• Title/Summary/Keyword: 접착강도시험

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Comparison of metal wire reinforcement and glass fiber reinforcement in repaired maxillary complete denture (상악 총의치 정중 파절 수리 시 금속선 및 유리섬유의 보강효과 비교)

  • Lee, Jung-Ie;Jo, Jae-Young;Yun, Mi-Jung;Jeon, Young-Chan;Jeong, Chang-Mo;Huh, Jung-Bo
    • The Journal of Korean Academy of Prosthodontics
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    • v.51 no.4
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    • pp.284-291
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    • 2013
  • Purpose: This study compared fracture strength and fracture modes between metal wire reinforcement and glass fiber reinforcement in repaired maxillary complete denture. Materials and methods: In this study, fracture was reproduced on center of maxillary complete dentures and the denture was repaired with auto-polymerizing resin. The experimental groups (n = 10) were subjected to the following condition: without reinforcing material (control group), reinforcing with metal wire (W group), reinforcing with glass fiber pre-impregnated with light-curing resin (SES MESH, INNO Dental Co., Yeoncheon, Korea, G group). The fracture strength and fracture modes of a maxillary complete denture were tested using Instron test machine (Instron Co., Canton, MA, USA) at a 5.0 mm/min crosshead speed. The flexure load was applied to center of denture with a 20 mm diameter ball attachment. When fracture occurred, the fracture mode was classified based on fracture lines. The Kruskal-wallis test and the Mann-whitney U test were performed to identify statistical differences at ${\alpha}=.05$. Results: W group showed the highest value of fracture strength, there was no significant difference (P>.05) between control group and G group. Control group and W group showed anteroposterior fracture mainly, group W showed adhesive fracture of denture base and reinforcing material. Conclusion: In limitation of this study, the glass fiber did not improve the fracture strength of repaired maxillary complete denture, and adhesive failure was occurred along the lines of glass fiber.

Effect of delayed time, surface treatment, and repair material on shear bond strength of repaired bis-acryl composite resin (수리된 비스 아크릴 복합 레진의 전단결합강도에 대한 지연시간, 표면처리, 수리 재료의 영향)

  • Park, Ji-su;Lee, Jae-In
    • Journal of Dental Rehabilitation and Applied Science
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    • v.34 no.2
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    • pp.89-96
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    • 2018
  • Purpose: The aim of this study was to evaluate the effect of delayed time, surface treatment, and repair materials on repair of bis-acryl composite resin through comparison of shear bond strength and to evaluate the utility of bis-acryl composite resin repair using polymethyl methacrylate resin. Materials and Methods: A total of 90 bis-acryl composite resin specimens were fabricated and classified into 9 test groups, each of 10 pieces according to delayed time, surface treatment and repair material. The shear bond strength of each specimen was measured using a universal testing machine immediately after fabrication and analyzed using a statistical analysis program (IBM SPSS statistics 20). After the shear bond strength measurement, the fracture surface of the specimen was observed. Results: The highest shear bond strength ($17.54{\pm}3.14MPa$) was observed in the experimental group bonded immediately with a light-curing flowable composite resin using a bonding agent. Conclusion: When repairing bis-acryl composite resin, it is necessary to consider whether to remake according to the delayed time. For effective repair, it is desirable to consider appropriate materials and surface treatment methods according to the site or purpose of use.

Development of a Drainage System to Mitigate Moisture Damage for Bridge Deck Pavements (교면포장의 수분손상 저감을 위한 체류수 배수공법 개발)

  • Lee, Hyun-Jong;Kim, Hyung-Bae;Seo, Jae-Woon
    • International Journal of Highway Engineering
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    • v.9 no.2 s.32
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    • pp.129-140
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    • 2007
  • A major purpose of this study is to develop a drainage system that can quickly drain water penetrated into pavement layers to mitigate pot holes which is one of the major distress types in bridge deck pavements. This system can be established by applying a thin drainage layer between waterproof and pavement layers. The most important elements for this system are the performance of waterproof layer and construction technique for the thin drainage layer. The porous asphalt mix with the maximum aggregate size of 10mm is first developed based on the porous asphalt mix design guide proposed by NCAT, and various physical and mechanical tests are performed to confirm that the porous mix satisfies all the specification requirements. In addition, a series of laboratory tests including low-temperature bending and bonding strength tests for the MMA(Methyl Methacrylate) type of waterproofing material. It is observed from the tests that the MMA material satisfies all the specification requirements. To evaluate the Reld performance of the drainage system, a field study has been conducted on a relatively small size bridge. The QC/QA tests are conducted on the both waterproofing and pavement materials. It has been found that the drainage system works well to drain the water penetrated into the pavement layers.

