• Title/Summary/Keyword: 재료과학적 특성

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Material properties and clinical application of zirconia-reinforced lithium silicate ceramics (지르코니아 강화 리튬 실리케이트 세라믹의 특성과 임상적용)

  • Kim, Jong-Eun;Kim, Jee-Hwan;Shim, June-Sung;Park, Young-Bum
    • The Journal of the Korean dental association
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    • v.56 no.3
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    • pp.159-166
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    • 2018
  • The zirconia-reinforced lithium silicate ceramic material is a material in which lithium silicate glass contains about 10% by weight of zirconia oxide (zirconia oxide). This material has both the advantages of glass ceramics and zirconia, and it is attracting attention as a CADCAM material for single tooth restoration. ZLS materials have improved strength compared to widely used e.max (lithium disilicate ceramic) materials. It can be used for single crown restoration and ensuring a thickness of 1.5 mm is very important for reliable treatment. In the case of Celtra Duo, heat treatment may be helpful in terms of strength and abrasion resistance. Hydrofluoric acid treatment is helpful for bonding and hydrofluoric acid for a short time may not help to improve the bonding strength. Although zirconia-reinforced lithium silicate ceramic materials have been continuously conducted and published in the laboratory, reliable clinical studies are still lacking. Additional clinical studies will be a very important part of establishing a scientific basis.

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An Analysis of Material Property on Eartherwares Excavated at Auraji site in Jeongseon (정선 아우라지 출토 토기의 재료과학적 특성 분석)

  • Lee, Byeong Hoon
    • Journal of Conservation Science
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    • v.37 no.5
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    • pp.545-556
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    • 2021
  • In this study, we aimed to elucidate the materialistic characteristics of 11 pieces of earthenware belonging to the Neolithic and Bronze Age excavated from Jeongseon Auraji, South Korea. As a result, the chemical composition of earthenwares belonging to the early Bronze Age was distributed in the intermediate area between the Neolithic and Bronze Age earthenwares, but no significant difference was confirmed based on their manufacturing period. Upon comparison, the earthenwares excavated from Jeongseon Auraji site were found to comprise less acidic components than those excavated from Yeongdong, and are characterized by the alkaline components depending on the excavated site. In the rare earth elements distribution pattern, all the analyzed earthenwares exhibited similar pattern, confirming that the raw materials present in the clay were the same. As a result of microstructure analysis, the clay particles and voids were found to be irregularly distributed in the analyzed earthenwares. Neolithic earthenwares exhibited many irregular voids, and an arrangement of aluminosilicate, including feldspar, was observed along with the clay substrate. Furthermore, we confirmed that the empty space in early Bronze Age earthenwares was filled with fine particles and cube crystals. Moreover, the main mineral phase of earthenwares excavated from Jeongseon Auraji exhibited similar composition, and therefore, there was no significant difference in the firing temperature of these earthenwares. The firing temperature of the earthenwares ranged from 750 to 850℃.

Analysis of characteristics of natural resins using organic residue analysis organic materials attached on wooden coffins from Singok-dong Site, Uijeongbu (유기잔존물 분석을 활용한 천연 수지 특성 분석 - 의정부 신곡동 유적 출토 목관 부착 유기물을 중심으로 -)

  • YUN, Eunyoung
    • Korean Journal of Heritage: History & Science
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    • v.54 no.4
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    • pp.78-89
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    • 2021
  • Organic residues analysis is an analysis method that reveals the types of organic material samples by using the characteristic that main components constituting substances are different depending on the species of animals and plants. In this study, scientific analysis of the organic residues attached to wood coffins in the Joseon Dynasty Hoemyo excavated from the site of Singok-dong, Uijeongbu was used to identify the types of remnants and to use them as information to restore the uses of organic materials and the way they lived in the past. As a result of FT-IR analysis of the residue attached to the inside of the wood, it was estimated to be a natural plant resin material. In addition, as a result of analysis by GC-MS to confirm the characteristic factors of natural resins, diterpenoids (abietane) and pimaran (pimarane), such as dehydroabietic acid and pimaric acid (diterpenoid) compounds, and saturated and unsaturated fatty acid components were detected together. Diterpenoid compounds are components mainly found in Pinaceae resins. It is confirmed in the literature that rosin, a representative material of Pinaceae resin, was used as an adhesive material. Considering the situation where an organic material remained at the joint of the wood, the organic material attached to the wood is judged to be an adhesive material made of Pinaceae resin. In addition, the fatty acid component detected together is a component derived from plant oil, and it is presumed to be made by mixing rosin and oil as recorded in previous studies. This study confirms that organic residues remain in the burial environment without losing their characteristics. It is expected that scientific analysis of organic residues will be conducted in the future to accumulate information necessary for the interpretation of past living culture.

