• Journal of the Korean Magnetics Society
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• v.2 no.1
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• pp.44-49
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• 1992

Magnetic properties and microstructures of $Nd_{12}Fe_{80}B_{6}(Nb,\;M)$ (M=Ti/Cu/Ga) melt-spun ribbons prepared by single wheel technique have been studied. The results of microstructural study have shown that Ga is effective for the orientation of c-axis normal to the ribbon plane. The Ga-added melt-spun ribbon, $Nd_{12}Fe_{80}B_{6}(Nb,\;Ga)$, quenched at $V_{s}=17.9\;m/s$ was mostly composed of fine grains of about 30 nm in size with the textured free-side surface. The powder of this ribbon aligned in mag-netic field showd a high remanence of 0.87 T which was about 5 % higher than that of ribbon itself. It is believed that there is a possibility to fabricate a new type of HIREM melt-spun ribbon with highly textured free-side surface.

• Journal of the Korean Society of Food Science and Nutrition
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• v.30 no.4
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• pp.617-622
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• 2001

Changes of quality properties of fermented tofu prepared with two molds like Actinomucor elegans (AE) and Rhizopus oligosporus (RO) and coagulants (CaCl$_2$ and citric acid) were investigated. Moisture and crude protein of fermented tofu were rapidly decreased during fermentation, the contents of crude lipid and crude ash were shown to be slightly increased, ad then total acidity was slowly decreased. The content of reducing sugar of fermented tofu was slowly increased for 7 day of fermentation, but rapidly increased after that time because of rapid hydrolysis of carbohydrate in fermented tofu. The contents of amino and ammonia type nitrogen were quickly increased during fermentation. The highest contents of amino type nitrogen of fermented tofu were found in sample of CaCl$_2$group as a coagulant and RO group as a mold. Contents of minerals in tofu fermented for 14 day were high in order of K>Ca>Mg>Na. Iin conclusion, AE was more effective than RO to enhance the contents of reducing sugar and amino type nitrogen as an indicator of fermentation within 7 day of fermentation, and then RO was more effective than AE after that time. Calcium chloride as a coagulant was more effective than citric acid in tofu fermented with the same strain for 14 day.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.13 no.8
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• pp.3537-3543
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• 2012

Therefore, to establish optimal condition and composition with magnesium chloride emulsion as coagulant, this study compared its properties by the usage of 60%(w/w) magnesium chloride solution, lastly measured the characteristics of soybean curd coagulation, coagulation time, state of texture, and water separation ratio with using emulsion as coagulant. After all the experiments, when manufacturing magnesium chloride emulsion with using 70% of quantity of 60%(w/w) magnesium chloride solution, it had the best result as coagulant according to the state of texture and the water separation ratio of soybean curd.

• Korean Journal of Metals and Materials
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• v.47 no.7
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• pp.440-446
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• 2009

Co base superalloys have been widely used for the parts of gas turbine due to their excellent strength, thermal fatigue, oxidation resistance and weldability at high temperature. In this study, directional solidifications were carried out at various solidification rates, including $0.5{\sim}300{\mu}m/s$ in the Co base superalloy FSX-414. The cellular interface were formed at a low solidification rate, $1{\mu}m/s$, and the dendritic interface was found at higher solidification rates, $5{\sim}300{\mu}m/s$. As the spacing of dendrite structure decreased, the size and spacing of eutectics decreased. Dendrite arm spacing decreased with increasing solidification rates and temperature gradient. It was interesting to find the $M_{23}C_{6}$ eutectic microstructure formed between $\gamma$ dendrites. Composition analysis showed that Cr and W were segregated severely between the dendrites, which resulted in the formation of Cr-rich $M_{23}C_{6}$ and W-rich MC carbides.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.8 no.1
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• pp.1-9
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• 1998

In this study, we have investigated the preparation conditions of 45$\times$45$\times$20(mm) square cross-section sapphire single crystal by the modified heat exchanger method using water as a coolant. Melting and solidification processes were optimized by the systematic change of the chamber pressure with the heater temperature. As a results, solidification temperature was between 1960 and $1970^{\circ}C$. The crucible was formed by handling. Therefore its shape should had the 'spiral type' ear at edge of its side. Heat exchanger affected to the temperature distribution and gradient of molten alumina. Heat flux and unmelted seed were controlled by volume of heat exchanger. Voids were controlled by the cooling rate of the heater below $0.2^{\circ}C$/min.