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A Study on Shear Bond Strength of Core-veneer Interface for Bilayered all Ceramics (Bilayered all Ceramics에서 Core와 Veneer 계면의 전단결합강도에 관한 연구)

  • Jung, Yong-Su;Lee, Jin-Han;Lee, Jae-In;Dong, Jin-Keun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.24 no.3
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    • pp.231-242
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    • 2008
  • Purpose: The purpose of this study was to investigate the bond strength of the core-veneer interface in all ceramic systems. Material and Methods: The all ceramic systems tested with their respective veneer were IPS Empress 2 with IPS Eris, IPS e.max Press with IPS e.max Ceram and IPS-e.max ZirCAD with IPS e.max Ceram. Cores (N=36, N=12/group, diameter: 10mm, thickness: 3mm) were fabricated according to the manufacturer's instruction and cleaned with ultrasonic cleaner. The veneer(diameter: 3mm, thickness: 2mm) were condensed in stainless steel mold and fired on to the core materials. After firing, they were again ultrasonically cleaned and embedded in acrylic resin. The specimens were stored in distilled water at $37^{\circ}C$ for 1 week. The specimens were placed in a mounting jig and subjected to shear force in a universal testing machine(Z020, Zwick, Germany). Load was applied at close to the core-veneer interface as possible with crosshead speed of 1.00mm/min until failure. Average shear bond strengths(MPa) were analyzed with a one-way analysis of variance and the Tukey test(${\alpha}=.05$). The failed specimens were examinated by scanning electron microscopy(JSM-6360, JEOL, Japan). The pattern of failure was classified as cohesive in core, cohesive in veneer, mixed or adhesive. Results: The mean shear bond strength($MPa{\pm}SD$) were IPS e.max Press $32.85{\pm}6.75MPa$, IPS Empress 2 $29.30{\pm}6.51MPa$, IPS e.max ZirCAD $28.10{\pm}4.28MPa$. IPS Empress 2, IPS e.max Press, IPS e.max ZirCAD were not significantly different from each others. Scanning electron microscopy examination revealed that adhesive failure did not occur in any all ceramic systems. IPS Empress 2 and IPS e.max Press exhibited cohesive failure in both the core and the veneer. IPS e.max ZirCAD exhibited cohesive failure in veneer and mixed failure.

The effect of silane treatment timing and saliva contamination on shear bond strength of resin cement to porcelain (Silane의 처리시기와 타액오염이 도재-레진 시멘트의 전단 결합강도에 미치는 영향)

  • Ro, Young-Seon;Ryu, Jae-Jun;Suh, Kyu-Won
    • The Journal of Korean Academy of Prosthodontics
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    • v.47 no.1
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    • pp.61-69
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    • 2009
  • Statement of problem: Porcelain veneers have become a popular treatment modality for aesthetic anterior prosthesis. Fitting porcelain veneers in the mouth usually involve a try-in appointment, which frequently results in salivary contamination of fitting surfaces. Purpose: An in vitro study was carried out to investigate the effect of silane treatment timing and saliva contamination on the resin bond strength to porcelain veneer surface. Material and methods: Cylindrical test specimens (n=360) and rectangular test specimens (n=5) were prepared for shear bond test and contact angle analysis. Whole cylindrical specimens divided into 20 groups, each of which received a different surface treatment and/or storage condition. The composite resin cement stubs were light-polymerized onto porcelain adherends. The shear bond strengths of cemented stubs were measured after dry storage and thermocycling (3,000 cycles) between 5 and $55^{\circ}C$. The silane and their reactions were chemically monitored by using Fourier Transform Infrared Spectroscopy analysis (FTIR) and contact angle analysis. One-way analysis of variance (ANOVA) and Dunnett's multiple comparison were used to analyze the data. Results: FT-IR analysis showed that salivary contamination and silane treatment timing did not affect the surface interactions of silane. Observed water contact angles were lower on the saliva contaminated porcelain surface and the addition of 37% phosphoric acid for 20 seconds on saliva contaminated porcelain increased the degree of contact angle. Silane applied to the porcelain, a few days before cementation, resulted in increasing the bond strength after thermocycling. Conclusion: Within the limitation of this study, it can be concluded that it would be better to protect porcelain prosthesis before saliva contamination with silane treatment and to clean the contaminated surface by use of phosphoric acid.

