• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.4
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• pp.1819-1824
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• 2014

The vacuum-glazing panel is a panel that keeps two glasses completely sealed in a vacuum condition. It is the high function insulation material of having the wall level minimizing the heat loss by the conduction and convection heat transmission coefficient. The edge sealing is a very important process of vacuum glass on the strength, thickness and air tightness. In this study, by using the hydrogen mixture gas torch, two sheets of glass was sealing in the furnace. The thickness and strength of the glass according to the process parameters is measurement and analysis, and predicting the edge sealing strength of glass by using taguchi method of experiment. We verified the validity of the experiment by checking the error rate through additional experiment.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.14 no.2
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• pp.567-572
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• 2013

In houses that use heating and cooling system, most of heat loss occurs through the windows, so that low-E glass, double-layered glass, and vacuum glazing are used to minimize the heat loss. In this paper, an encapsulating process that is a final process in manufacturing the vacuum glazing has been studied, and bonding in a vacuum chamber rather than atmospheric bonding was considered. For the efficiency of the encapsulating process, frit-melting temperature and bonding time were optimized with heater temperature, and the glass preheating temperature was optimized to prevent glass breakage due to thermal stress. Thus the vacuum glass was successfully manufactured based on these results and heat transmission coefficient measured was about $5.7W/m^2K$ which indicates that the internal pressure of the vacuum glazing is $10^{-2}$ torr.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.1 no.2
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• pp.94-103
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• 1991

ZnO-$P_2O_5$ system glasses containing 45 to 60 mol% ZnO have been melted at$1200^{\circ}C$and crystallized through controlled heat treatment. The properties of the base glass and crystallized glass were examined with XRD. FTIR. density. thermal expansion, electric conductivity, hardness. The principal crystalline phase was identified as zinc metaphosphate [$Zn(PO_3)_2$ in crystallized glasses containing 45-55mol% ZnO and zinc pyrophosphate ($Zn_2P_2O_7$) in the sample of 60mol% ZnO with X - ray diffraction analysis. Thermal expansion coefficient and DC electrical conductivity were varied with direction of oriented crystalline in the samples containing 50-60mol% ZnO. This suggests the existance of the oriented crystalline.

• Journal of Conservation Science
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• v.27 no.2
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• pp.163-179
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• 2011

This study was to identify the material characteristics and provenance of the crucibles, potteries and roof tiles from the Wonsinheungdong site in Daejeon, Korea. Similar mineral composition of each samples showed by microscopic observation and X-ray diffraction analysis. However, wall thickness and mineral characterization of each ceramic artifacts are quite different. The pottery is characterized by thin wall with 0.5 to 0.7 cm and fine grained clay matrix. While the crucible and roof tile has thick wall with 1.3 to 2.5 cm, poorly sorted texture of many quarz, orthoclase and plagioclase whithin ceramic fabric. And large elonagated voids formed by hydrocarbone of straw during the firing and loose matrix obseved in crucible. All ceramic samples and ground soil of the site show similar mineralogical characteristics geochemical behavior and clay-mineralization degree. This indicates making that the soil is probable to be a raw material of all ceramic from the Wonsinheungdong site. Also, firing temperature of most ceramic artifacts are estimated as 850 of all ceramic from the Wonsinheungdong site. Also, firing temperature of most ceramic artifacts are estimated as 850 to $950^{\circ}C$ but hardest pottery fired high temperature between 1,050 to $1,150^{\circ}C$. The vitreous molten materials interpreted in slag included segregation of copper and tin. But it can not exclude the possibility that the glass molten material because observed reddish and greenish vitreous fine structure under microscopic.

• The Journal of the Petrological Society of Korea
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• v.24 no.2
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• pp.141-147
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• 2015

Using laser-ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), we evaluated the reliability of trace element abundance data measured from the silicate rock references of JR-3, JG-3, JGb-1 and JB-1b using glass discs made by alkali fusion. For 28 elements including rare earth elements, relative standard deviations (RSD) are better than 7% in case when the concentrations of the elements in the rock samples are greater than 10 ppm. However, RSD shows somewhat increased values for the concentrations less than 10 ppm, but never exceeds 25%. Compared with previously reported averages of the compiled abundance data, our data display satisfactory results for the most cases with differences less than 10%. We suggest that LA-ICP-MS analysis using fused glass beads is a reliable, precise and time-saving method of trace element analysis for the silicate rocks spanning from mafic to felsic compositions.

