• Proceedings of the Korea Crystallographic Association Conference
• /
• 2003.05a
• /
• pp.9-9
• /
• 2003

최근에 Fe-CU, Fe-Si 등과 같이 자성금속과 비자성금속화합물에 대한 연구가 활발히 진행되고 있다. 본 연구에서는 기계적 합금법으로 제작한 Co/sub 5/C/sub 95/ 나노미립상 합금의 구조와 자기적 성질을 조사하였다. 그림(1)은 EXAFS 스펙트럼의 푸리에변환이다. 이로부터 합금화시간에 따라 Co-Co 결합은 점차적으로 작아지며 Co-C 결합이 진행됨에 알수 있다. 그림(2)은 합금화시간에 따른 포화자화값과 보자력의 크기이다. 포화자화는 합금화 시간에 따라 연속적으로 작아졌으며 보자력은 커지다가 작아지는 경향을 보였다. 포화자화가 작아지는 것은 Co-C 결합이 생기면서 Co의 쌍을 이루지 않은 전자가 C의 전자와 쌍을 이루면서 상쇄되기 때문인 것으로 보인다. 보자력의 거동은 Co 미립자가 다자구영역으로부터 단자구영역으로 전환되기 때문인 것으로 해석될수 있다. Co 미립자는 C의 캡슐형에 싸여있으며 60시간과 100시간에서 Co 미립자의 크기는 X-ray 회절선의 넓어짐으로부터 Scherrerr 공식을 이용하여 계산한 결과 18nm 와 15nm 정도가 됨을 알 수 있었다. 연구를 통하여 Co/sub 5/C/sub 95/ 나노미립상합금을 기계적합금법으로 만들 수 있음을 알 수 있었다. 이론적인 계산에 의하면 초상자성 Co 입자의 크기는 8.2nm 정도가 되었으며 본 실험에서 최종 입자의 크기는 15nm까지 작아졌다.

• Journal of the Korean Magnetics Society
• /
• v.9 no.4
• /
• pp.173-176
• /
• 1999

Errors of saturation magnetization and magnetocrystalline anisotropy constant determined by magnetization curve of magnetically aligned unixial power were analyzed. In case of alignment factor ${\Theta}_0=10{\circ}$, magnetic constant errors of $Nd_2Fe_{14}B$ were calculated to be error of $M_S{\risingdotseq}1{\%}\;and\;error\;of\;K_1{\risingdotseq}13\;{\%}$, respectively, and magnetic constant errors of Ba-ferrite were calculated to be error of $M_S{\risingdotseq}1{\%}\;and\;error\;of\;K_1{\risingdotseq}17\;{\%}$. In this method, $M_s$ was found to be determined with high accuracy. High alignment is desirable for high accuracy.

• Proceedings of the Korean Magnestics Society Conference
• /
• 1996.10a
• /
• pp.92-93
• /
• 1996

• Journal of the Mineralogical Society of Korea
• /
• v.24 no.1
• /
• pp.31-36
• /
• 2011

Meteorites are extraterrestrial solid rock fragments that fell from the outer space. Investigating mineral magnetic properties of the Meteorites is essential in understanding the evolution of planets and asteroids in the Solar System. In particular, magnetic characterization of magnetic mineral can provide constraints on the progress of differentiation in ancient planetary bodies. In the present study, ratio of thermoremanent magnetization (TRM) over saturation isothermal remanent magnetization (SIRM) was applied to diagnose the magnetic minerals in meteorites and igneous rocks. Distinctive classification of TRM/SIRM suggests that kamacite, tetrataenite, magnetite, and (Cr,Ti)-rich iron oxide are responsible for the magnetization of H5 Richardton, LL6 St. Severin, ALH84001, and DaG476, respectively. The TRM/SIRM ratio could be an efficient tool in identifying magnetic minerals especially when rocks or meteorites contain unstable material under heating.

• Journal of the Korean Magnetics Society
• /
• v.7 no.4
• /
• pp.191-195
• /
• 1997

$Co_{84}Hf_{16}$ (1300$\AA$, 2150$\AA$) thin films were prepared by dc magnetron sputtering method. To investigate the uniaxial anisotrpy of the sample, the saturation and effective magnetization of the thin films were measured by VSM and FMR, respectively. The spectroscopic splitting g factor were estimated from the ferromagnetic resonance curves. For 1300$\AA$, 2150$\AA$, the effective magnetization was measured at the temperatures from T=77K to T=300K. The results were analyzed in terms of Bloch's law $M_s(T)=M_s(0)(1BT^{3/2}CT^{5/2}$. The Bloch coefficient B and C were determined by fitting. $M_{eff}(0)$ was obtained by extrapolating $M_{eff}$ to 0 K. From this result, the spinwave stiffness constants D was also determined and the exchange stiffness constants $A_{eff}$ were calculated by Kittel's resonance conditions.