• Korean Journal of Materials Research
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• v.8 no.5
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• pp.436-443
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• 1998

2.3%C-26%Cr-1%Ni-0.5%Mo 조성의 다합금계 고크롬백주철을 고주파유도용해로를 사용하여 주조한 후 응고조직, 열처리조직 및 기계적성질간의 상관관계를 연구하였다. 주방상태에서는 초정덴드라이트조직인 기지조직과 공정탄화물로 구성되어 있었으며 기지조직의 73%가 오스테나이트, 27%가 마르텐사이트조직이었다. $900^{\circ}C$에서 5시간동안 균질화열처리만 행한 시편의 경우, 기지조직은 거의 페라이트로 구성되어 있었으며 $1100^{\circ}C$에서 불안정화열처리후 강제공냉시킨 시편의 경우, 유지시간에 따라 기지조직내의 잔류오스테나이트함량은 48.9-57.6%의 범위에 놓여 있었다. 주방상태 및 열처리시편 공히 마모량과 마모시간과의 관계가 직선적으로 얻어 졌는바 마모속도는 $2.77x10^{-2}$ /$~4.12x10^{-2mg}$ /sec의 범위에 걸쳐 있었다. 주방상태의 시편이 내마모성이 가장 우수하였으며 균질화열처리만 행한 시편이 가장 열악하였다. 기지조직내 잔류오스테나이트함량의 비율이 높아짐에 따라 경도는 감소하였고 반면에 내마모성은 향상되었다. 이는 마찰마모시험시 접촉부위의 오스테나이트가 가공경화를 일으켜 마르텐사이트로 변태되었기 때문으로 사려된다.

• Korean Journal of Materials Research
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• v.14 no.2
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• pp.101-109
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• 2004

The influences of solidification rates and carbon contents on the formation of the $\delta$-ferrite were studied by directional solidification in modified 12%Cr-l %Mo steels. Directional solidification experimental results showed that solidification microstructure depended on solidification rate and carbon content and chromium equivalent. The length of the mushy zone increased and the dendrite arm spacings decreased as the solidification rate increased. The volume fraction of the 8-ferrite decreased with increasing the solidification rate and carbon content. The volume fraction of the ferrite showed much higher at low solidification rates with planar and cellular interfaces than that at high solidification rates with dendritic interface. It is expected that macro-segregation of C causes lower C content at the lower solidification fraction in the directionally solidified sample, where lower C results in higher volume fraction of the ferrite. In order to estimate solidification microstructure in modified 12Cr-l%Mo steels, various solidification conditions, such as solidification rate, cooling rate, segregation, alloy composition, should be considered.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.4 no.3
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• pp.276-283
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• 1994

The dislocation configuration in web-grown silicon ribbon was investigated using chemical etching techniques. The presence of dislocation loops on twin planes is observed and acounted for by self-interstitial condensation. The interstitials were either quenched in, due to the rapid cooling of the ribbon from the solidification temperatures, or produced by oxide precipitation on the twin plane. Very large faulted loops of mm size were also observed.

• Journal of Powder Materials
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• v.11 no.3
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• pp.193-201
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• 2004

1960년 Au-Si계 합금에서 처음으로 비정질상이 급속 응고법에 의해 보고된 이래/sup 1)/ 지난 40년 간 많은 합금계에서 비정질상이 보고되어졌다. 대표적으로 Fe-, Ni-, Co기 합금 등 많은 합금계에서 비정질상이 보고되었으나, 비정질상의 형성을 위해서는 약 105 K/s이상의 높은 냉각속도를 필요로 하였다. 1980년대 수백 K/s의 낮은 냉각속도 하에서도 비정질상이 형성될 수 있는 다원계 합금(multi-component alloy)이 Mg-Ln-(Ni, Cu, Zn), Ln-Al-TM 합금에서 보고되어 졌으나 많은 관심을 받지 못하다가 1993년 Zr-Ti-Ni-Cu-Be 합금에서 수 ㎝ 크기의 비정질합금 제조가 보고되면서 전 세계적으로 많은 관심을 받게 되었다. Zr-Ti-Ni-Cu-Be계 벌크 비정질 합금이 보고된 후 Zr-(Nb,Pd)-Al-TM, Pd-Cu-Ni-P, Fe-Co-Zr-Mo-W-B, Ti-Zr-Ni-Cu-Sn등 여러 합금계에서 벌크 비정질 합금이 보고되었다. (중략)

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.17 no.2
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• pp.85-91
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• 1981

An equation was derived which describes the slip force that occurs at the casting of initial state due to unequilibrium with support bar weight, liquid metal, casting velocity, thickness, control roller, hydraulic motor and etc. The slip force equations are solved on the basis of velocity, gravity and thickness in casting ingot. In this paper the auther assumed that the other mechanisms are normal. The behaviour of slip force in many characteristics is calculated as a function of velocity, gravity and thickness with variation. The conclusion with this phenomena is reached that the present theory realistically predicts the growth of slip force in a flat plate ingot continuous casting machine.