• Title/Summary/Keyword: 전자제품

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$CH_4-H_2-N_2 $ 기체계에서 MW-PACVD를 이용한 결정상의 합성

  • 김도근;백영준;성태연
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.54-54
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    • 1999
  • 다이아몬드 합성시 질소 첨가는 Cn 화합물의 합성가능성을 비롯하여 다이아몬드의 질소 도핑, 성장 속도 및 결정성 변화 등 다양한 관점에서 중요한 의미를 가지고 있다. 본 연구에서는 다이아몬드의 일반적인 합성조건에서 질소를 첨가하여 합성된 막의 형상 및 상 변화에 대해 고찰하였다. 막은 다이아몬드 전처리시킨 Si 기판위에 microwave plasma CVD 장치를 이용하여 합성하였다. 유입되는 혼합가스(CH4+H2+N2)에서 N2 첨가량을 0-95%까지 변화시켰다. 이때 CH4 농도는 5%로 고정하였고, 합성온도는 90$0^{\circ}C$-115$0^{\circ}C$까지 변화시켰다. 이와 같이 합성된 막의 표면조직 및 성장 두께를 측정하기 위해 주사전자현미경을 이용하였다. 상의 분석은 Raman, XRD 및 TEM 분석을 이용하였으며, 조성분석을 위해 XPS 및 AES를 사용하였다. 질소 첨가량에 따라 합성된 막은 첨가하지 않은 경우에 다이아몬드 결정에서 시작하여 질소첨가에 따라 결정면이 깨지는 것으로 나타났다. 그러나 30%, 45%의 경우는 다시 결정면이 나타났다. 다량의 질소가 첨가되었을 때, 다시 결정면을 보이는 다이아몬드가 합성된 것은 매우 흥미로운 결과이다. 한편 질소와 메탄만의 기체하에서는 다시 결정면이 관찰되지 않았다. 이들 상의 구조는 XRD 및 TED 분석을 통해 모두 다이아몬드로 확인되었다. 기체내의 질소의 첨가에 관계없이 고상내에 질소는 확인되지 않았다. 따라서 이방법에 의한 CN 화합물의 합성은 힘든 것으로 보여진다. 이들 실험 결과를 근거로 온도 및 조성에 따른 기체의 열역학적 계산을 통하여 합성거동과의 연관성을 검토하였다. anode는 매우 높은 충전용량을 갖는데 첫 번째 방전시에 Li2O를 생성하여 비가역적 반응을 나타내고 계속되는 충방전 동안 Li-Sn 합금이 생성되어 2차전지의 가역적 반응을 가능하게 한다. SnO2 는 대기중에서 Li 금속보다 안정하기 때문에 전지의 제작 공정 및 사용 면에서 매우 우수한 물질이지만 아직까지 SnO2 구조적 특성과 전지의 충, 방전 특성에 대한 관계의 규명을 위한 정확한 정설은 제시되고 있지 못하다. 본 연구에서는 TFSB anode 물질로써 SnOx박막을 상온에서 여러 전도성 콜렉터 위에 증착하여 그 충, 방전 특성을 보고하였다. 증착된 SnOx박막의 표면은 SEM, AFM으로 분석하였으며 구조의 분석은 XR와 Auger electron spectroscope로 하였다. 충, 방전 특성을 분석하기 위하여 리늄 foil을 대극과 참조 전극으로 하여 EC:DMC=1:1, 1M LiPF6 액체 전해질을 사용한 Half-Cell를 구성하여 100회 이상의 정전류 충, 방전 시험을 행하였다. Half-Cell test 결과 박막의 구조, 콜렉터의 종류 및 Sn/O비에 따라 서로 다른 충, 방전 거동을 나타내었다.다. 거의 없었다. 5mTorr 일 때가 가장 좋았다.수 있음을 알 수 있었다. 그러므로, RNA바이러스의 하나인 BVDV의 viral replicon을 이용하여 다양한 종류의 포유동물 세포에 유전자 발현벡터로써 사용할 수 있음으로 post-genomics시대에 다양한 종류의 단백질 기능연구에 맡은 도움이 되리라 기대한다.다양한 기능을 가진 신소재 제조에 있다. 또한 경제적인 측면에서도 고부가 가치의 제품 개발에 따른 새로운 수요 창출과 수익률 향상, 기존의 기능성 안료를 나노(na

