• Title/Summary/Keyword: 유약

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Analysis of Pottery Sherds from Wonnae-dong, Daejeon and Yucheon-ri, Buan (대전 원내동과 부안 유천리 도자기의 분석)

  • Kang, Hyunsam;Lee, Hanhyoung;Park, Kicheol;Kim, Kunhan;Suh, Mancheol;Seo, Jungho;Choi, Ki-Young
    • Journal of Conservation Science
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    • v.12 no.1 s.15
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    • pp.48-70
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    • 2003
  • The characterization of chemical properties and analogy of mallufactured origin for the nine potsherds and eleven celadon sherds collected in Wonnae-dong, Daejeon and Yucheon-ri, Buan, respectively were performed by analyzing their body and glaze compositions and compared with previous data reported. The chemical compositions of the body and glaze were determined by XRF and EPMA, respectively. The trace elements of the body were analyzed by ICP-MS. The Seger analysis and principal components analysis were used to compare the major compositions of body and glaze of the potteries we found with previous data. Wonnae-dong's Whiteware (C-1) showed considerably high $SiO_2$ concentration differently from the other potteries. Wonnae-dong's Whiteware (C-2) showed similar characteristics with potteries of Seoul-Kyeongi and Daejeon-Chungnam provinces in chemical compositions of the body and the glaze. Wonnae-dong's celadons (B-1 and B-2) were classified as the group of Daejeon, Chungman provincial potteries in chemical compositions of the body. It was difficult to distinguish the characteristic differences in the Buncheong data between the provinces with the Seger formula analysis and the PCA. Celadon from Yucheon-ri site showed the same characteristics with previous data reported. The results above demonstrated that it is reasonable to study the characterization of potteries and analogy of manufactured origin with a comparison for the chemical compositions of the body and the glaze of the potteries by using the Seger formula analysis and the PCA.

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Pyriproxyfen Inhibits Hemocytic Phagocytosis of the Beet Armyworm, Spodoptera exigua (파밤나방(Spodoptera exigua)의 혈구세포 식균반응에 대한 피리프록시펜의 억제효과 Nalini Madanagopal)

  • Madanagopal, Nalini;Lee, Yong-Joon;Kim, Yong-Gyun
    • The Korean Journal of Pesticide Science
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    • v.11 no.3
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    • pp.164-170
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    • 2007
  • The concept of innate immunity in insects which refers to the first line of host defense constitutes the humoral and cellular components which are involved in recognition and actively participate in the elimination of the intruding foreign micro- or macro-organisms. Several recent studies suggest that juvenile hormone (JH) modulates the cellular immune reactions in response to pathogen. In this study, pyriproxyfen (a JH agonist as an insect growth regulator) was tested in its any inhibitory effect on the immune reactions of the beet armyworm, Spodoptera exigua. To this end, five different hemocyte morphotypes of final instar S. exigua were identified by phase contrast microscopy. Plasmatocytes and granular cells, which constitute about 90% of the total hemocyte count, were prominently distinguished based on their basophilic/acidophilic nature using Giemsa stain. The role of pyriproxyfen on the functional ability of hemocytes was analyzed using FITC-labeled Providencia vermicola for the phagocytic potential of the hemocytes. Both granular cells and plasmatocytes exhibited phagocytosis behavior. Pyriproxyfen significantly inhibited the phagocytosis of both cell types, proposing its novel action as an immunosuppressant.

Scientific Study of Punch'ong and Whiteware from Ch'unghyodong Kwangju (I). Analysis of Chemical Compositon (광주 충효동 분청과 백자의 과학기술적 연구 (Ⅰ). 성분분석을 중심으로)

  • Lee, Young Eun;Koh, Kyong Shin
    • Journal of the Korean Chemical Society
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    • v.42 no.3
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    • pp.251-265
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    • 1998
  • Punch'ong and whiteware sherds excavated from four kilns located in Ch'unghyodong, Kwangju, Chollanamdo were analyzed for their body and glaze composition. They are classified into eight different groups by the site and layer from which they were collected. In principal component analysis of major composition, the punch'ong body separates out into several different groups. CHE2, made in early fifteenth century, has a higher aluminum and lower iron content compared to the later groups of lower grade. Whiteware body has a very high aluminum content of around 30 wt. in both soft type and hard type. Punch'ong glaze was determined to be lime type and whiteware alkali-lime type.

