• Journal of Sensor Science and Technology
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• v.7 no.1
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• pp.67-72
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• 1998

The crystallized CuPc and PbTe films are formed by thermal evaporation and pulsed ArF excimer laser ablation. Structural and electrical properties of thin film is observed by XRD and current-voltage(I-V) curves. From XRD analysis, both PbTe and CuPc thin films show a-axis oriented structure. For the measurement of photovoltaic effect, the transverse current-voltage curve of CuPc/Si, PbTe/Si and PbTe/CuPc/Si junctions have been analyzed in the dark and under illumination. The PbTe/CuPc/Si junction exthibits a strong photovoltaic characteristics with short circuit current($J_{sc}$) of $25.46\;mA/cm^{2}$ and open-circuit voltage($V_{oc}$) of 170 mV. Quantum efficiency and power conversion efficiency are calculated to be 15.4% and $3.46{\times}10^{-2}$, respectively. Based on the results of QE and ${\eta}$, the photocurrent process of PbTe/CuPc/Si junction can be explained as following three effective steps; photocarrier generation in the CuPc layer, carrier separation at PbTe/CuPc interface, and finally a transportation of electrons through the PbTe layer.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.02a
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• pp.273-273
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• 2010

고열부하 환경에 노출되는 핵융합로의 플라즈마 대향부품은 주로 낮은 원자번호 물질-열전도가 좋은 물질-구조체의 순으로 다층 구조를 이루고 있으며, 이들 간의 우수한 접합성은 부품의 성능을 좌우하는 핵심 요소이다. 이러한 플라즈마 대향부품의 건전성을 평가하기 위해서는 고열속의 열부하를 반복적으로 인가하는 시험이 요구되며, 이를 위해 본 연구원에서는 KoHLT-1, 2의 시험시설을 운용하고 있다. 본 시설에서는 열부하원으로서 그라파이터 히터를 사용하며, 히터는 두 개의 시험 대상부품 사이에 설치되고, 히터에 고전류를 인가하여 복사열에 의해 시험 부품에 열부하를 가하게 된다. 고열부하 환경에서 열피로 시험을 위해 히터에 인가되는 전류를 시간에 따라 일정한 패턴으로 반복적으로 ON-OFF 하게 된다. 본 논문에서는 이러한 고열부하시험을 수행함에 있어 고려해야 할 여러 가지 요소에 대해 논의하였다. 우선 인가하는 열유속(heat flux) 값은 일차적으로 시험시설의 최대 출력에 의해 좌우되며, 시험대상물의 운전조건 및 열부하 반복횟수에 의해 결정된다. 열부하 반복횟수는 주어진 열유속 값에 대해 total strain이 파단에 이르는 수준에 의해 결정된다. 열부하를 인가하는 시간은 히터에 전류를 인가했을 때 요구되는 온도로 상승하는 데 걸리는 시간과 시험대상물의 온도가 더 이상 증가하지 않는데 걸리는 시간에 의해 좌우된다. 냉각시간은 길수록 시험대상물의 온도가 냉각수의 온도에 접근하게 되나 너무 길어지면 시험시간이 급격히 증가하게 되므로, 온도 감소 곡선을 검토하여 적절한 시간을 정하게 된다. 열유속 측정은 냉각수의 온도 상승값과 유량으로부터 계산하게 되며, 정확한 측정을 위해서는 열부하를 인가하는 시간이 충분히 길어야 한다. 또한 시험대상 부품에서 열부하가 인가되는 면적을 정확히 정의해야 하며, 냉각관로에 열부하가 인가되어서는 않된다. 또한 시험대상부품을 지지하는 지지구조체를 통한 열손실을 최소화해야 정확한 열유속을 측정할 수 있다. 시험대상부품을 설치할 때 히터와의 간격 또한 결정해야 할 중요한 요소이며, 간격이 좁을수록 최대 열유속 값을 증가시킬 수 있으나, 너무 가까운 경우 히터의 열변형에 의한 접촉 및 아크 방전의 가능성이 있으며, 이 경우 히터와 시험대상부품의 손상을 가져오게 된다. 시험대상물이 국제열핵융합로(ITER)의 일차벽과 같이 베릴륨이 포함되어 있는 경우 방전에 의한 손상은 인체에 유해한 오염의 원인이 될 수 있다. 또한 순간적인 방전은 고가의 고전류전원의 고장을 유발할 수도 있다. 열부하 시험 중 시험대상물의 온도를 정확히 측정하는 것은 필수적이며, 온도 변화 곡선으로부터 시험대상물의 건전성 여부를 판단할 수 있다. 이를 위해 변화를 가장 잘 탐지 할 수 있는 위치에 온도 센서를 설치하는 것이 관건이며, 이는 사전 분석을 통해 알 수 있다.

