• Title/Summary/Keyword: 잔류특성

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Thermal Residual Stresses in the Frequency Selective Surface Embedded Composite Structures and Design of Frequency Selective Surface (주파수 선택적 투과막이 결합된 복합재료의 잔류응력평가 및 선택적 투과막 설계)

  • Kim, Ka-Yeon;Chun, Heoung-Jae;Kang, Kyung-Tak;Lee, Kyung-Won;Hong, Ic-Pyo;Lee, Myoung-Keon
    • Composites Research
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    • v.24 no.1
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    • pp.37-44
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    • 2011
  • In this paper, Particle Swarm Optimization(PSO) is applied to the design of the Frequency Selective Surface(FSS) and residual stresses of hybrid radome is predicted. An equivalent circuit model with Square Loops arrays was derived and then PSO was applied for acquiring the optimized geometrical parameters with proper resonant frequency. Residual stresses occur in the FSS embedded composite structures after cocuring and have a great influence on the strength of the FSS embedded composite structures. They also effect transmission quality because of delamination. Therefore, the thermal residual stresses of FSS embedded composite structures were analyzed using finite element analysis with considering the effects of FSS pattern, and composite stacking sequence.

Catalytic Pyrolysis of Waste Paper Cup Containing Coffee Residuals (커피 잔류물을 함유한 폐종이컵의 촉매 열분해)

  • Shin, Dongik;Jeong, Seokmin;Kim, Young-Min;Lee, Hyung Won;Park, Young-Kwon
    • Applied Chemistry for Engineering
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    • v.29 no.2
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    • pp.248-251
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    • 2018
  • Catalytic pyrolysis of the waste paper cup containing coffee residual (WPCCCR) was performed using a fixed bed reactor and pyrolyzer-gas chromatography/mass spectrometry (Py-GC/MS). Non-catalytic pyrolysis of WPCCCR produced a large amount of oil together with gas and char. The use of both HZSM-5 and HY decreased the yields of oil and increased the yield of gas due to the additional catalytic cracking. Owing to the acidic catalytic properties of HZSM-5 and HY, catalytic Py-GC/MS analysis of WPCCCR increased the selectivity to aromatic hydrocarbons in product oil. Owing to properties of HZSM-5 having a stronger acidity and medium pore size, the catalytic pyrolysis of WPCCR over HZSM-5 produced much larger amounts of aromatic hydrocarbons than that of using HY.

Evaluation of Residual Strength of CFRP Pressure Vessel After Low Velocity Impact (저속 충격 하중을 받은 탄소섬유강화 복합재 압력용기의 잔류강도 저하 평가)

  • Park, Jae-Beom;Kim, Dong-Ryun;Kim, Hyung-Geun;Hwang, Tae-Kyung
    • Composites Research
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    • v.21 no.3
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    • pp.9-17
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    • 2008
  • In this paper, the low velocity impact characteristics of filament winding CFRP pressure vessel was investigated using numerical and experimental methods. The cylinder part of CFRP vessel was impacted using triangular shape impactor which simulated the sharp edge of dropping tools and impact response behavior of CFRP was reviewed. The mechanical behavior, such as deformation and stress distribution, were also predicted by explicit finite element method and the validity of the model was investigated. For the quantitative evaluation of the residual strength of the pressure vessel after impact, a series of the ring specimens was cut from the impacted vessel and its burst pressure was measured by hydraulic pressure hoop tension test. As the results, the relationship between the residual strength degradation and the impact energy was successively obtained and a useful methodology to evaluate quantitatively the impact damage tolerance of CFRP pressure vessel was established.

Residual Characteristics of Insecticides Used for Oriental Tobacco Budworm Control of Paprika (파프리카 재배기간 중 담배나방 방제에 사용되는 살충제의 잔류특성)