Conservation Treatment and Scientific Investigation of Daehye Bogakseonsaseo (Letters of Master Bogak) in the Goryeo Dynasty (고려시대 대혜보각선사서의 보존처리 및 과학적 조사)

  • Jang Yeonhee
    • Conservation Science in Museum
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    • v.29
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    • pp.47-64
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    • 2023
  • Daehye Bogakseonsaseo (Letters of Master Bogak) in the possession of the National Museum of Korea is a Goryeo-era book produced in 1387, which was acquired in 2005 in a state of severe general damage. Subsequently, its production techniques and materials were examined using bibliographical characteristics and scientific analysis, based on which an overall conservation treatment was carried out. Janghwang(mounting) in bibliographical characteristics is a five-hole-stitch binding (五針眼線裝本), a single-lined rectangular box (四周單邊), and no column lines. The conservation treatment was examined in two aspects: the basic form and the conservation treatment process. The book is composed of the outer cover, original cover, end paper, and inner paper of 0.04-0.07mm thick, which is significantly thinner than general book paper. The conservation treatment was applied after the entire book was disassembled, based on the assessment that both the cover and the inner sheets of paper were in a dire condition due to deterioration. The conservation treatment comprised of the process of disassembly, cleaning, reinforcement of defective parts, scanning, and binding, with a paulownia box made for its storage. At the time of disassembly, samples were made for the inner sheets and the book string in order to conduct fiber identification. The fibers were identified using Safranin and C-stains. Safranin staining identified a thick fiber wall, in addition to cross-marking, dislocation, and transparent membranes. C-stain staining identified the fiber as mulberry, given the dark red residue. The book strap has a flat, circular cross-section, and was identified as cotton fiber, since a lumen was observed in the center.

