• Polymer(Korea)
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• v.24 no.4
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• pp.545-555
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• 2000

Surface defects in injection molded parts due to the unsteady flow are related to the dimension of gate, operational conditions and rheological properties of polymer. In this study we have examined surface defects in injection molding for PC, PBT and PC/ABS alloy with several injection speeds. We have used various cavity shapes that are tensile, flexural and impact test specimens with various gate and cavity thicknesses. Through this study we have observed that the formation of surface defect associated with jetting during filling stage in injection molding is strongly related to not on]v die swell but retardation of die swell. Large die swell eliminates jetting however the large retardation of die swell stimulates jetting. Reducing the thickness ratio of cavity to gate can reduce or eliminate jetting and surface defects. It also enlarges process window that can produce steady flow of polymer melt in injection molding.

• Composites Research
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• v.18 no.6
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• pp.26-33
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• 2005

The mechanical properties of composite materials may severely degrade in the presence of damage. Especially, the high-velocity impact such as bird strike, a hailstorm, and a small piece of tire or stone during high taxing, can cause considerable damage to the structures and sub-system in spite of a very small mass. However, it is not easy to detect the damage in composite plates using a single technique or any conventional methods. In this paper, the PVDF(polyvinylidene fluoride) film sensors were used for monitoring high-velocity impact damage initiation and propagation in composite laminates. The WT(wavelet transform) and STFT(short time Fourier transform) are used to decompose the sensor signals. A ultrasonic C-scan and a digital microscope are also used to examine the extent of the damage in each case. This research shows how various sensing techniques, PVDF sensor in particular, can be used to characterize high-velocity impact damage in advanced composite.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.36 no.9
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• pp.841-850
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• 2008

Strength and failure of composite-to-aluminum rivetted, bonded, and rivet/bonding hybrid single-lap joints were investigated by experiment. A total of 82 joint specimens were tested with 3 different overlap lengths and 2 types of stacking sequence. FM73m adhesive film and NAS9308-4-03 rivet were used for hybrid joints. While failure loads of the bonded and hybrid joints increased as the overlap length increased, failure loads of the rivetted joints were not affected by the overlap length. Effect of the stacking sequence was not remarkable in the simple bonded or rivetted joints. Failure loads of the hybrid joints, however, showed the maximum of 30% difference depending on the stacking sequence. Major failure mode of the bonded and hybrid joints was the delamination of the composite adherend and failure mode of riveted joints was the rivet failure with local bearing.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2001.11a
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• pp.22-22
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• 2001

전통적으로 초경합금은 무라까미 용액에서 에칭하거나 묽은 염산에 넣고 끓이는 방법에 의해 그 밋구조를 관찰하였다. 그러나 carbide 입자가 suvmicron 크기인 초경합금에서는 전통적인 에칭 방법으 에칭 후에도 입자/기지상, 입자/입자 입계를 동시에 구분시킬 수 있는 SEM 사진을 얻을 수 없다. 본 연구에서는 submicron 크기 초경합금의 고배율 SEM 사진을 얻을 수있는 90H2O2 - 10HNO3 (vol%)의 새로운 에칭 용액을 개발하였다. 경명의 submicron 크기 WC-Co 시편을 샐운 에칭 용액인 90H2O2 - 10HNO3 (vol%)에 넣고 약 6$0^{\circ}C$에서 약 12분 동안 에칭하였다. 에칭에 의해 Co 기지상은 빠르게 제기(dissolution)되었고, 동시에 표면의 WC 입자들은 각각의 결정학적 방향에 따라 천천히(slowly) 다른 속도로 부식(sissolution)되었다. 고배율 SEM을 관찰한 결과 WC/기지상 계면과 WC/WC 입계가 명화갛게 관찰되었다. WC 입자의 성장을 억제시키는입자성장 억제제(Cr3C2, TaC,VC)가 첨가된 WC Co 초경합금을 새로운 에칭 용액인 90H2O2 - 10HNO3 (vol%)에 넣고 약 6$0^{\circ}C$에서 약 12분동안 에칭하였다. 매우 작은 입자를 갖는 미세구조임에도 불구하고 고배율 SEM에서 WC/기지상 계면과 WC/WC 입계가 명확하게 관찰되었다. 90H2O2 - 10HNO3 (vol%)에서 Co 기지상이 빠르게 제거되는 것은 산 (acid)인 HNO3)에서 금속인 Co가 쉽게 녹기 때문이다. 동시에 WC 입자들이 각각 다른 속도로 에칭 된 것은 강력한 산화제인 H2O2가 각각의 WC입자 표면에 얇은 텅스텐 산화물 층을 형성시켰고 이들이 산인 HNO3에서 녹았기 때문이다. 본 연구에서 개발된 새로운 에칭 용액인 90H2O2 - 10HNO3 (vol%)의 에칭 원리가 똑같이 적용 가능한 다른 종류의 초경 합금에서도 사용이 가능할 것으로 판단된다.로 판단된다.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.11a
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• pp.753-756
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• 2008