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Synthesis of wagnerite and its analogues for ceramic pigments (ll) (도자기 유약용 Wagnerite의 합성(II))

  • Yong- Sun Chung;Keun Ho Auh
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.4
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    • pp.648-657
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    • 1997
  • In order to investigate the polymorphism of wagnerite, the single phase of$Mg_3(PO_4)_2$ was synthesized by heating the stoichiometric mixture of $Mg_3(PO_4)_2$ and $MgF_2$ in a sealed platinum tube at $1040^{\circ}C$ (or 3 hours, One reversible inversion was detected at $1255^{\circ}C$ and the thermal decomposition was not observed until it reached the melting point. As a result, wagnerite is thermally stable enough to be used as pigments for glazes and plastics if substituted with divalent metal ions. The contractions of d-values in $Zn_4P_2O_8F_2$ and $Zn_3MgP_2O_8F_2$ phases were observed by the substitution with metal ions which resulted in intense purple, gold and green colors. Among the several attempts of charge - coupled sub-stitution, only $A^{1+}A_3^{2+}X^{5+}X^{6+}O_8_F2$ compositions were successful to synthesize the wagnerite phase.

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Composition and Microstructure of Punch'ong Sherds from Bokwang-ri, Kangnung (강릉 보광리 분청도편의 성분과 미세구조 연구)

  • Kim, Kyung-nam;Han, Sang-mok;Shin, Dae-yong
    • Journal of Conservation Science
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    • v.8 no.1 s.11
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    • pp.10-15
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    • 1999
  • The chemical compositions and microstructure of the punch'ong excavated from Bokwangri, Kangnung were investigated by the scanning electron microscope (SEM) with an energy dispersive X-ray spectrometer (EDS), X-ray diffractometer (XRD), and dilatometer. The compositions of body were $SiO_2(73-78\%),\;Al_2O_3(13-16\%)$, $RO{\cdot}R_2O(4-5\%,\;R=Ca,\;Mg,\;Na,\;K),\;R_xO_y(3-6\%,\;R=Fe,Ti)$ in weight ratio, which were higher silica and flux $(RO{\cdot}R_2O)$ but lower alumina. Owing to the high content$(21-30\%)$ of calcium oxide the glaze is considered lime type. Firing temperature range for the ceramic was presumed to about $1150^{\circ}C$.

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A Case of Acquired Myasthenia Gravis in German Shepherd Dog (개에서 발생한 후천성 중증근육무력증 일례)

  • Lee Sang-Gwan;Hoh Woo-Pil;Kim Youn-Ju;Kim Tae-Wan;Yoo Jong-Hyun;Eom Ki-Dong;Oh Tae-Ho;Lee Keun-Woo
    • Journal of Veterinary Clinics
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    • v.22 no.4
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    • pp.392-395
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    • 2005
  • A three-year old intact female German shepherd dog weighing 32kg was presented with the history of regurgitation and vomiting. Physical examination revealed a thin body condition, hoarse voice, hypersalivation, and pelvic limb weakness. In radiograph, meagaesophagus was identified. The neostigmine challenge test was positive. The titer of acetylcholine receptor (AChR) antibody was 1.58 nmol/L (reference range, <0.6nmol). Therefore, the dog was diagnosed to be suffering with chronic generalized form of acquired myasthenia gravis and followed by treatment with pyridostigmine bromide, 1mg/kg, q12 hrs. Treatment improved the pelvic limb weakness, however intermittent regurgitation and vomiting persisted. This resulted in aspiration pneumonia f3r which antibiotics were administered However, the dog was euthanized due to poor management and owner's request.

