• Title/Summary/Keyword: 온도 안정시간

Search Result 999, Processing Time 0.029 seconds

A Study on Preparation of Colloidal Gas Aphrons and Stability (Colloidal Gas Aphrons의 제조와 안정성에 대한 연구)

  • Yoon, Mi-Hae;Cho, Dae-Chul
    • Journal of Korean Society of Environmental Engineers
    • /
    • v.29 no.6
    • /
    • pp.670-677
    • /
    • 2007
  • The stability of CGAs(colloidal gas aphrons) prepared from non-ionic and ionic surfactants was investigated. Those surfactants were sodium dodecyl sulfate(SDS), Triton X-100, Tween 80 and Quillaja Saponin. The stability of CGAs prepared from single surfactants or mixed surfactants(two components) using a CGA generate. was investigated as functions of temperature, surfactant concentration and stirring time. Saponin among the single surfactants has shown the longest duration time(143 min) and then, Triton X-100, SDS, and Tween 80 were followed by at room temperature. In case of CGAs heated up to $70^{\circ}C$, SDS endured for 116 min but Saponin lasted for only 105 mit which was a considerable reduction of the duration time of CGAs at room temperature. For mixed surfactant pairs, stability of any one pairs stood between the two. That meant no synergic effect for surfactant blending. At the higher temperature, Saponin+Triton X-100 was disclosed to be the lowest, 53 min meanwhile Saponin+SDS was the highest at ambient temperature. The CGAs, initially about 140 ${\mu}m$ in diameter, began to grow right after the agitation to be about 190 ${\mu}m$ owing to coalescence of the bubbles and then became to collapse. When heated, CGAs including Saponin tended to be smaller while the others to be larger. In summary, we found that the stability of CGAs or the duration time was greater for single surfactants and at room temperature rather than for mixed surfactants that caused substantial intermolecular interactions in the CGA structure and at the higher temperature.

Optimization of Extraction Condition and Stability of Olive Leaf Extract (올리브 잎의 적정 추출조건 및 추출물의 안정성 조사)

  • Lee, Ok-Hwan;Lee, Hee-Bong;Lee, Jun-Soo;Lee, Boo-Yong
    • Korean Journal of Food Science and Technology
    • /
    • v.37 no.2
    • /
    • pp.178-182
    • /
    • 2005
  • Basic optimal extraction condition and stability data were determined for prediction of usefulness of olive leaf as functional food material. Solid contents of olive leaf extracts increased with increasing extraction temperature and ethanol content, and was the highest (38%) under $85^{\circ}C$, 80% ethanol, and 5 hr treatment conditions, Total phenol contents and electron-donating abilities of olive leaf extracts also increased with Increasing ethanol content, and were the highest under $25^{\circ}C$, 80% ethanol, and 1 hr treatment conditions, then slightly decreased during storage at $25,\;55,\;and\;85^{\circ}C$. Olive leaf extract showed high stability under acidic storage condition, while low under alkalic condition.

Change of Korean Ginseng Components with High Temperature and Pressure Treatment (고온고압처리에 의한 인삼의 성분 변화)

  • Yang, Seung-Joon;Woo, Koan-Sik;Yoo, Jeong-Sik;Kang, Tae-Su;Noh, Young-Hee;Lee, Jun-Soo;Jeong, Heon-Sang
    • Korean Journal of Food Science and Technology
    • /
    • v.38 no.4
    • /
    • pp.521-525
    • /
    • 2006
  • Korean ginseng was heat treated at various temperatures (110, 120, 130, 140 and $150^{\circ}C$) and times (1, 2, 3, 4, and 5 hr). The heat treated ginseng extract was analyzed for the total polyphenol content, total flavonoid content, DPPH free-radical scavenging, 5-HMF and ginsenoside. The total phenolics and flavonoid content increased with increasing treatment temperature and time. The highest total phenolics content was 29.46 mg/g (d.b) in $150^{\circ}C$ for 1hr (control: 2.68 mg/g). The highest total flavonoid content was 4.75mg/g (d.b) in $150^{\circ}C$ for 2hr (control: 0.39 mg/g). The antioxidant activity increased until $140^{\circ}C$ for 3 hours. An extension of the treatment time did not have any effect, and the antioxidant activity decreased at temperatures higher than $150^{\circ}C$ for more than 2 hours. The content of ginsenoside $Rg_1$, Re, $Rb_2$ and Rb3 rapidly decreased with increasing treatment temperature and time. Ginsenoside $Rg_3$ and $Rh_2$ were newly produced, or their contents increased with increasing treatment temperature and time.

