• Food Science and Preservation
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• v.8 no.3
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• pp.338-344
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• 2001

The oxidative stability of cholesterol in tallow heated at different frying temperatures (130$\^{C}$, 150$\^{C}$, and 180$\^{C}$) was studied by identifying cholesterol oxides by thin layer chromatography(TLC). And fatty acid compositions in tallow heated were also measured and compared with cholesterol oxides. Unsaturated fatty acid contents slightly decreased as the heating time increased, whereas saturated fatty acid contents increased This phenomenon became excessive especially by heating to higher temperature. It was found that RF value and spot color of the nonsaponifiable lipids from tallow heated on TLC analysis accorded with the synthetic cholesterol oxides in this experiment. Four kinds of cholesterol oxides were detected in tallow heated for 24 hours at three different temperatures. The oxides were identified as 7-$\alpha$-hydroxycholesterol, 7-$\beta$-hydroxycholesterol, 7-ketocholesterol and cholesterol epoxide. It was found that there was a little difference in oxidative pattern of cholesterol between several heating temperatures.

• Korean Journal of Microbiology
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• v.39 no.3
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• pp.197-200
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• 2003

In order to establish effective in situ PCR on the glass slide using the conventional DNA thermal cycler, several parameters should be considered. These include full accessibility of PCR reagents into the cells, prevention of diffusing PCR products out of the cells, loss of PCR reagents by nonspecific adherence onto the glass slide, dryness of PCR reagents by heat, and heat conductivity from the heat block to the glass slide. Especially, to guarantee the full accessibility of PCR reagents to sample, relatively higher concentration of PCR reagents (particularly 4.5 mM of $Mg^{++}$) was required while 5 to 10 units/50 ${\mu}l$ reaction of Taq enzyme was enough as long as the step of pre-PCR incubation was included. Dryness of sample was prevented by addition of distilled water into the empty slots in the heat block, thereby providing the reproducible temperature-time profile of PCR. Observed temperature was lower than the programmed temperature by 3 to $4^{\circ}C$.

• Journal of the Korea Institute of Information and Communication Engineering
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• v.18 no.2
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• pp.401-407
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• 2014

There are increasing interests in COB (Chip On Board) that densely arranged many LED chips on one board in order to solve the heat issue. There are many problems being on the rise: the lifespan decreases as the temperature of LED devices increases; Red Shift phenomenon, in which wave length of spectral line moves from original wave length to long wave length, occurs; and optical power decreases as $T_j$ increases. In order to resolve such problems, this study selected the optimum thickness and length of Fin, planned the second Heat sink that is optimum for COB LED with 15W, and analyzed thermal mode by Solid Works Flow Simulation through 15W COB packaging with the planned Heat sink. 15W COB down-light Heat sink that is produced based on this analysis was utilized to analyze thermal mode through contact thermometer and electrical properties through Kelthley 2430.

• Journal of the Korean Society of Propulsion Engineers
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• v.23 no.4
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• pp.42-49
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• 2019

This paper presents a method to predict the storage reliability of springs for turbo engine components based on an accelerated degradation test. The reliability assessment procedure for springs is established to proceed with the accelerated degradation test. The spring constant is selected as the performance degradation characteristic, the temperature is determined to be the stress factor that deteriorates the spring constant. The storage tests are performed at three temperature test conditions. The spring constant is measured periodically to check the degradation status of the springs. Failure times of the springs are predicted by using the degradation model. Finally, the storage lifetime of the springs at normal use conditions is predicted using an accelerated model and failure times of all test conditions.

• Journal of the Korean Wood Science and Technology
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• v.31 no.2
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• pp.38-44
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• 2003

This study was carried out to evaluate the feasibility of using HDF as surface panels as well as core materials for flush door manufacturing. Six core constructions were developed and applied to manufacture door specimens and conventional skin door specimen was also manufactured for comparison. Door specimens were tested under changing interior environmental condition for 3~4 months during winter and summer seasons. During the test period, deformation of doors were measured weekly, and temperature and relative humidity of testing area were also recorded. From this study, it was concluded that HDF can be used to manufacture quality flush doors and core construction developed in this study showed good quality compared to conventional skin door. Deformation of doors increased as temperature and relative humidity of the surrounding environment increased. Flush doors generally showed less deformation than skin doors, and evaluated to be stable and good quality when compared to skin door.

• Applied Chemistry for Engineering
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• v.28 no.5
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• pp.576-580
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• 2017

In the present paper, the thermal deactivation characteristics of plate-type commercial $V_2O_5-WO_3/TiO_2$ SCR catalyst were investigated. For this purpose, the plate-type catalyst was calcined at different temperatures ranging from $500^{\circ}C$ to $800^{\circ}C$ for 3 hours. Structural and morphological changes were characterized byXRD, specific surface area, porosity, SEM-EDS and also NOx conversion with ammonia according to the calcine temperature. The NOx conversion decreased with increasing calcine temperature, especially when the catalysts were calcined at temperatures above $700^{\circ}C$. This is because the crystal phase of $TiO_2$ changed from anatase to rutile, and the $TiO_2$ grain growth and $CaWO_4$ crystal phase were formed, which reduced the specific surface area and pore volume. In addition, $V_2O_5$, which is a catalytically active material, was sublimated or vaporized over $700^{\circ}C$, and a metal mesh used as a support of the catalyst occurred intergranular corrosion and oxidation due to the formation of Cr carbide.

