• Composites Research
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• v.30 no.2
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• pp.84-93
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• 2017

This study investigates thermal and mechanical characterization of environmental barrier coating on the $SiC_f-SiC$ composites. The spherical environmental barrier coating (EBC) powders are prepared using a spray drying process for flowing easily during coating process. The powders consisting of mullite and 12 wt% of Ytterbium silicate are air plasma sprayed on the Si bondcoat on the LSI SiC fiber reinforced SiC composite substrate for protecting the composites from oxidation and water vapor reaction. We vary the process parameter of spray distance during air plasma spray of powders, 100, 120 and 140 mm. After that, we performed the thermal durability tests by thermal annealing test at $1100^{\circ}C$ for 100hr and thermal shock test from $1200^{\circ}C$ for 3000 cycles. As a result, the interface delamination of EBC never occur during thermal durability tests while stable cracks are prominent on the coating layer. The crack density and crack length depend on the spray distance during coating. The post indentation test indicates thermal tests influence on the indentation load-displacement mechanical behavior.

• Transactions of the Korean Society of Automotive Engineers
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• v.3 no.1
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• pp.1-12
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• 1995

Isothermal and thermal-mechanical fatigue characteristics of 12Cr heat resisting steel used for high temperature applications were investigated including hold time effects. Isothermal low cycle fatigue test at $600^{\circ}C$ and in-phase, out-of-phase thermal-mechanical fatigue test at 350 to $600^{\circ}C$ were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Regardless of thermal-mechanical and isothermal fatigue tests, cyclic softening behavior was observed and much more pronounced in the thermal-mechanical fatigue tests with hold times due to the stress relaxation during the hold time. The phase difference between temperature and strain in thermal-mechanical fatigue tests resulted in significantly shorter fatigue life for out-of-phase compared to in-phase. The differences in fatigue lives were dependent upon the magnitudes of plastic strain ranges and mean stresses. During the hold time in the strain-controlled fatigue tests, the increase in the plastic strain range and the stress relaxation were observed. It appeared that the increase in plastic strain range per cycle and the introduction of creep damage made important contributions to the reduction of thermal-mechanical fatigue life with hold time, and the life reduction tendency was more remarkable in the in-phase than in the out-of-phase thermal-mechanical fatigue. Isothermal fatigue tests performed under the combination of fast and slow strain rates at $600^{\circ}C$ showed that the fatigue life decreased as the strain rate and frequency decreased,especially for the low strain ranges.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.33 no.12
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• pp.109-116
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• 2005

Elastic-plastic structural analysis for regenerative cooling chamber of liquid rocket thrust chamber is performed. Uniaxial tension test is also conducted for the copper alloy in order to get material data necessary for the structure analysis. The results of uniaxial tension test reveal that copper alloy become ductile after brazing process and flow stress becomes lower as temperature becomes higher. As a result of structural analysis using the material data, the deformation of cooling channel is more increased by thermal load than by internal pressure of cooling fluid. Therefore, the results of analysis show that structural stability and cooling performance of combustion thrust chamber which is designed to endure mechanical load and minimized a channel thickness are improved by decreased thermal load as possible.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.5
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• pp.1192-1202
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• 1994

Fatigue behavior and life prediction were presented for thermal-mechanical and isothermal low cycle fatigue of 12Cr forged steel used for high temperature applications. In-phase and out-of-phase thermal-mechanical fatigue test at 350 to 600.deg. C and isothermal low cycle fatigue test at 600.deg. C were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Cyclic softening behavior was observed regardless of thermal-mechanical and isothermal fatigue tests. The phase difference between temperature and strain in thermal-mechanical fatigue resulted in significantly shorter fatigue life for out-of-phase than for in-phase. The difference in fatigue lives was dependent upon the magnitudes of inelastic strain ranges and mean stresses. Increase in inelastic strain range showed a tendency of intergranular cracking and decrease in fatigue life, especially for out-of-phase thermal-mechanical fatigue. Thermal-mechanical fatigue life prediction was made by partitioning the strain ranges of the hysteresis loops and the results of isothermal low cycle fatigue tests which were performed under the combination of slow and fast strain rates. Predicted fatigue lives for out-of-phase using the strain range partitioning method showed an excellent agreement with the actual out-of-phase thermal-mechanical fatigue lives within a factor of 1.5. Conventional strain range partitioning method exhibited a poor accuracy in the prediction of in-phase thermal-mechanical fatigue lives, which was quite improved conservatively by a proposed strain range partitioning method.

• Journal of Welding and Joining
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• v.16 no.6
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• pp.44-51
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• 1998

It is well known that the fine bainitic microstructure obtained by TMCP(thermo-mechanical control process) secures the high toughness of base metal. Besides, TMCP steel is very suitable for high heat input in welding as it has low carbon equivalent. In HAZ, however, the accelerated cooling effect imparted on the matrix by the weld thermal cycles is relieved and thus the weldment of TMCP steel has softening zone which shows low fracture toughness compared with base metal. Therefore, PHWT of weldment is carried out to improve the fracture toughness in weldment of TMCP steel which has softening zone. In this study, the effects of PWHT on the weldment of AH36-TMCP steel are investigated by the small punch (SP) test. From the several results such as SP energy and displacement at room temperature, the behavior of transition curves, the fracture strength at -196$^{\circ}C$, distribution of (DBTT)sp and (DBTT)sp, the PWHT condition of A.C. after 85$0^{\circ}C$-1 sec W.C. was suitable condition for recovering a softening zone of HAZ as welded.