Stability of Naphthoquinone Pigments Isolated from the Roots of Lithospermum erythrorhizon by Various Temperatures and Metal Ions (자근(紫根)으로부터 분리한 Naphthoquinone류 색소의 온도 및 금속에 대한 안정성)

  • Chung, Mi-Sook;Lee, Mie-Soon
    • Korean Journal of Food Science and Technology
    • /
    • v.27 no.1
    • /
    • pp.97-100
    • /
    • 1995
  • The pigments of acetylshikonin and isobutylshikonin isolated from the roots of Lithospermum erythrorhizon were determined over a period of storage for their stabilities influenced by temperatures and metal ions. In dark condition, both pigment solution were unstable at 488 and 560 nm; alcoholic solutions of acetylshikonin pigment were stable at $25^{\circ}C$ and $50^{\circ}C$ for 1 hour, but isobutylshikonin showed severe discoloration within 1 hour at $95^{\circ}C$ . Buffered solutions of acetylshikonin tended to be discolored with the addition of $Fe^{++}$, while those of isobutylshikonin with $Fe^{++}$ and $Cu^{++}$. These studies indicated that acetylshikonin and isobutylshikonin can be used in foods as the natural colorant under selected conditions in case of considering storage temperature and metal ions.

  • PDF

A Study on the Degradation Properties of DGEBA/TETA Epoxy System for Restoration of Ceramics by Temperature (도자기 복원용 DGEBA/TETA Epoxy계 수지의 온도에 의한 열화 특성 연구)

  • Nam, Byeong Jik;Jang, Sung Yoon
    • Journal of Conservation Science
    • /
    • v.31 no.4
    • /
    • pp.373-386
    • /
    • 2015
  • This study identified degradation properties by temperature stress with Araldite$^{(R)}$ AY103-1/HY956 used for ceramics. Tensile and compressive strength of durability increased for 6,480 hours at temperature of $34{\sim}45^{\circ}C$. In stability of external stress and temperature, compressive strength is superior to tensile strength, it requires conservation plans considering strength properties and stress of restoration materials. The tensile shear strength of adhesion properties decreased for 4,320 hours at temperature of $40{\sim}60^{\circ}C$. In ceramics with porosity, environments under isothermal-isohumidity are important because interfacial properties of adherend are concerned with performance variation. Glossiness decreased for 6,480 hours at temperature of $34{\sim}45^{\circ}C$ and color difference increased. Gloss stability was superior and color stability was weak, which requires improvement of optical properties. In artifacts on display in museums, there is concern about temperature rise on restoration materials by lighting therefore, it needs to minimize change in physical properties by exposure environments.

Preparation of Iron-Coated Sand and Arsenic Adsorption (철코팅 모래흡착제 제조 및 비소흡착)

  • Chang, Yoon-Young;Kim, Kwang-Sub;Jung, Jae-Hyun;Lee, Seung-Mok;Yang, Jae-Kyu;Park, Joon-Kyu
    • Journal of Korean Society of Environmental Engineers
    • /
    • v.27 no.7
    • /
    • pp.697-703
    • /
    • 2005
  • Iron-coated sand(ICS) was prepared with variation of particle size of Joomoonjin sand, primary and secondary coating temperature, coating time, and dosage of initial Fe(III). An optimum condition of the preparation ICS was selected from the coating efficiency, stability of coated Fe(III), and removal efficiency of As(V). Coated amount of Fe(III) increased as primary coating temperature increased with smaller particle size of sand. Coating efficiency was quite similar over the investigated secondary coating temperature and time, while adsorption efficiency of As(V) onto ICS was severely reduced with ICS prepared at higher secondary coating temperature. By considering these results, an optimum secondary coating temperature and time for the preparation of ICS was selected as $150^{\circ}C$ and 1-hr, respectively. Coating efficiency increased us the dosage of initial Fe(III) up to 0.8 Fe(III) mol/kg sand and then no distinct increase was noted. Maximum As(V) adsorption was observed at 0.8 Fe(III) mol/kg sand. Secondary coating temperature and time were important parameters affecting stability of ICS, showing decreased dissolution of Fe(III) from ICS prepared at higher coating temperature and at longer coating time. From anionic type adsorption of As(V) onto ICS, it is possible to suggest the application of ICS for the removal of As(V) contaminated in acidic water system.

Digital Control Based Bridgeless CRM PFC Converter For HID Ballast (디지털 제어 기반의 HID 안정기용 브릿지리스 CRM PFC 컨버터)

  • Kim, Tae-Hun;Lee, WooCheol
    • Proceedings of the KIPE Conference
    • /
    • 2016.07a
    • /
    • pp.263-264
    • /
    • 2016
  • 일반적으로 HID 램프용 안정기에는 디지털 제어기를 사용하지 않지만 디지털 제어로 구현하는 경우 여러 가지 이점이 있다. 따라서 본 논문에서는 DSP를 기반으로 Bridgeless CRM PFC Converter 제어를 디지털로 구현 할 것을 제안하였다. 이때 인덕터 전류 검출을 하지 않기 위하여 DSP 연산에 의해 계산된 온, 오프 시간으로 동작하도록 하였으며, 과도상태 시 출력 전압에 따른 주파수 제한 방법을 통해 안정적인 구동이 가능하도록 하였다. 제안한 방식은 시뮬레이션을 통해 검증하였다.