• Journal of Korean Tunnelling and Underground Space Association
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• v.24 no.1
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• pp.39-55
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• 2022

This study carried out the laboratory tests for AE signal attenuation to determine the attenuation coefficient (α) of silo concrete in Gyeongju low and intermediate-level disposal environments. The concrete samples were prepared by satisfying the concrete mixing ratio used in the Gyeongju disposal silo, and these samples were additionally exposed depending on the temperature conditions and saturation and, dry condition. As a result of attenuation tests according to the transmission distance on three concrete specimens for each disposal condition, the AE amplitude and absolute energy measured on the saturated concrete were higher than that of the dry concrete in the initial range of the signal transmission distance, but the α of the saturated concrete was higher than that of the dry concrete. Regardless of the saturation and dry conditions, the α tended to decrease as the temperature increases. The α had a more major influence on the saturation and dry condition than the temperature condition, which means that the saturation and dry condition is the main consideration in measuring the signal attenuation of a concrete disposal structure. The α of concrete in the disposal environment expect to be used to predict the integrity of silos concrete in Gyeongju low and intermediate-level disposal environments by estimating the actual AE parameter values at the location of cracks and to determine the optimum location of sensors.

• Journal of Energy Engineering
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• v.8 no.2
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• pp.224-232
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• 1999

Latent heat storage system using micro-encapsuled phase change material is effective method for floor heating of house and building. The temperature profile in capsule block and flow rate of hot water are important parameters for the development of heat storage system. In the present study, a mathematical model based on 3-D, non-steady state, Navier-Stokes equations, scalar conservation equations and turbulence model ($\kappa$-$\varepsilon$), is used to predict the temperature profiles in capsule and the velocity vectors in hot water pipe. The multi-block grids and fine grids embedding are used to join the circle in hot water pipe and square in capsule block. The phase change process of the capsule is quite complex not only because the size of phase change material is very small, but also because phase change material is mixed with the cement to form thermal storage block. In calculation, it's assumed that the phenomena of phase change is limited only the thermal properties of phase change material and the change of boundary is not happened in capsule. The purpose of this study is to calculate the temperature profiles in capsule block and velocity vectors in hot water pipe using the numerical calculation. Two kinds of thermal boundary condition were considered, the first (case 1) is the adiabatic condition for the both outside surfaces of the wall, the second (case 2) is the case in which one surface is natural convection with atmosphere and another surface is adaibatic. Calculation results are shown that the temperature profile in capsule block for case 1 is higher than that for case 2 due to less heat loss in adaibatic surface. Specially, in the domain of near Y=0, the difference of temperature is greater in case 1 than in case 2. The detailed experimental data of capsule block on the temperature profile and the thermal properties such as specific heat and coefficient of heat transfer with the various temperature are required to predict more exact phenomena of heat transfer.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.17 no.7
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• pp.434-441
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• 2016

Friction Stir Welding (FSW) is a solid-state joining process involving the frictional heat between the materials and tools. The amount of heat conducted into the workpiece determines the quality of the welded zone. Excessive heat input is the cause of oxides and porosity defects, and insufficient heat input can cause problems, such as tunnel defects. Therefore, analyzing the temperature history and distribution at the center of the Friction Stir Welded zone is very important. In this study, the temperature distribution of the friction stir welding region of an AZ61 magnesium alloy was investigated. To achieve this goal, the temperature and metal flow was predicted using the finite element method. In FE analysis, the welding tool was simplified and the friction condition was optimized. Moreover, the temperature measuring test at the center of the welding region was performed to verify the FE results. In this study, the tool rotation speed was a more dominant factor than the welding speed. In addition, the predicted temperature at the center of the welding region showed good agreement with the measurement results within the error range of 5.4% - 7.7%.

• Journal of the Korean Magnetics Society
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• v.7 no.3
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• pp.140-145
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• 1997

The amorphous state of $NdFe_{10.7}TiB_{0.3}$ and its nanocrystallization have been studied by X-ray diffraction, 모스바우어 spectroscopy, and a vibrating sample magnetometer (VSM), $NdFe_{10.7}TiB_{0.3}$ amorphous ribbons were fabricated by a sigle-roll melt-spinning method. The average hyperfine field $H_{hf}$(T) of the amorphous state shows a temperature dependence of $[H_{hf}(T)-H_{hf}(0)]/H_{hf}(0)=-0.46(T/T_c)^{3/2}-0.34(T/T_c)^{5/2}$ for $T/T_c<0.7$ indicative of spin wave excitation. The quadrupole splitting just above the Curie temperature $T_c$ is 0.46 mm/s, whereas the average quadrupole shift below $T_c$ is zero. The Curie and crystallization temperatures are determined to be $T_c$=380K and $T_x=490K$, respectively, for a heating rate of 5 K/min. The occupied area of nanocrystalline phase at around 770K is about 65%. Above the Curie temperature, VSM data show magnetic moments increases again. The formation of $\alpha$-Fe is the main reason for the increasing moment as conformed with the 모스바우어 measurements.