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The formation of N-Nitrosamine in Commercial Cured Products 2. The effect of cooking methods on N-Nitrosamine formation in commercial Ham and Sausages (시판 식육제품 중 N-Nitrosamine의 생성 제2보. 조리방법이 햄 및 소시지의 N-Nitrosamine 생성에 미치는 영향)

  • 박계란;이수정;신정혜;성낙주;임상선
    • Journal of Food Hygiene and Safety
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    • v.13 no.4
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    • pp.406-411
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    • 1998
  • Representive cured products such as ham and sausage produced in Korea were purchased at retail and cooked using heating tools such as a gas range (GR), an electric range (ER) and electric range after boiled (BE). Changes of N-nitrosamine (NA), nitrate and nitrite in the cured meats containing< $2.0\;\mu\textrm{g}/kg$ of N-nitrosodimethylamine (NDMA) were checked and analyzed during their cooking process. Contents of nitrate and nitrite in ham products prior to cooking were 2.0 and 1.8 mg/kg, respectively; their contents in regular hams were slightly increased, but those of nitrate in press hams were decreased while those of nitrite were increased during its cooking process. Their contents in sausage products were 1.8 and 0.9 mg/kg; those of nitrate were decreased, while nitrite were slightly increased during its cooking process. NDMA detected only NA in all the collected cured products. Changes of NDMA, regardless of cooking methods, tend to drastically increase in all samples after their cooking; Its contents were increased by average 6.0~70.7 times in the GR samples, by average 2.4~39.2 times in the ER samples and by average 7.0~56.3 times in the BE samples. Virtually, the fact that all of this nitrosamine appeared to arise by the action of precursor such as NOx was produced during the cooking of cured products.

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Antioxidative Capacity and Quality Characteristics of Yanggaeng using Fermented Red Ginseng for the Elderly (발효홍삼 농축액을 이용한 노인용 기능성 간식(양갱)의 항산화성 및 품질특성)

  • Kim, Ae-Jung;Han, Myung-Rhun;Lee, Soo-Jeong
    • The Korean Journal of Food And Nutrition
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    • v.25 no.1
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    • pp.83-89
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    • 2012
  • In this study red ginseng was extracted with ethanol and then fermented by yeasts including Lactobacillus casei and Bifidobacterium longum. Fermented red ginseng extracts(FRGE) were found to be more effective antioxidants in vitro with regards to 1,1-diphenyl-2-picrylhydrazyl(DPPH) radical scavenging activity than red ginseng extracts(RGE). In FRGE, the contents of ginsenosides $Rb_1$, $-Rb_2$ and -Rc were much lower than in RGE, however, the contents of ginsenosides 20(S)$-Rg_3$, 20(R)$-Rg_3$ and compound K were higher than RGE. FRGE was added to Yanggaeng(0, 5, 10, 15, 20%), and physicochemical and sensory evaluations of the Yanggaeng were conducted. The L and b values of Yanggaeng with added FRGE were decreased by increasing the ratio of FRGE, while the a value was increased. Sensory evaluations for, taste, color, flavor, texture and overall acceptability of Yanggaeng with addition of FRGE (10%) were applicable for improving the Yanggaeng product.

HVPE growth of Mg-doped AlN epilayers for high-performance power-semiconductor devices (고효율 파워 반도체 소자를 위한 Mg-doped AlN 에피층의 HVPE 성장)

