• Polymer(Korea)
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• v.35 no.2
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• pp.113-118
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• 2011

Solid dispersion is used to improve the solubility of water-insoluble drug. Release properties depend on the characteristics of polymer and the physicochemical properties of solid dispersion. In this study the solid dispersions of ibuprofen and cellulose acetate were prepared using spray-drying and rotary evaporation. The physicochemical properties of the solid dispersions were analyzed by SEM, XRD, DSC, and FTIR. The hydrophilicity of polymer was analyzed by measuring the contact angle of water. The results of DSC and XRD analysis demonstrated that the crystallinity of ibuprofen was changed by solid dispersion preparation. The results of contact angle showed that hydrophilicity was proportional to polymer content. Release profile showed that for solid dispersion. the release rate of ibuprofen decreased as polymer content increased in intestinal juice (pH 6.8). The dissolution rate of ibuprofen was improved with increasing polymer content in gastric juice (pH 1.2).

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.6 no.4
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• pp.600-608
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• 1996

Specific structural properties of Li intercalation reaction into the spinel relatedmanganese dioxide, $Li_{x}Mn_{2}O_{4}(0.2{\leq}x{\leq}2.0)$, are investigated by X-ray diffractional and electrochemical studies of Li/1M $LiClO_{4}$-propylene carbonate solution/$Li_{x}Mn_{2}O_{4}$ cell. The effect of the chemical composition and the reaction temperature on electrochemical parameter of $Li_{x}Mn_{2}O_{4}$ are studied by the phenomena of phase-transition, analysis of crystal lattice, fine structure, and thermal analysis. Treatment of the spinel $Li_{x}Mn_{2}O_{4}$ with aqueous acid was found to result in conversiton of $Li_{x}Mn_{2}O_{4}$ to nearly pure $MnO_{2}$, as evidenced by a reduction in the lattice constant $a_{c}$ from 8.255 to $8.031\;{\AA}$. At a composition range of $0.2{\leq}x{\leq}0.6$ in $Li_{x}Mn_{2}O_{4}$ the reduction proceeded in a homogeneous phase, which was characterized by a constant voltage of 3.9~3.7 V together with a lattice constant of $8.255\;{\AA}$.

• Polymer(Korea)
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• v.33 no.4
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• pp.358-363
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• 2009

Maleic anhydride-grafted polypropylene has been widely used to improve the interfacial interaction between the components in PP/polar polymer blends and PP/filler composites and to maximize the physical properties and thermal properties. In this paper. the maleic anhydride (MAH)-grafted polypropylene (co-PP) was fabricated through reactive extrusion process with di-cumyl peroxide (DCP) as an initiator. The grafting degree of MAH depending on the contents of DCP and MAH was investigated by FT-IR spectra and chemical titration. The grafting degree increased with increasing MAH concentration and also showed maximum value at 0.06 wt% of DCP concentration. Melt flow index (MFI) of the grafted copolymer was increased with increasing the contents of MAH. The DSC and TGA analysis data indicate the melting temperature and thermal degradation of PP depending on the grafting degree of MAH.

• Journal of the Korea institute for structural maintenance and inspection
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• v.27 no.3
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• pp.30-37
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• 2023

The PSCB girder bridge is a closed cross-section in which the top and bottom flanges and the web are integrated, and the structural characteristics are generally different from the bridges in which the girder and the floor plate are separated, so a maintenance plan that reflects the characteristics of the PSCB girder bridge is required. As a result of analyzing damage types by collecting detailed safety diagnosis reports of highway PSCB girder bridges, most of the deterioration and damage occurring during use is concentrated on the top flange. In particular, cracks in the bridge direction on the underside of the top flange occurred in about 70 % of the PSCB girder bridges to be analyzed, and these cracks were judged to be caused by indirect loads such as heat of hydration and drying shrinkage rather than structural cracks caused by external loads. In order to improve durability and reduce maintenance costs of PSCB girder bridges in use, it is necessary to control restraint drying shrinkage cracks from the design stage. Therefore, in this paper, the cracks caused by drying shrinkage under restraint, which is the main cause of cracks under the flanges of the top part of the PSCB girder bridge, were directly calculated using the Gilbert Model, and the influencing factors such as the amount of reinforcing bars, diameter and spacing of reinforcing bars were analyzed. As a result of the analysis, it was found that the crack width caused by restraint drying shrinkage exceeded the allowable crack width of 0.2 mm for reinforcing bars with a reinforcing bar ratio of 0.01 or less based on the H16 reinforcing bar and a reinforcing bar with a diameter greater than H19 based on the reinforcing bar ratio of 0.01. Finally, based on the results of the crack width review, a method for controlling the crack width of the top flange of the PSCB girder bridge was proposed.