HPFRCC (High-Performance Fiber Reinforced Cementitious Composites), which is relatively more ductile and has the characteristic of high toughness with high fiber volume fractions, can be used in structures subjected to extreme loads and exposed to durability problems. In the case of using PVA(polyvinyl alcohol) fibers, it is noted by former studies that around 2% fiber volume fractions contributes to the most effective performance at HPFRCC. In this study, therefore, compressive and flexural tests were implemented to evaluate the compressive and flexural capacities of HPFRCC while the total fiber volume fractions was fixed at 2% and two different PVA fibers were used with variable fiber volume fractions to control the micro-crack and macro-crack with short and long fibers, respectively. Moreover, specimens reinforced with steel and PVA fiber simultaneously were also tested to estimate their behavior and finally find out the optimized mixture. In the result of these experiments, the specimen consists of 1.6% short fibers (REC 15) and 0.4% long fiber (RF4000) outperformed other specimens. When a little steel fibers added to the mixture with 2% PVA fibers, the flexural capacity was increased, however, when high steel fiber volume fractions applied, the flexural capacity was decreased.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.2
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• pp.160-164
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• 2013

A laser ultrasonic inspection system is a non-contact inspection device which generates and measures ultrasonics by using laser beam. A laser ultrasonic inspection system provides a high measurement resolution because the ultrasonic signal generated by a pulse laser beam has a wide-band spectrum and the ultrasonic signal is measured from a small focused spot of a measuring laser beam. In this study, galvanic corrosion phenomenon was measured by non-destructive and non-contact method using the laser. The case of mixed foreign material on the part of corrosion was assumed and laser ultrasonic experiment was conducted. Ultrasonic was generated by pulse laser from the back side of the specimen and ultrasonic signal was acquired from the same location of the front side using continuous wave laser and Confocal Fabry-Perot Interferometer(CFPI). The characteristic of the ultrasonic signal of exist foreign material part was analyzed and the location and size of foreign material was measured.

• Journal of the Korean Ceramic Society
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• v.41 no.3
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• pp.202-209
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• 2004

Hydroxyapatite(HA)/TiO$_2$ composite powders were prepared by mixing of spherical TiO$_2$ (10-15 nm, 500 nm) and needle-shaped HA (50-70 nm, 120-250 nm) powders which had been synthesized through precipitation, sol-gel and hydrothermal methods. From the three types of starting composite powders (HA/TiO$_2$ wt% of 75/25, 50/50, and 25/75), dense $\beta$-TCP/TiO$_2$ composites were prepared by hot-pressing at 800-100$0^{\circ}C$ for 30 min under the pressure of 30 ㎫ in Af atmosphere. The $\beta$-TCP/TiO$_2$ composites showed different microstructures and sintering densities depending on their powder morphology, composition and sintering temperature. With increasing the sintering temperature and the content of TiO$_2$, sintered density was increased and microstructure became more homogeneous.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2017.05a
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• pp.98.1-98.1
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• 2017