  • Lee, Dong Yeol;Kim, Yeong Jin;Kim, Sang Gon;Kang, Kyu Young
    • Korean Journal of Environmental Agriculture
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    • v.32 no.1
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    • pp.84-93
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    • 2013
  • BACKGROUND: This study was carried out to investigate the residual characteristics of insecticides used for Oriental Tobacco Budworm control and to establish the recommended pre-harvest residue limit leading to contribution in safety of paprika production. METHODS AND RESULTS: The recommended Pre-Harvest Residue Limits (PHRLs) of insecticides during cultivation of paprika were calculated from residue analyses of insecticides in fruits 1, 3, 5, 7, 10, 12, 15, 18 and 21 days after treatment. Paprika samples were extracted with QuEChERS method and cleaned-up with amino propyl SPE cartridge and PSA, and insecticide residues were analyzed either by HPLC/DAD or GLC/ECD. The limits of detection were 0.01 mg/kg for 5 insecticides. Average recoveries were $81.3{\pm}1.62%$-$98.3{\pm}1.58%$ of 5 insecticides at fortification levels of 0.1 and 0.5 mg/kg. The biological half-lives of the insecticides were 8.5 days for bifenthrin, 11.8 days for chlorantraniliprole, 16.8 days for chlorfenapyr, 7.1 days for lamda-cyhalothrin and 31.3 days for methoxyfenozide at recommended dosage, respectively. CONCLUSION(S): The pre-harvest residue limits for 10 days before harvest were recommended 1.05 mg/kg, 1.41 mg/kg, 0.93 mg/kg, 2.06 mg/kg and 1.08 mg/kg as bifenthrin, chlorantraniliprole, chlorfenapyr, lamda-cyhalothrin and methoxyfenozide, respectively. This study can provide good practical measures to produce safe paprika fruit by prevention of products from exceeding of MRLs at pre-harvest stage.

Analysis of Interior Permanent Magnet Synchronous Machines using Thin Type Ferrite Magnet (고밀도화 페라이트 자석을 이용한 매입형 영구자석 동기기의 특성 해석)

  • Im, Young-Hun;Hwang, Seon-Ik;Jang, Seok-Myeong
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.858-859
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    • 2011
  • 고성능과 고효율 전동기인 매입형 영구자석 동기기에 사용되고 있는 희토류계 영구자석은 높은 가격과 수급 문제로 인해 최근 이슈화 되고 있다. 희토류계 영구자석을 대체하여 페라이트 영구자석을 적용할 수 있지만 낮은 잔류자속밀도로 인해 고출력을 얻을 수 없다는 문제점이 있다. 그러나 최근 높은 잔류자속밀도를 가진 고밀도화 페라이트 자석이 출시되면서 이를 적용한 매입형 영구자석 동기기의 특성을 해석할 필요성을 가지게 되었다. 본 논문에서는 고밀도화 페라이트 자석을 이용한 매입형 영구자석 동기기의 특성 해석을 하였다. 특히 영구자석의 재질 변경으로 인해 동기기의 토크와 토크 리플의 변화를 비교하고 코깅 토크에 의한 변화도 비교하였다. 또한 매입형 회전자내에 영구자석의 형상을 1층 및 3층으로 적용하여 구조에 따른 해석을 통해 특성을 비교함으로서 고밀도화 페라이트 자석의 효율적인 적용을 얻기 위한 회전자 구조를 선택하고자 한다. 또한 이를 통해 고밀도화 페라이트 자석의 적용 가능성을 예측하고자 한다.

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Crystalline and Electrical Properties of (Pb, La)TiO3 Ferroelectric Films ((Pb,La) TiO3 강유전체막의 결정성과 전기적특성)

  • 장호정
    • Journal of the Microelectronics and Packaging Society
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    • v.5 no.2
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    • pp.59-64
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    • 1998
  • Pt/SiO2/Si 기판구조위에 스크린인쇄법과 졸-겔법에 의해 (Pb, La)TiO3(PLT) 후막 과 박막을 도포시켜 $650^{\circ}C$후속열처리 온도에서 결정화한후 결정특성과 전기적 특성을 조사 하였다. $650^{\circ}C$ 온도에서 후속열처리된 PLT 시료의 경우 전형적인 perovskite 결정구조를 보 여주었다. SEM 단면형상으로부터 Pt 전극과 PLT막 사이에는 비교적 평활한 계면형상을 보여주었다. PLT 후막과 박막시료의 잔류분극(2Pr) 값은 약 1$\mu$C/cm2 으로각각 나타났으며 이와같이 후막 PLT시료에 비해 박막시료의 잔류분극값이 큰이유는 박막시료가 보다 양호 한 결정성을 지니기 때문이었다. 상온부근에서 후막과 박막시료의 초전계수값은 약 1.5nC/cm2.$^{\circ}C$와 4.0nC/cm2.$^{\circ}C$의 값을 각각 나타내었으며 누설전류의 크기는 약 0.3~0.8$\mu$ A/cm2의 비교적 양호한 누설전류 특성을 얻었다.

