• Title/Summary/Keyword: 연속추출분석법

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The study on the Separation of Waste acid containing Acetic acid, Hydrofluoric acid and Nitric acid (초산, 불산 및 질산을 함유한 폐혼산의 분리 연구)

  • Kim, Jun-Young;Lee, Hyang-Sook;Shin, Chang-Hoon;Kim, Ju-Yup;Kim, Hyun-Sang;Ahn, Jae-Woo
    • Proceedings of the Korean Institute of Resources Recycling Conference
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    • 2006.05a
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    • pp.47-55
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    • 2006
  • Recovery of acids from the waste etching solution of containing nitric, hydrofluoric and acetic acid discharged from silicon wafer manufacturing process has been attempted by using solvent extraction method. With EHA (2-Ethylhexlalcohol) for acetic acid and TBP(Tri-butly Phosphate) for nitic and hydrofluoric acid as extraction agent was carried on experiment to obtain the process design data in separation procedure. From the McCabe-Thiele diagram analysis, we obtained the optimum conditions of phase ratio(O/A) and stages to separate the each acid sequently from the mixture acids. The recovery yield was obtained 90% above for acetic acid from the acid mixtures, 90% above for nitric acid from acetic acid extraction raffinate and then 67% above for hydrofluoric acid from final extraction raffinate.

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Localization of a mobile robot using the appearance-based approach (외향 기반 환경 인식을 사용한 이동 로봇의 위치인식 알고리즘)

  • 이희성;김은태
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.41 no.6
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    • pp.47-53
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    • 2004
  • This paper proposes an algerian for determining robot location using appearance-based paradigm. First, this algorithm compresses the image set using Principal Component Analysis(PCA) to obtain a low-dimensional subspace, called the eigenspace, and it makes a manifold that represent a continuous-appearance function. Neural network is employed to estimate the location of the mobile robot from the coefficients of the eigenspace. Then, Kalman filtering scheme is used for the fine estimation of the robot location. The algorithm has been implemented and tested on a mobile robot system. It is shown that the robot location is estimated accurately in several trials.

Chemical Speciation of Arsenic in the Water System from Some Abandoned Au-Ag Mines in Korea (국내 폐금은광산 주변 수계내의 As의 화학적 특성)

  • 이지민;이진수;전효택
    • Economic and Environmental Geology
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    • v.36 no.6
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    • pp.481-490
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    • 2003
  • The objectives of this study are (1) to determine the extent and degree of As contamination of the water and sediments influenced by mining activity of the abandoned Au-Ag mines, (2) to examine As speciation In contaminated water, (3) to monitor variation of As contamination in water system throughout the dry and wet seasons, and (4) to investigate the As chemical form in the sediments through the sequential extraction analyses. Natural water(mine water, surface water and groundwater) and sediments were collected in six abandoned Au-Ag mine(Au-bearing quartz veins) areas. The contamination level of As in mine water of the Dongil(524${\mu}m$/L) is more higher than the tolerance level(500 ${\mu}m$/L) for waste water of mine area in Korea. Elevated levels of As in stream water were also found in the Dongil(range of 63.7∼117.6 ${\mu}m$/L.) and Gubong(range of 56.1∼62.9 ${\mu}m$/L) mine areas. Arsenic contamination levels in groundwater used by drinking water were more significant in the Dongil(11.3∼63.5 ${\mu}m$/L), Okdong(0.2∼68.9 ${\mu}m$/L) and Gubong(2.0∼101.0${\mu}m$/L) mine areas. Arsenate[As(V), $H_2AsO_4^-$] is more dominant than arsenite[As(III), $H_3AsO_3$] in water system of the most mine areas. The concentration ratios of As(III) to As(total), however, extend to the 95% in stream water of the Okdong mine area and 70∼82% in groundwater of the Okdong and Dongjung mine areas. As a study of seasonal variation in the water system, relatively high levels of As from the dongil mine area were found in April rather than in September. Sequential extraction analysis showed that As was predominantly present as coprecipitated with Fe hydroxides from sediment samples of the Dongjung and Gubong mine(35.9∼40.5%), which indicates its possibility of re-extraction and inducing elevated contamination of As in the reductive condition. In sediments from the Dongil, Okdong and Hwachon mine area, high percentage(55.2∼83.4%) of As sulfide form was found.