  • Bae, Sung Geun;Jeon, Injun;Yang, Min;Yi, Sam Nyung;Ahn, Hyung Soo;Jeon, Hunsoo;Kim, Kyoung Hwa;Kim, Suck-Whan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.27 no.6
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    • pp.275-281
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    • 2017
  • AlN is a promising material for wide band gap and high-frequency electronics device due to its wide bandgap and high thermal conductivity. AlN has advantages as materials for power semiconductors with a larger breakdown field, and a smaller specific on-resistance at high voltage. The growth of a p-type AlN epilayer with high conductivity is important for a manufacturing an AlN-based applications. In this paper, Mg doped AlN epilayers were grown by a mixed-source HVPE. Al and Mg mixture were used as source materials for the growth of Mg-doped AlN epilayers. Mg concentration in the AlN was controlled by modulating the quantity of Mg source in the mixed-source. Surface morphology and crystalline structure of AlN epilayers with different Mg concentrations were characterized by FE-SEM and HR-XRD. XPS spectra of the Mg-doped AlN epilayers demonstrated that Mg was doped successfully into the AlN epilayer by the mixed-source HVPE.

TEM 도파관을 이용한 전자파 장해 측정 연구 및 표준화 동향

  • 권종화
    • The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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    • v.13 no.1
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    • pp.51-62
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    • 2002
  • EMI/EMS 측정을 위해서는 주변 전자파 잡음(background noise)이 낮은 야외시험장(Open Area Test Site)이 가장 바람직하나, 근래 전자(전기 기기 사용의 증가와 방송.무선통신 시스템의 다양화로 인한 인공잡음(artificial noise)의 증대로 조건에 부합된 부지 선정이 어렵고, 설치 비용이 매우 크며 날씨 변화에 따라 시험 계획이 변경 될 수도 있는 단점이 있다. 전자파 분-무반사실(Semi Anechoic Chamber)은 대부분의 환경 잡음을 감쇠시키므로 야외시험장처럼 장소의 구애를 받지 않아 도시나 혹은 제품 생산지 가까이에 설치 운용이 가능하다. 그러나 큰 설치 공간과 많은 시설 유지 비용을 필요로 하며, 저주파 대역에서는 반사에 의한 공진을 완전히 제거할 수 없어 성능이 떨어진다. 또한, 최근 컴퓨터 CPU의 동작주파수가 급속하게 높아지고 PCS, IMT-2000 등과 같은 이동전화의 사용주파수도 계속해서 높아짐에 다라 미연방통신위원회(Federal Communication Commission)에서는 5㎓까지의 복사 방출 시험을 요구하고 있다. IEC 61000-4-3 복사 내성 시험규격도 휴대폰 주파수인 2㎓까지 확장되었으며 IMT-2000, Bluetooth 등 새로운 이동통신서비스가 속속 개발됨에 따라 18㎓ 까지 시험 주파수가 확장되는 추세이다. 그러나, 현재 국내 각 연구실에서 보유하고 있는 야외시험장이나 전자파 반-무반사실의 경우 1㎓이상에서의 시험이 곤란하여 수 ㎓주파수대역에서 시험이 가능한 복사 및 내성시험 시설이 필요하게 되었다. 이러한 문제점들을 해결하기 위해 고안된 대용 측정 시설 중 대표적인 것이 TEM 셀이나 GTEM셀과 같은 TEM 도파관(waveguide) 형태의 장비들이다. 이들은 본래 EMS 측정을 위한 장비이지만 협소한 공간이나 외부와의 전자파 간섭의 우려가 없고, 설치가 비교적 자유로워 여러 연구기관에서 도파관 원리를 이용한 측정 방식을 연구(개발하여 범용적인 전자파 적합성 측정 장비로서 활용하고 있다. 야외시험장과 무반사실 등이 안테나에 의한 피시험기기 주변 공간에서의 1점 측정으로 인해 시험 시간이 많아 소요되는 공통적인 단점이 있는 반면, TEM 도파관에 의한 측정은 일단 피시험기기의 모델링 정보만 얻어지면 계산에 의해 EMI 측정을 바로 할 수 있다. <표 1>에서 현재 상용화되어 사용되고 있는 TEM/GTEM 셀, 야외 시험장 및 전자파 무반사실에 대해 EMI 측정과 관련된 몇 가지 사안에 대해 비교하였다. 본 문서에서는 야외시험장이나 전자파 반-무반사실 등과 같은 기존 EMI/EMS 측정 시설의 단점을 보완하고, 광대역 특성을 갖는 대용 측정 시설로서의 TEM 도파관에 대해 소개하고 야외시험장 결과와의 상관관계 알고리즘 및 표준화 동향에 대해 기술하였다. 2절에서는 대표적인 TEM 도파관 구조의 측정 시설인 TEM 셀과 GTEM 셀의 전기적.구조적 특징에 대해 간단히 기술하고, 3절에서는 TEM 셀과 GTEM 셀에서이 측정결과를 이용하여 야외 시험장 결과를 얻어내는 상관관계 알고리즘에 대해 기술하였다. 4절에서는 IEC/CISPR와 TC77에서의 표준화 활동을 중심으로 현재 진행중인 TEM 도파관 관련 표준화 동향과 내용에 대해 기술하고자 한다.