• The Journal of the Petrological Society of Korea
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• v.13 no.1
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• pp.34-45
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• 2004

This paper describes the textural relations of mantle xenoliths and fluid inclusions in mantle-derived rocks found in alkaline basalts from Jeju Island which contain abundant ultramafic, felsic, and cumulate xenoliths. Most of the ultramafic xenoliths are spinel-lherzolites, composed of olivine, orthopyroxene, clinopyroxene and spinel. The felsic xenoliths considered as partially molten buchites consist of quartz and plagioclase with black veinlets, which are the product of ultrahigh-temperature metamorphism of lower crustal materials. The cumulate xenoliths, clinopyroxene-rich or clinopyroxene megacrysts, are also present. Textural examination of these xenoliths reveals that the xenoliths are typically coarse grained with metamorphic characteristics, testifying to a complex history of evolution of the lower crust/upper mantle source region. The ultramafic xenoliths contain protogranular, porphyroclastic and equigranular textures with annealing features, indicating the presence of shear regime in upper mantle of the Island. The preferential associations of spinel and olivine with large orthopyroxenes suggest a previous high temperature equilibrium in the high-Al field and the original rock-type was a Al-rich orthopyroxene-bearing peridotite without garnet. Three types of fluid inclusions trapped in mantle-derived xenoliths include CO$_2$-rich fluid (Type I), multiphase silicate melt (glass ${\pm}$ devitrified crystals ${\pm}$ one or more daughter crystals ＋ one or more vapor bubbles) (Type II), and sulfide (melt) inclusions (Type III). C$_2$-rich inclusions are the most abundant volatile species in mantle xenoliths, supporting the presence of a separate CO$_2$-rich phase. These CO$_2$-rich inclusions are spatially associated with silicate and sulfide melts, suggesting immiscibility between them. Most multiphase silicate melt inclusions contain considerable amount of silicic glass. reflecting the formation of silicic melts in the lower crust/upper mantle. Combining fluid and melt inclusion data with conventional petrological and geochemical information will help to constrain the fluid regime, fluid-melt-mineral interaction processes in the mantle of the Korean Peninsula and pressure-temperature history of the host xenoliths in future studies.

• Journal of the Korean Ceramic Society
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• v.39 no.2
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• pp.145-152
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• 2002

Four commercial alumina powders having different particle size of $0.5{\mu}m,\;2.8{\mu}m,\;12{\mu}m,\;and\;45{\mu}m$ were presintered at 1120$^{\circ}C$ for 2h and then lanthanum aluminosilicate glass was infiltrated at 1100$^{\circ}C$ for 2h in the interval of 0.1h to investigate the penetration kinetic of the glass into the alumina preforms. The infiltration distance is parabolic with respect to time as described by the Washburn equation and the penetration rate constant, K, increases with raising the alumina particle size. The strength of glass-alumina composites increases as the alumina particle size reaches to 2.8${\mu}m$ due to the increase in packing, however, decreases with further increasing the alumina particle size. The fracture toughness of the composites rises with increasing the alumina particle size due to the crack bowing and the interaction between crack and alumina particles.

• Journal of the Korean Ceramic Society
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• v.39 no.6
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• pp.558-565
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• 2002

Coal fly ash, produced from a power plant in Korea was used for the production of glass-ceramics and the physical properties of glass-ceramics were evaluated. CaO and TiO$_2$ were added into the fly ash during the melting process to reduce the viscosity of molten glass and to induce internal crystallization of glass, respectively. Glass-ceramic was produced through a single stage heat treatment (at 950∼1050$\^{C}$ for 37∼240 min) after preparing glass (iota fly ash powder. As a result, a new tiny rod type crystals (a=7.4480, b=10.7381, c=4.3940 A, $\alpha$=94.9, $\beta$=98.6, γ=108.5°) was found in the glass-ceramics, which showed attractive mechanical properties, high hardness (7.1∼7.6 GPa) and wear resistance (by erosion test). Thus a glass-ceramic produced from thermal power plant fly ash and cell as a source for CaO exhibits a suitable treatment for the recycling and exploitation of waste materials and would be acceptable for a new application far building materials.

• Proceedings of the Korean Fiber Society Conference
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• 2003.04a
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• pp.384-385
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• 2003

최근 나노기술에 대한 관심이 급격히 부각되어짐에 따라 섬유에 있어서도 나노섬유 제조에 관하여 많은 관심이 모아지고 있다. 현재까지 알려진 나노섬유 제조법 중 공정, 설비 및 제조원가면에서 가장 유리한 전기방사법에 관하여 지대한 관심이 모아지고 있다. 전기방사법이란 고분자 용액이나 용융된 고분자에 고전압의 전하를 걸어주어 부직포를 집속 할 수 있는 금속소재의 콜렉터(collector)와 팁사이에 전기장을 형성시켜 부직포를 제조하는 방법이다 [1-3]. (중략)

• Proceedings of the KAIS Fall Conference
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• 2007.05a
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• pp.126-128
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• 2007

본 논문은 산업현장에서 발생하는 대표적인 폐유리를 기본 소재로 카본의 입도에 분포에 따른 발포 기공의 변화와 그에 따른 강도의 변화를 측정하고자 한다. 산업체에서 발생하는 폐유리는 그 양이 점차 늘어나고 있으며， 매립으로 인한 토양 오염 또한 심각한 상태이며 이에 활용도로 발포와 재용융의 다양한 방법으로 재활용이 이루어지고 있으며， 본 실험은 발포를 통한 여과제 또는 경량 골재， 수질 정화용 필터로 사용을 하고 있는 발포의 기본 특성 중에 카본 발포제의 입도의 영향에 대하여 좀 더 확인해 보기 위해 실험을 진행 하였다.