• Conservation Science in Museum
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• v.29
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• pp.153-162
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• 2023

Clay figure of Baekje, produced by forming and molding various shapes using clay, are mainly excavated from temple sites and provide essential information for studying the Buddhist art of Baekje. Research on clay figures of Baekje primarily focuses on the characteristics of Baekje-era temples in which such figures are excavated, as well as the role and production techniques of clay figures, by comparing regional and morphological characteristics. In particular, research on the manufacturing method of clay figures is mainly carried out by visual observation, whereas precise scientific analysis is required to understand production techniques and characteristics of raw materials in greater detail. In this study, to confirm such production techniques and material characteristics, computed tomography (CT) scans were conducted on the Clay Bodhisattva excavated from the Neungsan-ri Temple site in Buyeo. As a result, it was found that the Clay Bodhisattva was made using a cylindrical core of fine clay, tied together with several thin branches or reeds with straws. The clay used in the figure bore traces indicating the presence of herbaceous plants, which increase adhesion between clay and prevent cracks in the contraction process. On the other hand, the density of the fine clay differs on the inside and outside of the clay figure. Based on this, it is presumed that the clay was applied around the cylindrical core to shape the Clay Bodhisattva. The clay was reapplied on top of the figure to express the detailed shape and pattern.

• Journal of Powder Materials
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• v.20 no.2
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• pp.114-119
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• 2013

In the DBC (direct bonding of copper) process the oxygen partial pressure surrounding the AlN/Cu bonding pairs has been controlled by Ar gas mixed with oxygen. However, the direct bonding of Cu with sound interface and good adhesion strength is complicated process due to the difficulty in the exact control of oxygen partial pressure by using Ar gas. In this study, we have utilized the in-situ equilibrium established during the reaction of $2CuO{\rightarrow}Cu_2O$ + 1/2 $O_2$ by placing powder bed of CuO or $Cu_2O$ around the Cu/AlN bonding pair at $1065{\sim}1085^{\circ}C$. The adhesion strength was relatively better in case of using CuO powder than when $Cu_2O$ powder was used. Microstructural analysis by optical microscopy and XRD revealed that the interface of bonding pair was composed of $Cu_2O$, Cu and small amount of CuO phase. Thus, it is explained that the good adhesion between Cu and AlN is attributed to the wetting of eutectic liquid formed by reaction of Cu and $Cu_2O$.

• Journal of Life Science
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• v.10 no.3
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• pp.229-235
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• 2000

The absorption characteristics of Korean yam powder according to different drying methods were investigated. The physical properties of yam powder by different drying methods were showed the biggest porosity in freeze drying sample, while the smallest in hot air drying sample. No difference was founded in proximate compositions of yam powder by various drying methods. The amount of total phenolic compound and Vit C were showed the bigger decrement in freeze dried sample than other drying methods. The time reaching to equilibrium moisture content were determined in 12 days. Monolayer moisture contents were predicted to 0.0508∼0.0588 by BET equation and 0.0705∼0.0811 g H2O/g solid by GAB equation. BET equation for isothermal absorption curve showed over 0.95 R-square for every drying methods. GAB equation showed over 0.99 in vacuum and freeze drying but a poor R-square in hot air drying.

• Journal of Welding and Joining
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• v.33 no.2
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• pp.47-55
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• 2015

With using adaptive control of the resistance spot welding machine, the advantage on electrode life time for galvanized steels has been addressed. This study was aimed to evaluate the electrode life time of galvanized steels with applying the constant current control and the adaptive control resistance spot welding process for a comparison purpose. The growth in diameter of electrode face was similar for both the constant current and the adaptive control up to 2000 welds. The button diameter was decreased with weld numbers, however, sudden increase in button diameter with use of the adaptive control after 1500 welds was observed. The peak load was continuously decreased with increasing number of welds for both the constant current and the adaptive control. The current compensation during a weld was observed with using the adaptive control after 1800 welds since the ${\beta}$-peak on dynamic resistance curve was detected at later weld time. The current compensation with adaptive control during resistance spot welding enhanced the nugget diameter at the faying interface of steel sheets and improved the penetration to thinner steel sheet.