A Microstructural Study on Firing Process of Korean Traditional Ceramics;Punch'ong from Ch'unghyodong, Kwangju (한국 전통 도자기의 번조 공정에 관한 미세구조 연구;광주 충효동 분청사기를 중심으로)

  • Lee, Yeong Eun;Go, Gyeong Sin
    • Journal of the Korean Chemical Society
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    • v.46 no.2
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    • pp.125-138
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    • 2002
  • The kiln at Chollanamdo Kwangjusi Ch'unghyodong, which produced punch'ong and white wares for a period of 70 to 80 years in the 15th century, is examined for their scientific technological param-eters. Punch'ong sherds were divided into seven different groups according to the location and the layer of the waste mounds from which they were excavated. Optical and scanning electron microscope were used for microstructural observations and X-ray diffraction and polarized microscope for mineral characteristics. For determining the firing temperature, sherds were refired at different temperatures and their micro-structural changes were observed. Some wares such as the group CHE2 was high quality wares fired at high emperature around 1200$^{\circ}C$ for palace use, but as the ceramics ware became more widely used and the white wares increasingly preferred over punch'ong, lower quality wares of rougher raw materials were firedat lower temperatures around 1100-1150$^{\circ}C$ in quantity. They used local raw materials of several types, all available locally.

Compositional and microstructural analyses of grayish-blue-powdered celadon in Yeongseo Region in Gangwon-do:by Wonju Beopcheon-temple site (강원도 영서지역 출토 분청사기의 조성 및 미세구조 분석: 원주(原州) 법천사지(法泉寺址)를 중심으로)

  • Lee, Byoung-Hoon;So, Myoung-Gi
    • Analytical Science and Technology
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    • v.26 no.3
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    • pp.211-221
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    • 2013
  • This research aims to examine compositional and microstructural properties of grayish-blue-powdered celadon in Wonju Beopcheon-temple site. X-ray fluorescence sequential spectroscopy (XRF) with micro-point analysis, scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD) were applied to determine the chemical composition, microstructure and crystallinity of samples, respectively. As a result, the average compositions of bodies were low silica ($RO_2$) and high flux (RO+$R_2O$). Owing to the high content of calcium oxide the glaze is considered lime type between limealkali type. The body of celdon sheard was found quarts, mullite, microcline, albite. Especially, the body's chemical compositions were compared to the results of previous studies by using a Seger formula. The compositional properties of Grayish-blue-powdered celadon in Wonju Beopcheon-temple site showed diffrently from the the other grayish-blue-powdered celadon.

Antibody-dependent rat macrophage-mediated damage Into the excysted metacercariae of Paragonimus westeymani in vitro (폐흡충(Paragonimus westermani) 감염시의 세포 면역학적 장어 기전)

  • 정평림;장재경;소진천
    • Parasites, Hosts and Diseases
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    • v.29 no.1
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    • pp.43-54
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    • 1991
  • An in vitro immune effector mechanism against the target encysted metacercariae of Paragonimus westermani was demonstrated in the rat system. Peritoneal exudate cells, mainly macrophages from normal rats, showed adherence to and killing of encysted metacercariae of p. westermani in the presence of complement-independent serum from rats infected with Paragonimus metacercariae. These reactions were specific for the excysted metacercariae, as tissue-migrating juvenile worms were not affected. Damage of encysted metacercariae of p. westermani due to antibody and macrophages was assessed by morphological observation, by cell adherence reaction and by the use of vital dyes. frypan blue dye exclusion proved to be a reliable indicator of judging metacercarial viability. Electron microscopic studies demonstrated that macrophages reacted with fusty material on the tegumental surface and fine structures in the syncytium of the parasites. The tubular tunnels formed between the basement membrane and muscle layers of the damaged parasites were also noticeable. The relevance of these findings to cellular immunity in the early paragonimiasis was discussed.

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A Comparative Study on the Decoration of Korean Celadon and Chinese Celadon in the 12th and 13th Centuries (12~13세기 고려청자와 중국청자의 장식디자인 비교 연구)

  • Yue, kun;Ren, chuan;Kim, Hea-jin
    • Journal of Digital Convergence
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    • v.17 no.3
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    • pp.427-432
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    • 2019
  • In the 12th century to the 13th century, was the heyday of celadon, Koryo celadon after experienced celadon firing technology of imitation to the peak period of the development of Chinese celadon, especially on decoration technology pioneered the self unique style, the way of engraving, $xi{\grave{a}}ngqi{\grave{a}}n$. During this period, the southern Song dynasty celadon in China also innovated in the mature celadon firing technology and became more distinctive. The decorative style also promoted the aesthetic interest of the Song dynasty. Celadon decoration is not only a decorative art of ceramic art, but also a representation of national cultural phenomenon with the traditional culture in the development of contemporary art, play a more important role and value.