본 연구에서는 정전류 조건에서 알루미늄 합금의 PEO(Plasma Electrolytic Oxidation) 피막 형성 거동에 대한 전해질 조성의 영향을 아크 발생 양상, 전압-시간 곡선 및 형성된 표면피막의 구조를 관찰하여 연구하였다. 실험에 사용된 전해질은 NaOH 수용액에 $Na_2SiO_3$을 혼합하여 구성되었으며, NaOH와 $Na_2SiO_3$의 농도는 각각 0.01 ~ 1.0 M 와 0 ~ 2.0 M 사이로 조절되었다. 0.01 M NaOH 이하의 용액에서는 양극전압이 500 V 이상으로 상승되고 미세한 아크가 시편 표면 전체에 발생했으나, 0.02 M NaOH 이상의 농도에서는 양극전압이 300 V 이하로 감소되었고 아크발생이 관찰되지 않았다. 아크발생이 일어나지 않는 고농도의 0.5 M NaOH 용액의 경우 0.1 M 이상의 $Na_2SiO_3$를 첨가하였을 때 작은 아크의 무리가 발생되었다. 0.5 M NaOH 수용액에 0.1 M ~ 0.2 M $Na_2SiO_3$가 첨가되었을 땐 아크 무리가 발생하나 이내 일부 영역에서만 반복적으로 아크가 발생하는 로컬 버닝 현상이 일어났다. 한편 0.5 M NaOH 수용액에 0.5 M 이상의 $Na_2SiO_3$가 첨가되었을 때는 로컬 버닝이 일어나지 않고 전 표면에 걸쳐서 아크 무리가 이동하며 PEO 피막이 형성되었다. 0.01 M NaOH 수용액에서 형성된 PEO 피막의 두께는 처리 시간에 따라 증가하지 않고 $10{\mu}m$ 이하의 낮은 값을 보였다. 반면에 NaOH와 $Na_2SiO_3$ 혼합수용액에서 형성된 피막의 두께는 약 $30{\mu}m$ 이상의 높은 값을 보였다.

• Composites Research
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• v.14 no.2
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• pp.22-32
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• 2001

Damage induced by low-velocity impact on the curved composite laminates was experimentally evaluated for CFRP cylindrical shells with the radius of curvatures of 50, 150, 300, and 500 mm. The result was then compared with that of flat laminates and with the results by nonlinear finite-element analysis. The radius of curvatures and the effective shell stiffness appeared to considerably affect the dynamic impact response of curved shells. Under the same impact energy level, the maximum contact force increased with the decreasing radius of curvatures, with reaching 1.5 times that for plates at the radius of curvature of 50 mm. Since the maximum contact farce is directly related to the impact damage, curved laminates can be more susceptible to delamination and less resistant to the low-velocity impact damage. Delamination was distributed rather evenly at each interface along the thickness direction of curved laminates on the contrary to the case of flat laminates, where delamination is typically concentrated at the interfaces away from the impact point. This implies that the effect of curvatures has to be considered for the design of a curved composite laminate.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.1
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• pp.40-45
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• 2013

The purpose of this study was to detect the pin hole defect of dental composite restoration using lock-in thermography method. Amplitude and phase images of the composite resin specimens were analyzed according to the lock-in frequency and the diameter of defect area. Through the amplitude image analysis, at lock-in frequency of 0.05 Hz, defect diameters 2-5 mm exhibited the highest amplitude contrast value between defective area and sound area. The lock-in frequency range of 0.3-0.5 Hz provided good phase angle contrast for the defect area. At lock-in frequency range of 0.5 Hz, defect diameter of 5 mm exhibited the highest phase contrast value. It is concluded that the infrared lock-in thermography method verified the effectiveness for detecting the pin hole defect of dental composite restoration.