  • PDF

Fire Resistance of High Performance Concrete(High Strength Concrete & Fiber Reinforced Concrete) (고성능 콘크리트의 내화성능(고강도 및 섬유보강 콘크리트))

  • 소양섭
    • Magazine of the Korea Concrete Institute
    • /
    • v.14 no.2
    • /
    • pp.37-44
    • /
    • 2002
  • 콘크리트의 내화성능에 대한 다각적인 연구가 1970년대부터 원자로의 안정성 확보차원에서 진행되어 왔으며 특히 콘크리트의 취성파괴(brittle failure)등에 대한 연구가 많다. 콘크리트의 내화성이란 화재로부터 보호되고 고열환경에 견디는 재료적 특성 즉 화재온도 1,00$0^{\circ}C$ 정도의 고온을 30분에서 3시간 정도를 받은 경우 콘크리트 중에 매립된 철근 등 철강을 소정의 온도 이하고 유지하기 위한 피복 역할을 유지하면서 구조물의 큰 변형이나 붕괴 등을 막기 위한 소요 압축강도 및 영계수 등의 성능을 가지고 있는 성질을 말한다.(중략)

Effect of Microstructure on Thermal Conductivity of Cu and Ag Thin Films (구리와 은 금속박막의 열전도도에 미치는 미세구조의 영향)

  • Ryu, Sang;Jeong, U-Nam;Kim, Yeong-Man
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2008.11a
    • /
    • pp.19-20
    • /
    • 2008
  • 본 연구에서는 박막의 미세구조, 특히 결정립의 크기에 따라 박막 열전도도를 측정하여 실제 박막 응용제품의 제조 공정에 피드백 하여 부품의 안정성을 제고하고자 한다. 우리는 온도 분포법을 사용하여, 구리와 은 박막의 열전도도를 박막의 미세구조를 변화시키면서 측정하였다. 박막제조공정 중 기판온도를 변화시켜서 박막의 미세구조를 변화시켰다. 두께의 영향을 최소화하기 위해서 증착 시간을 조절하여 500nm정도로 두께를 일정하게 하였다. 4-point probe를 이용하여 코팅된 박막의 비저항을 측정하였다. 이로부터 박막의 Lorenz number를 계산하였다.

  • PDF

Fabrication of low power micro-heater based on electrochemically prepared anodic porous alumnia (다공성 알루미늄 산화물을 이용한 저전력 마이크로 히터의 제조)

  • Park, Seung-Ho;Byeon, Seong-Hyeon;Lee, Dong-Eun
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2016.11a
    • /
    • pp.116.1-116.1
    • /
    • 2016
  • 반도체 가스센서에서는 가연성 및 탄화수소계 가스를 감지 하기 위해서 $100{\sim}500^{\circ}C$ 이상의 동작온도를 필요로 한며, 이에 따라 반도체식 가스센서의 마이크로 히터 소재는 고온에서 열적 안정성이 있는 소재가 요구된다. 현재 상용화되고 있는 반도체식 가스센서는 실리콘(Silicon) 기반의 MEMS 기술을 이용한 가스센서이며, 구조적으로나 성능적 한계가 드러남에 따라 실리콘 이외의 다양한 재료의 MEMS 응용기술 개발이 필요한 실정이다. 본 연구에서는 이러한 실리콘의 재료적 한계를 극복하기 위해 다공성 알루미늄 산화물(AAO)을 기판으로 사용하여 마이크로 히터를 제작하였다. AAO의 제작에 앞서 CMP, 화학연마, 전해연마를 이용하여 적합한 전처리 공정을 선정하였고, AAO 제작 시 온도, 시간, 전압의 변수를 주어 마이크로 히터 기판에 적합한 공정을 탐색하였다. 마이크로 플랫폼은 MEMS 공정으로 제작되었으며, PR(Photo Resist)을 LPR(Liquid Photo Resist)과 DFR(Dry Film Resist)로 각각 2종 씩 선택하여 AAO에 적합한 제품을 선정하였다. 제작된 마이크로 히터는 $1.8mm{\times}1,8mm$로 소형화 하였고, 열손실의 제어를 위해 열확산 방지층을 추가하였다. 구동 온도, 소비전력, 장시간 구동시 안정성의 측정 및 평가는 적외선 열화상 카메라와 kiethly 2420 source meter를 이용하여 측정하였으며, 열확산 방지층의 유 무에 따른 온도 분포 및 소비전력을 비교평가 하였다. 최종적으로는 현재 사용화 되어있는 가스센서들의 소비전력과 비교 평가 하여 논의 하였다.

  • PDF