MCC의 부유부상 효율에 미치는 MCC의 표면에너지와 액상의 표면장력의 영향에 대한 기초연구

  • Lee, Hak-Rae;Lee, Jin-Hui;Park, Il;Lee, Yong-Min;Han, Sin-Ho;Jo, Jung-Yeon
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2001.11a
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    • pp.20-20
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    • 2001
  • 우리나라 제지산업은 화학펼프의 80%를 수입에 의존하고 었으나 고지회수율 및 이용율이 세계적으로 볼 때 매우 높은 환경친화적 산업이다. 고지 재활용 공정 중에 서 가장 핵심적인 공정인 부유부상 공정은 고상계의 표면특성 차이를 이용하여 소수성 의 잉크업자를 기포에 부착시켜 부상을 통하여 제거하는 공정이다. 고지 사용의 고도화 를 위해서는 부유부상 공정의 효율 증대가 절실히 요구되고 있다. 또한 부유부상 공정 의 핵심적인 인자로 부유부상을 통하여 제거되는 고형물질의 표면 특성 특히 소수화도 가 중요하다는 것은 보고된 바 있으나 부유부상에 필요한 표면 특성의 존재 여부와 표 면 에너지와 부유부상 효율의 관계 등에 관한 기본적인 연구가 더욱 필요한 실정이다. 이에 본 연구에서는 부유부상 공정을 기초과학적 측면에서 규명하기 위해 마 이 크로 크리 스탈린 셀룰로오스(Microcrystalline cellulose: MCC)를 모델 물질로 사용하 고 이들의 표면특성을 접촉각 측정을 통하여 평가하였다. 친수성의 표면 특성을 지닌 M MCC의 표면 특성을 소수성으로 바꾸기 위하여 AKD(alkyl ketene dimer)의 함량별로 사이징 처리하여 소수성을 지닌 잉크를 모벨링 하고 친수성 MCC를 염색시약을 이용 하여 흑색으로 염색함으로써 소수화 된 MCC와의 색차를 두어 섬유를 모델링 하였다. 이렇게 제조된 MCC의 소수화 정도를 평가하기 위하여 분말상태인 MCC를 pellet으로 제조하여 각기 다른 표면장력과 표변특성을 지난 용액을 이용하여 Advancing Contact A Angle을 측정하고 다양한 방법으로 이를 분석하여 시료의 표면에너지를 평가하였다 그 리고 부유부상 셀내의 액상의 이온강도와 표면장력 등 화학적인 인자에 의한 부유부상 분리효과를 평가하였다.있었다 (그림 2). 칼렌다는 종이를 높은 전단력과 압축력으로 변형시키는데 비해 도침은 단순히 압축 압력만을 종이에 가하는 것이 다르다고 볼 수 있는데, 라 이너지와 백상지가 같은 조건하에서 왜 이러한 큰 차이를 보이는 이유를 아직 알수 없다.해 동일한 공정 데이터들올 이용하여 보편적으로 사용하는 통계기법 중의 하나인 주성분회귀분석을 실시하였다. 주성분 분석은 여러 개의 반응변수에 대하여 얻어진 다변량 자료의 다차원적인 변 수들을 축소, 요약하는 차원의 단순화와 더불어 서로 상관되어있는 반응변수들 상호간 의 복잡한 구조를 분석하는 기법이다. 본 발표에서는 공정 자료를 활용하여 인공신경망 과 주성분분석을 통해 공정 트러블의 발생에 영향 하는 인자들을 보다 현실적으로 추 정하고, 그 대책을 모색함으로써 이를 최소화할 수 있는 방안을 소개하고자 한다.금 빛 용사 둥과 같은 표면처리를 할 경우임의 소재 표면에 도금 및 용 사에 용이한 재료를 오버레이용접시킨 후 표면처리를 함으로써 보다 고품질의 표면층을 얻기위한 시도가 이루어지고 있다. 따라서 국내, 외의 오버레이 용접기술의 적용현황 및 대표적인 적용사례, 오버레이 용접기술 및 용접재료의 개발현황 둥을 중심으로 살펴봄으로서 아직 국내에서는 널리 알려지지 않은 본 기 술의 활용을 넓이고자 한다. within minimum time from beginning of the shutdown.및 12.36%, $101{\sim}200$일의 경우 12.78% 및 12.44%, 201일 이상의 경우 13.17% 및 11.30%로 201일 이상의 유기의 경우에만 대조구와 삭제 구간에 유의적인(p<0.05) 차이를 나타내었다.는 담수(淡水)에서 10%o의 해수(海水)로 이주된지 14일(日) 이후에 신장(腎臟)에서 수축된

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Literature Review on The Korean Traditional Non-Alcoholic Beverages -II. Recent Status of Research and Developments- (한국 전통음료에 관한 문헌적 고찰 -II. 최근의 연구동향-)

  • Lee, Cherl-Ho;Kim, Sun-Young
    • Journal of the Korean Society of Food Culture
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    • v.6 no.1
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    • pp.55-60
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    • 1991
  • The scientific research results on the Korean traditional non-alcoholic beverages published in the literatures were reviewed. A total of 79 research papers were collected; 11 papers were on green tea, 38 on tea analog, 3 on rice tea, 4 on roasted cereal powder, 9 on malt saccharified rice beverage, 1 on ginger-fruit drink, 10 on fruits drink and 5 papers on others. Most of the researches were concerned to the chemical composition and processing conditions. More researches are needed on the quality requirements of the ingredients, the keeping qualify of the products and the industrialization of the traditional processing methods.