The Effects of Etch Chemicals on the Electrical Properties of Metal-Oxide-Semiconductor (MOS) Device with Plasma Enhanced Atomic Layer Deposited (PEALD) TiN Metal Electrode

  • Kim, Yeong-Jin;Han, Hun-Hui;Im, Dong-Hwan;Son, Seok-Gi;Sergeevich, Andrey;Choe, Chang-Hwan
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.11a
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    • pp.244-245
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    • 2015
  • PEALD TiN 금속 전극을 갖는 MOS device에서 SC1 ($NH_4/H_2O_2/H_2O=1:2:5$), SPM ($H_2SO_4/H_2O_2=10:1$), $H_2O_2$ etch chemical을 이용해 TiN 식각 후 oxide 표면 잔류 Ti에 의한 전기적 특성 분석을 진행 하였다. Etch chemical 중 SPM을 이용한 소자의 전기적 특성이 우수하였는데, 이는 잔류Ti atom의 양이 다른 etch chemical을 사용한 것 대비 낮았기 때문이다. 이로 인하여 낮은 leakage current, less frequency dependence의 특성이 관찰되었다. 또한, 후속 열처리를 통해 더욱 우수한 특성이 관찰 되었다. 이러한 공정기술은 single 전극을 갖는 CMOS 형성 시 사용 될 수 있을 것으로 기대된다.

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Ferroelectric Properties of Sol-Gel Derived pb(Zr,Ti)$\textrm{O}_3$Thin Films (SoI-Gel법에 의한 Pb(Zr, Ti)$\textrm{O}_3$박막의 강유전체 특성)

  • Go, Ga-Yeon;Lee, Eun-Gu;Park, Jin-Seong;Lee, Jong-Guk;Lee, U-Seon;Lee, Jae-Gap
    • Korean Journal of Materials Research
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    • v.7 no.6
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    • pp.479-483
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    • 1997
  • Sol-gel법으로 제작한 여러 종류의 Zr/Ti비율을 갖고 있는 PZT박막의 전지적 특성과 신뢰성 특성을 상부 백금 전극을 sputtering으로 증착하고 Ar 기체로 반응성 이온 식각(RIE)방법으로 패턴을 형성한 후 열처리온도의 변화에 따라 조사하였다. Hysteresis loop특성을 되찾게 하였다. Zr/Ti 비율이 감소함에 따라 voltage shift가 증가하였으며 internal field가 없어지는 열처리 온도가 증가하였다. Zr/Ti비율이 감소함에 따라 초기 잔류 분극은 증가하였으나 switching 횟수가 증가됨에 따라 잔류 분극이 급속히 감소하였다.

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A Study on the Polysilicon Etch Residue by XPS and SEM (XPS와 SEM을 이용한 폴리실리콘 표면에 형성된 잔류막에 대한 연구)

  • 김태형;이종완;최상준;이창원
    • Journal of the Korean Vacuum Society
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    • v.7 no.3
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    • pp.169-175
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    • 1998
  • The plasma etching of polysilicon was performed with the HBr/$Cl_2/He-O_2$ gas mixture. The residual layers after photoresist strip were investigated using x-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM). The etch residue was identified as silicon oxide deposited on the top of the patterned polysilicon. In order to clarify the formation mechanism of the etch residue, the effects of various gas mixtures such as $Cl_2/He-O_2$and HBr/$Cl_2$were investigated. We found that the etch residue is well formed in the presence of oxygen, suggesting that the etch residue is caused by the reaction of oxvgen and non-volatile silicon halide compounds. Wet cleaning and dry etch cleaning processes were applied to remove the polysilicon etch residue, which can affect the electrical characteristics and further device processes. XPS results show that the wet cleaning is suitable for the removal of the etch residue.

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Safety Evaluation of Pesticide Residue in Five Fruits by Dietary Risk Index (소비자 위해지수를 이용한 5종 과일 중 잔류농약 안전성평가)

  • Lee, Je Bong;Hong, Su-Myeong;Kwon, Hye-Young;You, Are-Sun;Hong, Soon-Sung;Ihm, Yangbin
    • The Korean Journal of Pesticide Science
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    • v.18 no.4
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    • pp.336-341
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    • 2014
  • In order to determine the residual characteristics of pesticides in fruits and their effects on human health, monitoring of pesticide residues were conducted in apples, peaches, pears, grapes and citrus from the major cultivation areas in 2010. Safeties of the pesticides detected from the fruits were evaluated using the amounts of pesticide residue detected and dietary risk index (DRI). Samples were taken from 4-5 major fruit cultivation areas and then pesticide residues in the test fruits were analyzed with a liquid chromatographymass spectrometry (LC-MS/MS). Mean residue levels of the pesticides in fruits were 0.001-0.144 mg/kg. The DRIs were 0.55 for apple, 0.066 for peach, 0.008 for pear, 0.025 for grape, and 0.37 for citrus, respectively. The results indicated that the amounts of pesticide residues in domestic fruits might be safe, considering the regulatory concerning level 1.0.