Prediction of Ultimate Strength and Strain of Concrete Columns Retrofitted by FRP Using Adaptive Neuro-Fuzzy Inference System (FRP로 보강된 콘크리트 부재의 압축응력-변형률 예측을 위한 뉴로퍼지모델의 적용)

  • Park, Tae-Won;Na, Ung-Jin;Kwon, Sung-Jun
    • Journal of the Korea Concrete Institute
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    • v.22 no.1
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    • pp.19-27
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    • 2010
  • Aging and severe environments are major causes of damage in reinforced concrete (RC) structures such as buildings and bridges. Deterioration such as concrete cracks, corrosion of steel, and deformation of structural members can significantly degrade the structural performance and safety. Therefore, effective and easy-to-use methods are desired for repairing and strengthening such concrete structures. Various methods for strengthening and rehabilitation of RC structures have been developed in the past several decades. Recently, FRP composite materials have emerged as a cost-effective alternative to the conventional materials for repairing, strengthening, and retrofitting deteriorating/deficient concrete structures, by externally bonding FRP laminates to concrete structural members. The main purpose of this study is to investigate the effectiveness of adaptive neuro-fuzzy inference system (ANFIS) in predicting behavior of circular type concrete column retrofitted with FRP. To construct training and testing dataset, experiment results for the specimens which have different retrofit profile are used. Retrofit ratio, strength of existing concrete, thickness, number of layer, stiffness, ultimate strength of fiber and size of specimens are selected as input parameters to predict strength, strain, and stiffness of post-yielding modulus. These proposed ANFIS models show reliable increased accuracy in predicting constitutive properties of concrete retrofitted by FRP, compared to the constitutive models suggested by other researchers.

STUDY ON THE SHEAR BOND STRENGTH OF ALL-IN-ONE DENTIN BONDING SYSTEM (우치에 대한 All-in-one 상아질 결합제의 전단결합강도 비교 연구)

  • Park, Hyung-Joo;Yoo, Seung-Hoon;Kim, Jong-Soo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.33 no.4
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    • pp.661-672
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    • 2006
  • This study was performed to compare the shear bond strength of AQ Bond $Plus^{TM}$ with AQ $Bond^{TM}$ and Single $Bond^{TM}$. Also by observing the fractured interface under scanning electro-microscope, the fracture pattern and the quality of hybrid layer were analyzed. The possibility of clinical application of all-in-one system which has an advantage to reduce chair time for children with difficult behavior pattern was evaluated, The results obtained are as follows ; 1. There was no significant difference between AQ $Bond^{TM}$ and AQ Bond $Plus^{TM}$ in shear bond strength and Single Bond showed the highest bond strength with statistical significant difference (p<0.05). 2. Adhesive fracture pattern was mainly observed in both enamel/dentin in AQ $Bond^{TM}$ and AQ Bond $Plus^{TM}$ group while Single Bond group showed equal numbers for cohesive and adhesive pattern. 3. Under scanning electro-microscope, resin tags observed in AQ $Bond^{TM}$ and AQ Bond $Plus^{TM}$ were very weak and tangled while strong and thick tags were shown with many lateral branches in Single Bond. Careful case selection and accurate clinical application is recommended when using AQ $Bond^{TM}$ and AQ Bond $Plus^{TM}$considering the result showing its weaker strength than Single $Bond^{TM}$.

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THE EFFECTS OF MECHANICAL AND THERMAL FATIGUE ON THE SHEAR BOND STRENGTH OF ORTHODONTIC ADHESIVES (기계적 및 열적 피로가 교정용 접착제의 결합강도에 미치는 영향)