• Journal of the Korean Wood Science and Technology
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• v.19 no.1
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• pp.22-30
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• 1991

This study was carried out to determine the Joint characteristic of L-type specimens. L-type specimens were made of two kinds uf solid woods(Antiaris, Sepetir) and three kinds of wood based materials(plywood, particleboard, medium density fiberboard). They were constructed with PVC anchor and screw, and were discussed with joint strength and stiffness coefficients. The obtained results were as follows: 1. Bending strength showed very high increasing rate from one to three used PVC anchor and screw but was a little rise from three to four used PVC anchor and screw in solid wood. However. in wood based materials, it was unchanged without increasing rate or slight decreased from three to four used PVC anchor and screw. 2. The stiffness coefficients, or Z-values, were in the range from $4.704\times10^{-4}$ to $1.864\times10^{-3}$(rad/kgf-cm). They showed $10^{-3}$ level in one PVC anchor and screw but $10^{-4}$ level in two, three. four PVC anchor and screw. Accordingly, they indicated flexible joints in one PVC anchor and screw and relatively stable joints in two, three. four PVC anchor and screw. 3. Measured ultimate bending moments were 258.70kgf-cm in plywood and 142.68kgf-cm in medium density fiberboard. 4. Comparing with dowel joint. the joint strength used PVC anchor screw was inferior to 8mm and 10mm dowel diameter but differ little from 6mm dowel diameter.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.2 no.2
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• pp.7-10
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• 2001

Recently, most jewelry design employ multiple prongs that grasp the front surface of the jewel to the metal frame To keep up with recent trends in fashion. jewelry manufacturers need to produce single-prong neckalces and earings constructed with non-precious metals. In responce to this demand, Ameth Development Division and The University of Seoul researched jointly and developed a technique for setting the jewel safely using a single prong with less weight. The setting process consists of making a small trench through the jewel at the mounting point and using a low melting point tin solder, to fill the trench and bonding with the prong. The application or this technology in the setting of a natural amethyst to a single 18K gold prong resulted in a 40% reduction in cost and weight and improvement of feeling for wearing.

• Analytical Science and Technology
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• v.23 no.1
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• pp.60-67
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• 2010

A sensitive competitive heterogeneous bioluminescence immunoassay for serotonin was developed using photoprotein, aequorin as a label for the first time with the optimal assay conditions; especially, serotoninavidin conjugate was prepared by Mannich reaction and the synthetic process of serotonin-avidin conjugate was optimized by controlling the initial molar ratios of serotonin, formaldehyde and avidin (1:12,000:25). The developed bioluminescence immunoassay for serotonin showed good sensitivity (LOD of 0.68 ng/mL) with wide area of dynamic range ($5.0{\times}10^{-10}\;M\sim5.0{\times}10^{-7}\;M$). (cf. the range for serotonin in human blood serum is $151{\pm}45\;ng$/mL). In addition, cross-reactivity studies demonstrated that 5-methoxytryptamine showed some cross-reactivity (28.0%), whereas 3-methylindole, melatonin and 5-hydroxylindole-3-acetic acid showed no crossreactivity, and good recoveries were obtained in serum. Thus, this developed method provides a good tool to monitor serotonin in serum.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.10 no.10
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• pp.2779-2785
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• 2009

Among the livestock, chickens are raised because of the merit ingested protein in low-priced cost of production and are primary livestock increased the consumption of meat. The factors of influencing condition, odor is the most important factor. Odor substances are ammonia, amines, hydrogen sulfide and mercaptan which come from night soil. Livestock are prevented from rearing by means of these odor substances. Though the henhouse is heated using hot air type heater in the winter season, it is ventilated for the control of odor because of the increase of odor concentration. In the present work, composite catalytic system combined the existing facilities(hot air type heater) with catalytic system was developed, it could controled odor and hazardous gas using the oxidation/reduction reaction without extra operating cost. Moreover, the purpose of this work is to develop the catalysts which are cost competitive and can maximize energy efficiency. The catalysts are noble metal(Pt-Rh) and composite transition metal(Mn) type.