• Journal of Welding and Joining
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• v.29 no.1
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• pp.59-64
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• 2011

Al6082-T6 is widely used because of its corrosion resistance and excellent strength. HAZ softening occurs in MIG welding process for this aluminium alloys because this aluminium alloy is heated to higher temperature than its aging temperature during welding. Therefore, low heat input and minimum standard deviation of heat input are required for narrow HAZ width and, for higher strength of welds. In this study, Al6082-T6 was used to examine for HAZ softening with various heat input in aluminium MIG welding. For weldments, micro hardness was measured and tensile test was carried out. Minimum hardness was increased at high speed welding such as 80cm/min and 120cm/min in welding speed comparing with 40cm/min. Also, in case of high speed welding such as 80cm/min and 120cm/min, tensile strength of weldments was increased about 10% comparing with low speed welding(40cm/min).

• Food Science of Animal Resources
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• v.20 no.4
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• pp.264-271
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• 2000

정육 대체물질의 첨가에 따른 효과를 살피기위해 건조 소 혈장 단백질을 단계별로 높이면서 제조한 비엔나 소시지의 물성적 특성 드을 경시적으로 고찰 비교하였다. 수율은 방냉후 축정된 것으로 81.60~84.88% 범위이며 대조구와 D-2, D-3간의유의적인 차이를 보였다. (P<0.05). 조직의 부분적인 연화 정도는 대조구에 비해 비교구에서 소 혈장 단백질의 첨가수준이 높은 시럼구에서 높았고 열 매체에 의한 영향은 boiled>microwave>fried의 순이 었다. 겔강도와 경도는 대조구와 비교구 사이, 수직 측정과 수평 측정 사이, 저장기간에 따라 유의적인 차이를 볼 수 있었다.(P<0.05), 전단 강도는 수직측정보다는 수평측정이 높은 수치를 보이고 initial에서 대조구와 비교구 사이 차이가 적게 나타나나 40일 저장한 것에서는 차이 값이 높았다. 전단 경도에 있어서는 initial 에 비해 10일 , 40일 에는 감소함을 보이나 수칙측정과 수평측정간 차이를 보였다 L 값은 시험구간과 저장기간에 의해서도 안정함을 보이며 a값은 대조구에 비해 비교구에서 감소함을 보이나 10일 40일 저장된 것에서 증가함을 보이고, b값은 시험구간 사이 비슷한 수준이나 저장기간에 따라서는 감소를 보였다. 기호성 평가에서 색상, 풍미, 조직감은 시험 제품 사이에 차이를 보이고 저장기간에 의해서는 약간의 감소를 보이며 천제적인 수용도는 대조구가 가장 높은 점수였다.

• Journal of the Korean Society of Food Science and Nutrition
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• v.22 no.6
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• pp.803-806
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• 1993

The properties of proteolytic enzymes from the fruit of Broussonetia Kazinoki Siebold were investigated. The protease activity of the enzymes from the fruit of Broussonetia Kazinoki Siebold was 1.6 unit. The optimum temperature and pH of the enzymes were $60^{\circ}C$ and 7.0, respectively. The enzymes were stable at pH values from 6 to 8 for 1 hr. at $37^{\circ}C$ of incubation and also retained all activity after incubation for 1 hr. at $60^{\circ}C$. The enzyme preparations showed strong activities toward hemoglobin and collagen.

• Journal of Korea Foundry Society
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• v.27 no.5
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• pp.221-223
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• 2007

공구강은 C, Cr, V, Mo, W, Co 및 Si 과 같은 첨가원소를 함유한 복잡한 철계 합금으로 주요 특성인 경도, 부식저항성, 열 연화저항성 그리고 인성의 요구수준에 따라 화학성분이 결정된다. 본 연구에서는 1.0C, 0.2Mn, 3.8Cr, 1.5W, 8.5Co, 9.2Mo, 1.0V 조성의 M42 공구강의 미세조직과 열간가공성에 미치는 Si 함량의 효과를 체계적으로 조사하였다. 진공유도용해를 이용하여 Si 함량을 중량비로 0.33 에서 1.7% 까지 변화시켜 $140{\times}140{\times}330\;mm^{3}$ 크기의 잉곳으로 제조하였다. 이렇게 제조한 잉곳들은 $1150^{\circ}C$에서 1.5시간 동안 용체화처리한 후 노냉하였고, 이어 $1180^{\circ}C$에서 15mm 두께의 판재로 열간압연하였다. 공정 탄화물의 형상 및 분해 거동을 중심으로 미세조직을 관찰한 결과 Si 함량이 증가함에 따라 분해속도가 느려지는 것을 알 수 있었고 이로 인해 열간성형성이 급격히 저하되는 것으로 나타났다.

• Journal of the Korean Society of Marine Environment & Safety
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• v.18 no.3
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• pp.273-278
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• 2012

The use of Al alloys instead of fiber-reinforced plastic(FRP) in ship construction has increased because of the advantages of Al-alloy ships, including high speed, increased load capacity, and ease of recycling. This paper describes the effects of probe diameter on the optimum friction stir welding conditions of 5456-H116 alloy for leisure ship, measured by a tensile test. In friction stir welding using a probe diameter of 5 mm under various travel and rotation speed conditions, the best performance was achieved with a travel speed of 61 mm/min. Using a probe diameter of 6 mm, rotation speeds of 170-210 rpm, and a travel speed of 15 mm/min produced a rough surface and voids because of insufficient heat input produced by the low rotation speed. At 500-800 rpm, chips were observed, although there were no voids, and the weld surface was excellent. However, at 1100-2500 rpm, many chips were produced due to excessive heat input. Heat effects were very evident on the bottom. For a travel speed of 15 mm/min, heat input caused by friction increased as the rotation speed increased. The mechanical characteristics were degraded by accelerated softening due to increasing heat input.