  • Shin, Wan-Cheal;Kim, Jong-sung;Kim, Jong-Ghee
    • The korean journal of orthodontics
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    • v.26 no.2 s.55
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    • pp.175-186
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    • 1996
  • The purpose of this study was to examine the effects of mechanical and thermal fatigue on the shear bond strength(SBS) of stainless steel mesh brackets bonded to human premolar teeth with 3 no-mix adhesives. The stainless steel mesh bracket was Ormesh(Ormco, .022 slot) and three types of no-mix adhesives were Ortho-one(Bisco), $Monolok^2$(RMO), $System\;1^+$(Ormco). The $10^6$ loadcycles of $17.4{\times}10^2sin2{\pi}ftlg{\cdot}cm$ and the 1,000 thermocycles of 15 second dwell time in each bath of $5^{\circ}C\;and\;55^{\circ}C$ were acturated as mechanical and thermal fatigue stress, and SBS were measured after each fatigue test. The fracture sites were analyzed by stereoscope and scanning electron microscope. The results obtained were summarized as follows; 1. Before thermocycles, $Monolok^2$ showed the highest Knoop hardness number(KHN, $64.03kg/mm^2$) and $System\;1^+$ showed the lowest value($31.60kg/mm^2$). After thermocycling, $Monolok^2$ also showed the highest KHN($38.03kg/mm^2$) and $system\;1^+$ showed the minimum($20.87kg/mm^2$). The KHN of Ortho-one, $Monolok^2,\;System\;1^+$ significantly decreased after thermocycling (P<0.01). 2. In static shear bond test, three adhesives had no significant differences in the SBS(P>0.01). 3. After thermocycling test, $Monolok^2$ showed the maximum SBS($19.34{\pm}2.75MPa$) and Ortho-one showed the minimum SBS($13.66{\pm}2.23MPa$). The SBS of Ortho-one(P<0.01) and $System\;1^+$(P<0.05) significantly decreased after $10^3$ thermocycles. 4. The SBS of three adhesives after $10^6$ loadcycles were similar and were not significantly decreased compared with static group(P>0.01). 5. The failure sites were usually bracket/resin interface in all groups irrespective of experimental conditions.

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Testing and Numerical Analysis on the Fracture Characteristics of Composite Adhesive Bonded Single-Lap Joints (복합재료 Single-Lap 본딩 조인트의 파괴 특성에 대한 실험 및 수치해석 연구)

  • 김광수;박재성;장영순;이영무
    • Composites Research
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    • v.16 no.5
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    • pp.45-53
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    • 2003
  • The experimental and numerical investigations on the failure characteristics of the secondary bonded composite single-lap joints were performed. The initiations and growths of cracks were observed using CCD camera and acoustic emission sensor during the tension tests of the joint specimens. The structural behaviors of the specimens were predicted by the geometric nonlinear two-dimensional finite element analysis. The three types of observed initial cracks were included in each finite element models and the strain energy release rates of each specimen models were calculated by VCCT(Virtual Crack Closure Technique) technique. The tension tests showed that the initial cracks occurred in the 60∼90% of final failure loads and the major failure modes of the specimens were adhesive failure and the delamination between the 1st and 2nd ply of laminate. The specimens with the thicker bondline had earlier crack initiation loads but higher crack propagation resistance and eventually better loading capability. The delaminations were mostly observed in the thicker bondline specimens. The mode I values of calculated strain energy release rates were higher than the mode II values in the all specimen models considering the three types of initial cracks. The mode I and total strain energy release rates were calculated as higher values in the order of initial crack in the edge interface, comer interface and delamination between the plies of laminate.

A Study on the Water Permeability and Drying Shrinkage of Polymer Cement Composites (폴리머 시멘트 복합체의 투수성 및 건조수축에 관한 연구)

  • Jo, Young-Kug
    • Journal of the Korea Institute of Building Construction
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    • v.9 no.5
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    • pp.71-77
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    • 2009
  • In a range of forms, such as latex, water-soluble polymer, liquid resin, and monomer, polymer dispersions have been widely used in the construction industry as cement modifiers because of their excellent properties, such as acid-resistance, water-proofness, and good ductility in mortar and concrete. Polymer cement slurry (polymer-modified slurry) is made of cement and polymer dispersions, with a high polymer-cement ratio of 50% or more. The purpose of this study is to evaluate the water permeability and drying shrinkage of polymer cement mortar (polymer-modified mortar) and cement concrete coated by polymer cement slurry. The polymer cement mortar and cement concrete are prepared with various polymer types, polymer-cement ratios and curing methods, and are tested for water permeability, drying shrinkage and strength. The test results showed thatthe weight of permeable water of polymer cement mortar decreases with an increase in the polymer-cement ratio, reaching a minimum at the polymer-cement ratio of 20%. In particular, the weight of permeable water of St/BA-modified mortar with a polymer-cement ratio of 20% coated with St/BA-modified slurry is about 1/55 that of unmodified mortar. The EVA- and St/BA-modified slurries coated on cement concrete have about 4 or 5 times higher drying shrinkage compared to cement concrete. The strength of polymer cement mortars tends to increase with a higher polymer-cement ratio, and is considerably higher than that of unmodified mortar. It is thus concluded that polymer cement mortars coated by polymer cement slurry are effective for industrial application, and have superior properties such as waterproofness and strengths, compared with conventional cement mortar.