except for the ventromedian area between the two suckers. The spines at anterior body were digitated into 3-5 points, and their size decreased at posterior one third or the body. Adult worms were rhomboid or ellipsoid in shape and covered with tegumental spines except for the ventromedian area. The shape and distribution of the tegumental spines and sensory papillae were similar to those of metacercariae. However, sensory papillae arranged in a row on the ventral surface of metacercariae were not observed in adults. The ventral pit became larger and more prominent as the fluke grew. It is suggested that the ventral pit function as an additional adhesive organ to the host tissue.

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