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A Study on Metal Bound Rims Adhered to the Brim of Ceramics (도자기 구연에 부착된 금속 테두리 연구)

  • Hwang, Hyun-Sung;Yang, Pil-Seung;Seo, Jeong-Ho
    • Journal of Conservation Science
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    • v.22
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    • pp.109-120
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    • 2008
  • Understanding the whole knowledge of ceramics is essential for a person in charge of conservation of ceramics since their methods of manufacturing or materialistic features have very close relationship with their damaging process. Also, various executions of repair and restoration dealing with any damage in use have to be looked into. The information attained through those studies finds damaging causes of ceramics, which becomes a critical element when choosing a proper conservation treatment method and utilizes as indispensable data for permanent preservation. As part of scrutinizing materials of repair and restoration, this study examines the purpose, date, and the constituents of the materials used in metal bound rims adhered to the brim of ceramics. Among the subjected ceramics, the metal bound rims possible to scientific analysis were gone through element analyses with Portable ${\bullet}\"{I}$-XRF Spectrometer and SEM-EDS while the ingredients of the ceramics difficult to analyze were inferred by eye inspection of exhibition catalogues. The results of this study confirm that metal bound rims consisted of diverse materials were adhered to the brim of ceramics.

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Making Technique Studies of Mural Paintings in the No. 6 Tomb of Songsanri, Gongju (공주 송산리 6호분 벽화의 제작기술 고찰)

  • Han, Kyeong-Soon
    • Journal of Conservation Science
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    • v.27 no.4
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    • pp.451-458
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    • 2011
  • This study aims at identifying wall painting production technique of Songsanri No. 6 tomb based on optical examination and scientific analysis along with the investigation of written records of ancient wall paintings. The result displays that bricks with mortar were used for the construction of the wall, and masonry joint were made of lime, sand and gypsum. The surface of brick were plastered with black and thereafter with white lime. Finely sifted clay on the top of the white surface, were applied not with plasterer's trowel but with a brush for making ground surface. The clay are mineral particles smaller than $30{\mu}m$ of silt. The wall paintings of Sonsanri No. 6 is the only example of making ground layer with clay for painting of Sasindo (literally four heavenly animals painting) among remaining wall paintings of ancient tombs. The historical value of the painting should be attributed not only in terms that it displays a rare production techniques which were never discovered in any other paintings in Korea and Asia, but also it might had been uncompleted when the tomb were closed, even though it considers the fact that the wall painting were discovered in damaged condition in 1933.

Conservation of Waterlogged Wooden Finds Excavated in Wet-Site (저습지 출토 목재유물의 보존과 현황)

  • Yi, Yong Hee
    • Journal of Conservation Science
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    • v.6 no.2 s.8
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    • pp.126-140
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    • 1997
  • There were some cases in the past that waterlogged wooden finds were neglected and damaged severely because adequate methods of conservation processing could not be found. However, since a wooden ship unearthed in Anapji of Kyongju was processed by poly(ethylene glycol) (PEG) impregnation method in 1975, most of waterlogged wooden finds have been processed by diverse scientific methods. Most commonly-used conservation processing methods of waterlogged wooden finds in Korea are PEG impregnation method, alcohol-ether-resin method and vacuum freeze-drying method. New methods developed recently in Europe and Japan such as sucrose method, sugar-alcohol method and higher alcohol method are also being studied here. The most important task in conservation processing of waterlogged wood is to find good impregnation materials suitable to Korean climate and environments and develop their application methods. For efficient conservation processing, it is important to know the natures of finds and impregnation materials and relation between impregnation and drying condition. To achieve it, many experiments and studies are needed.

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An Examination of the Characteristics and Manufacturing Techniques of Joseon-era Metal Bullets (조선시대 금속제 탄환의 특징과 제작기법 검토)

  • Choi, Bo Bae;Lee, Hye Jin;Kim, Myung Hoon;Jeong, Hyeon Jin
    • Conservation Science in Museum
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    • v.28
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    • pp.65-88
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    • 2022
  • The characteristics and behavior of bullets are important because they are directly related to the firearm performance. However, research related to bullets have been small. In this paper, scientific analysis was conducted to find out the materials and manufacturing process of metal bullets during the Joseon Dynasty, owned by Korea Army Museum, and the types of firearms available were classified and organized according to the bullet diameter. As a result, bullets were classified into iron bullets, lead bullets, and lead-coated iron bullets. Most of the iron bullets and lead bullets were made from casting. Some iron bullets were made from forging. And the lead-coated iron bullet was made by pouring molten lead after putting the iron bullet into the mold. Finally, the bullets could be used for Hand Cannon, Matchlock Musket, Frankish Cannon, Hyeon-ja Cannon, Dae-Wiwon Cannon, Small Cannon, and Hong-Yi Cannon.