• Journal of the Korean Vacuum Society
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• v.10 no.3
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• pp.328-334
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• 2001

The characteristics of $NO/N_2O$ nitrided oxide and reoxidized nitrided oxide being studied as super thin gate oxide and gate dielectric layers of nonvolatile semiconductor memory(NVSM) was investigated by dynamic secondary ion mass spectrometry(D-SMS), time-of-flight secondary ion mass spectrometry(ToF-SIMS), and x-ray photoelectron spectroscopy (XPS). The specimen was annealed in $NO/N_2O$ ambient after initial oxide process. The result of D-SIMS exhibits that the center of nitrogen exists at the initial oxide interface and the distribution of nitrogen is wider in the annealing process with $N_2O$ than with NO annealing process. For investigating the condition of nitrogen that exists within the nitrided oxide, ToF-SIMS and XPS analysis were carried out. It was shown that the center of nitrogen investigated by D-SIMS was expected the SiON chemical bonds. The nitrogen near the newly formed reoxide/silicon substrate interface was appeared as $Si_2NO$ chemical bonds, and it is agreed with the distribution of SiN and $Si_2NO$ species by ToF-SIMS.

• The Transactions of the Korea Information Processing Society
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• v.6 no.1
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• pp.148-158
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• 1999

ABR traffic form ATM LAN is controlled through RM cell, and the interface function to public ATM network is necessary to provide ABR service efficiently. This paper presnets new interface architecture, which is based on "Projected Node" [6]. using AIPU(ABR Interface Proxy Unit) to support ABR traffic streams incoming from ATM LAN in the public ATM network. For the efficient interworking, the AIPU has designed for interworking functions with ERICA switch mechanism. Conventional ERICA switch mechanism specified in TM 4.0 is basically used for short distance comparative to public network, however AIPU adopts the novel control mechanism to cover logng roud trip time (RTT). To improve the problems and to provide a dynamic range of UCI(Update Count Interval), this paper proposes, a novel control scheme, DUCI ( Dynamic Update Count Interval. And the paper shows inefficiencies of ERICA mechanism with fixed UCI through the simulation results, and represents the performance enhancement of DUCI mechanism developed to adjust the update count interval dynamically.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.32 no.6A
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• pp.379-387
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• 2012

This study investigates free vibration characteristics of new energy harvesting multi-layer block structures with different geometrical shapes using solid and shell finite elements and evaluate their piezoelectric effect on experiments. The two and three-dimensional finite element (FE) delamination models for block structures described in this paper is attractive not only because it shows excellent accuracy in analysis but also it shows the entire vibration mode shape. The FE model using ABAQUS is used for studying free vibrations of multi-layer block structures for various tip mass and PZT. In particular, new results reported in this paper are focused on the significant effects of the global and local vibration modes for various parameters, such as size of block shape, existence of tip mass and hole, and location of tip mass and PZT. In addition, we evaluate the power generation capacity of developed energy block structures through a laboratory-scale experiment.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.37 no.1
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• pp.27-33
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• 2013

To ensure proper functioning of electrical and mechanical systems, cooling devices are of great importance. A heat sink is the most common cooling device used in many industries such as the semiconductor, electronic instrument, LED lighting, and automotive industries. To design an optimal heat sink, the required surface area for heat radiation should be calculated based on an accurate expectation of the heat flow rate in the target environment. In this study, the convective heat flow characteristics were numerically investigated for a vertically installed typical heat sink and a horizontally installed one in free convection using ANSYS CFX. Comparative experiments were carried out to reveal the quantitative effect of the installation direction on the cooling performance. Moreover, the result was analyzed using the dimensionless correlation with the Nusselt number and Rayleigh number and compared with well-known theories. Finally, it was observed that the cooling performance of the vertically installed heat sink is approximately 10~15% better than that of the one in natural convection.

• Analytical Science and Technology
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• v.14 no.3
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• pp.253-258
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• 2001

This is a research on hazardous characteristics and potentials of bottom ash from 9 municipal solid waste combustors(200 tons/day) of Korea by the test methods of leaching and content. The leaching method was performed by Waste Test Method of Korea. In case of the content method, mercury was determined by thermal decomposition amalgamation atomic absorption spectrometer, other 9 elemets including Pb, which were pretreated by U.S.EPA SW-846 3050B method, were determined by flame atomic absorption spectrometer(FAAS) or inductively coupled plasma atomic emission spectrometer(ICP-AES). Results of leaching test showed that Pb and Cu was main pollutants. It was interested that the distribution rate of metals' contents of each combustors was similar and the rank of concentration was Fe>Zn>Cu>Mn>Pb>Cr>As>Cd>Hg.

• Korean Journal of Ecology and Environment
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• v.37 no.2 s.107
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• pp.241-247
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• 2004

Isolation and identification of alga-lytic bacteria were carried out. Fifteen isolates of alga-lytic bacteria were screened by the double layer method using A. cylindrica NIES-19 as a sole nutrient and four isolates among them were compared with their alga-lytic activity. The isolate AK-05 exhibiting the highest alga-lytic activity was identified as Acidovorax temperans base on its 16S rDNA sequence. The culture supernatant of the isolate AK-05 was reliable for the alga-lytic. Alga-lytic activity assays of culture supernatant revealed that the major substances for alga-lytic activity were non-proteins and heat stable. The highest alga-Iytic activity was practical under alkaline conditions and at 25${\sim}$$30^{\circ}C$. It is indicating an advantage for the application of water blooms by cyanobacteria in eutrophic lakes where the pH is generally in alkaline region.