• Journal of the Korean Magnetics Society
• /
• v.6 no.4
• /
• pp.199-203
• /
• 1996

To study the magnetization reversal behavior of Co/Pd multilayers, we first demagnetized the samples by the field-demagnetized method and then measured initial curves and minor loops. The coercivity and the perpendicular magnetic anisotropy were obtained from the perpendicular and parallel magnetization curves measured at different temperatures. We interpret our experimental results by applying several qualitative and semiquantative approaches. From these study, we found that the magnetization reversal behavior is dominated by the domain wall pinning for all samples and the coercivity incremental tendency can be explained by Kronmuller's formula $H_c(T)\;{\propto}\;r_0.K_u$.

• Progress in Medical Physics
• /
• v.19 no.4
• /
• pp.269-275
• /
• 2008

Although MR imaging is generally applicable to depict knee joint deterioration it, is sometimes occurred to mis-read and mis-diagnose the common knee joint diseases. In this study, we employed magnetization transfer ratio (MTR) method to improve the diagnosis of the various knee joint diseases. Spin-echo (SE) T2-weighted images (TR/TE 3,400-3,500/90-100 ms) were obtained in seven cases of knee joint deterioration, FSE T2-weighted images (TR/TE 4,500-5,000/100-108 ms) were obtained in seven cases of knee joint deterioration, gradient-echo (GRE) T2-weighted images (TR/TE 9/4.56/$50^{\circ}$ flip angle, NEX 1) were obtained in 3 cases of knee joint deterioration, In six cases of knee joint deterioration, fat suppression was performed using a T2-weighted short T1/tau inverse recovery (STIR) sequence (TR/TE =2,894-3,215 ms/70 ms, NEX 3, ETL 9). Calculation of MTR for individual pixels was performed on registration of unsaturated and saturated images. After processing to make MTR images, the images were displayed in gray color. For improving diagnosis, three-dimensional isotropic volume images, the MR tristimulus color mapping and the MTR map was employed. MTR images showed diagnostic images quality to assess the patients' pathologies. The intensity difference between MTR images and conventional MRI was seen on the color bar. The profile graph on MTR imaging effect showed a quantitative measure of the relative decrease in signal intensity due to the MT pulse. To diagnose the pathologies of the knee joint, the profile graph data was shown on the image as a small cross. The present study indicated that MTR images in the knee joint were feasible. Investigation of physical change on MTR imaging enables to provide us more insight in the physical and technical basis of MTR imaging. MTR images could be useful for rapid assessment of diseases that we examine unambiguous contrast in MT images of knee disorder patients.

• Korean Journal of Materials Research
• /
• v.6 no.10
• /
• pp.1043.2-1048
• /
• 1996

자기기록의 고밀도화로 인해 보자력(Hc)이 큰 자기기록매체가 필요하게 되었다. 고보자력매체에 신호를 충분히 기록하기 위해서는 보다 강한 자장이 필요하다. 이 때문에 포화자화(Ms)가 큰 재료가 필요하며 고주파 영역에서 실효투자율($\mu$eff)이 높아야 한다. Fe계 합금박막은 이에 적합한 재료이다. 본 연구에서는 Fe의 결정자기이방성에 영향을 미치는 Si과 Fe의 격자 변형을 유도할 수 있는 B를 첨가하였다. Fe-B-Si 계 박막을 질소분위기 중에서 RF Matnetron Sputter로 제작하여 연자기적 특성에 관하여 고찰하였다. Fe91.49B4.01Si4.50at% 박막은 35$0^{\circ}C$에서 1시간 열처리를 행함으로써 약 900(10MHz) 정도의 투자율과 7.6Oe의 보자력을 나타냈으며 포화자화는 1300emu/㎤를 얻었다.

• Electronics and Telecommunications Trends
• /
• v.18 no.6 s.84
• /
• pp.41-48
• /
• 2003

본 논문은 아이솔레이터의 소재 파라미터에 의한 삽입손실 영향에 대하여 서술하였다. 본 논문에서는 페리자성공명반치폭($\Delta$Η), 유전손실, 자계세기 그리고 포화자화에 대한 아이솔레이터 삽입손실의 관계를 알아 보았고, 또한 공진 아래 모드를 사용한 아이솔레이터의 온도안정화 연구 및 구조설계에 대하여알아 보았다. 아이솔레이터의 온도특성은 영구자석, YIG(Yttium Iron Garnet) 페라이트 그리고 공진기로사용되는 도체 등에 의한 변화에 대하여 본 논문에서는 실험시제품을 제작하여 측정 분석하였다. 측정결과 시뮬레이션 결과와 실험시제품 측정결과가 거의 일치하는 것을 알 수 있었다. 삽입손실 0.18~0.24dB, 반사손실 27dB, 아이솔레이션 27dB 그리고 대역폭 500MHz를 얻을 수 있었다. 이때 실험에 사용한 소재 파라미터는 포화자화 550G, 유전손실, $0.0004\Delta$Η20, 유전율 14로 하였다. 또한 온도안정화실험에서는 구조를 개선하여 온도안정화를 이루었다.

• Proceedings of the Korean Magnestics Society Conference
• /
• 1992.03a
• /
• pp.34-35
• /
• 1992