The Quality Characteristic and Antioxidant Properties of Saccharified Strawberry Gruels (당화 딸기죽의 품질특성 및 항산화능)

  • Kim, Jin-Sook;Kim, Ja-Young;Chang, Young-Eun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.41 no.6
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    • pp.752-758
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    • 2012
  • We conducted this study to investigate the quality and antioxidant properties of saccharified strawberry gruel with different ratios of strawberry rice mash. Different samples of saccharified strawberry gruel with different ratios of strawberry puree were prepared, and the proximate composition, sweetness, pH, acidity, color difference, texture, free sugar, sensory evaluation, and physiological activities of the sample were measured. With increasing strawberry puree content, the proximate compositions, sweetness, and total acidity of the strawberry gruel increased, and pH decreased significantly (p<0.05). Saccharified strawberry gruel prepared with 15% to 45% strawberry puree displayed significantly lower viscosity. As the amount of strawberry puree increased, the Lvalue, and b-value decreased, whereas the a-value increased. The free sugar content of fructose, glucose, maltose, sucrose, and total free sugar increased significantly (p<0.05). Strawberry gruel with 30% added strawberry puree was the most preferred for, its color, flavor, taste, texture, and overall acceptability preference. With increasing strawberry puree content, the total polyphenol contents, total flavonoid contents, DPPH, and ABTS radical scavenging of strawberry gruel increased significantly (p<0.05). From these results, we found that adding 30% strawberry puree was the best way to make gruel with high sensory qualities.

The Effect on Technology Innovation Performance of Private-Public R&D Cooperation of ICT SMEs: Focused on Collaboration with Government-funded Research Institutes (ICT 중소기업의 산·연 R&D협력이 기술혁신성과에 미치는 영향: 출연연구기관과의 협력을 중심으로)

  • Park, Wung;Park, Ho-Young;Yeom, Myoung-Bae
    • Asia-Pacific Journal of Business Venturing and Entrepreneurship
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    • v.12 no.6
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    • pp.139-150
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    • 2017
  • In Korea, small and medium-sized enterprises (SMEs) play an pivotal role in the national economy, accounting for 99.9% of all enterprises, 87.9% of total employment, and 48.3% of production. In spite of their crucial role in the national development, most of SMEs suffer from a lack of R&D related resources. Public R&D organizations such as government-funded research institutes can provide SMEs with valuable supplementary technological knowledge and help them build technological capacity. In this regard, this study estimated the effect of internal R&D investment and private-public R&D cooperation on technological innovation of ICT SMEs based on 2016 ETRI Survey. Building on previous literatures, the study established and tested a research model using binary logistic regression analysis. First, internal R&D investment and preferences for open innovation demonstrated the strengthening of R&D collaboration. Second, internal R&D investment and R&D cooperation showed a positive effect on both product and process innovation. Therefore, internal R&D capability and taking advantage of R&D collaboration are needed to achieve technological innovation for SMEs in ICT sector. This study also discuss implications for encouraging private-public R&D cooperation.

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Comparative analysis of students and teachers' perceptions on internet-based learning style (사이버 학습에서 학습양식에 대한 학습자와 교수자의 인식차이 분석)

  • Cho Eun-Sun;Kim In-Sook
    • Proceedings of the Korea Contents Association Conference
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    • 2005.05a
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    • pp.19-30
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    • 2005
  • This study examined student's and teachers' perceptions of learning style on internet-based learning. Many research have studied student's learning style both in traditional learning settings and inter-based learning settings. These studies emphasized that student's learning style is one of the important indicators of establishing learning strategies and expecting positive learning outcomes. However, it has been rare to find the comparative analyses between learners and teachers to see how differently they perceive the learning style on internet-based learning. This study analyzed 386 elementary and 627 middle school students and 130 cyber teachers. They filled out the 15 items questionnaire on internet-based learning style. The results showed that the student's and teachers preferred the self-directed internet learning style rather than cooperative and dependent styles. However, the teachers judged the students more self-directed and dependent style preferred than the students self perception. In conclusion, this study suggests the differentiated teaching-learning design and development strategies on internet learning, especially based on subject matter. Also, there should be advanced tutor strategies considering learners' different learning styles. Finally, many research on internet learning styles should be conducted in various learning areas and learner ages and characteristics.

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The Effect of Heat Sterilization on the Surface Topography and the Tensile Properties in Various Nickel Titanium Wires Including a Korean Product (열멸균과정이 nickel titanium호선의 기계적 성질과 표면상태에 미치는 영향)

  • Kim, Byoung-Ho;Nahm, Dong-Seok;Yang, Won-Sik
    • The korean journal of orthodontics
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    • v.28 no.6 s.71
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    • pp.927-935
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    • 1998
  • The purpose of this study is to investigate the changes of mechanical properties and surface topography of various nickel titanium wires after heat sterilization for recycling with quantitative method. The materials used were four kinds of nickel titanium orthodontic wires including a Korean product. Experimental specimens were treated with two kinds of heat sterilization methods ; dry heat ($180^{\circ}C$, 60min) and autoclave ($121^{\circ}C$, 15-20psi, 30min). Mechanical properties were evaluated by tensile test with Instron 4466 (load cell capacity:.1000 kg, cross head speed:5mm/min, grip distince:40mm in room temperature). Surface topography of various wires was compared with each other qualitatively by using scanning electron microscopy and quantitatively by using profilometer. The findings were analyzed statistically with student t-tests. The results were as follows; 1. Neither method of heat sterilization had any effects on tensile properties of the nickel-titanium wires used in this experiment. 2. Before heat sterilization, the surface smoothness was highest in Optimalloy, followed by Align and Sentalloy, with NiTi showing the lowest smoothness value. 3. In surface topography, Align and Optimalloy were not influenced by heat sterilization. NiTi, on the other hand, had increased roughness after dry heat sterilization and Sentalloy showed the same tendency after each of the two heat sterilization procedures.

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Experimental Study on the Properties of Solid Material Made by Autoclave Curing according to CaO/SiO2 Ratio and W/B (CaO/SiO2비 및 W/B 변화에 따른 오토클레이브 양생 경화체의 특성에 관한 실험적 연구)

  • Kang, Cheol;Kang, Ki-Woong;Kim, Jin-Man
    • Journal of the Korea Concrete Institute
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    • v.21 no.5
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    • pp.557-563
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    • 2009
  • This study is on the properties of inorganic porous calcium silicate material made from silica powder through the autoclaving curing, the results of this study should be utilized fundamental data for the development of noise reduction porous solid material using siliceous byproduct generated by various manufacture process. For the manufacture of autoclave curing specimen, various calcareous materials used and siliceous materials used silica powder. In this study, properties in density and compressive strength according to the change of W/B and C/S ratio, microscopy for the shape of pore, SEM and XRD for the examination of hydrate after autoclave curing are carried out respectively. The test results shown that the more slurry density decrease, the more W/B increase at the fresh state, this tendency shown similar to in hardened state. Among the specimens of C/S ratio, the compressive strength of C/S ratio of 0.85 gave the highest the compressive strength. In the results of XRD, tobermorite generated by autoclaving curing was created all of specimens regardless of C/S ratio. To ascertain pore structure, we compared with existing porous calcium silicate product(ALC, organic sound absorbing porous material). The results of microscope observation, pore structure of specimen of this study was similar to that of existing inorganic sound absorbing foam concrete. therefore, we could conformed a possibility of sound absorbing porous solid material on the basis of the results.