Development of Surface Image Velocimetry with Space-Time Image Analysis (시공간 영상 분석을 이용한 영상 유속계의 개발)

  • Yu, Kwon-Kyu;Kim, Nam-Kil;Yoon, Byung-Man
    • Proceedings of the Korea Water Resources Association Conference
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    • 2010.05a
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    • pp.483-487
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    • 2010
  • 하천에서 물이 비교적 빠른 속도로 흘러가면 압력 변동, 하상의 조도, 하천내 구조물 등의 영향에 의해 수면이 끊임없이 변형을 일으키며 수면에 작은 물결(수면 파문)이 생긴다. 이러한 수면 파문은 유수에 의해 유수의 평균 유속으로 이류되며, 이 때문에 인간이 유수의 흐름을 시각적으로 인식할 수 있다. 이러한 표면 파문은 적절한 영상 분석을 하면 표면 유속 측정의 추적자로 이용할 수 있다. 본 연구는 유수 표면을 연속된 영상을 촬영하고, 일련의 영상을 시공간 영상(space-time image)으로 만든 뒤, 휘도 경사법(graylevel gradient method)으로 유속 벡터를 추출하는 새로운 방법을 제시하였다. 이 분석 과정은 기존의 입자 영상 유속계(PIV, Particle Image Velocimetry) 기법을 이용하는 방법보다 훨씬 간단하고 분석 시간도 크게 절약할 수 있다. 또한, 수면 파문의 전파에 따른 중력파의 영향을 시공간 영상의 처리 과정에서 잡음으로 간주하여 처리할 수 있다는 장점을 가지고 있다. 개발된 루틴을 표면 영상 유속계(SIV, Surface Image Velocimtery)에 구현하여 새로운 영상 유속계를 개발하였다. 시공간 영상 분속을 이용하는 새로운 영상 유속계를 실험실 수로의 영상 자료에 적용하여 그 정확도, 적용성, 장단점 등을 분석하였다. 제안된 방법에 의한 평균류 산정 결과는 물리적으로 타당하며, 저속 또는 저휘도에서의 분석 성능이 뛰어난 것으로 밝혀졌다. 다만, 이방향 흐름의 분석에서는 문제가 있는 것이 밝혀졌다.

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Classification of K-POP Dance Motion Using Multilinear PCA (다선형 PCA를 이용한 K-POP 댄스모션 분류)

  • Lee, Jae-Neung;Kwak, Keun-Chang
    • Proceedings of the Korea Information Processing Society Conference
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    • 2018.05a
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    • pp.486-487
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    • 2018
  • 본 논문에서는 다선형 PCA(Principal Component Analysis)를 이용한 키넥트 센서 기반 댄스 모션분류방법을 제안한다. 댄스 모션 분류를 수행하기 위해서, 먼저 키넥트 데이터 깊이 영상과 이진영상을 보간법을 통해 데이터의 크기를 정렬시켜준다. 다음으로 다선형 주성분 분석 기법 (MPCA)을 이용하여 연속된 댄스모션영상들에 대한 특징을 추출하고, 유클리디안 분류기를 통해 클래스 분류한다. 본 실험에 사용된 데이터베이스는 키넥트 센서를 기반으로 전문 댄서 4명을 통해 취득된다. 총 100곡의 K-POP을 선정하였고, 곡마다 2개의 포인트 안무를 통해 총 200개의 포인트 댄스모션 데이터베이스를 구축하였다. 실험결과 제안된 방법은 89.5%의 성능을 나타낸다.

Comparison of HRV Time and Frequency Domain Features for Myocardial Ischemia Detection (심근허혈검출을 위한 심박변이도의 시간과 주파수 영역에서의 특징 비교)

  • Tian, Xue-Wei;Zhang, Zhen-Xing;Lee, Sang-Hong;Lim, Joon-S.
    • The Journal of the Korea Contents Association
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    • v.11 no.3
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    • pp.271-280
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    • 2011
  • Heart Rate Variability (HRV) analysis is a convenient tool to assess Myocardial Ischemia (MI). The analysis methods of HRV can be divided into time domain and frequency domain analysis. This paper uses wavelet transform as frequency domain analysis in contrast to time domain analysis in short term HRV analysis. ST-T and normal episodes are collected from the European ST-T database and the MIT-BIH Normal Sinus Rhythm database, respectively. An episode can be divided into several segments, each of which is formed by 32 successive RR intervals. Eighteen HRV features are extracted from each segment by the time and frequency domain analysis. To diagnose MI, the Neural Network with Weighted Fuzzy Membership functions (NEWFM) is used with the extracted 18 features. The results show that the average accuracy from time and frequency domain features is 75.29% and 80.93%, respectively.

Aroma Components of Ookjook Tea (Polygonatum Involucratum Maxim) (옥죽차의 향기성분)

  • Choi, Sung-Hee;Baik, Young-Keun
    • Korean Journal of Food Science and Technology
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    • v.31 no.4
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    • pp.894-898
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    • 1999
  • Aroma components of Ookjook tea made from Polygonatum involucratum Maxim roots were collected and identified. The extraction of aroma compounds was accomplished by a simultaneous distillation and extraction method using a Likens and Nickerson's extraction apparatus. The concentrated extract was analyzed and identified by GC and GC-MS. The most abundant aroma components of this tea were furanic compounds including 2-furfural, 2-methyl-dihydro-3(2H)-furanone, 2-acetylfuran and 5-methylfurfural. These compounds seem to be originated from the thermal degradation of carbohydrates during the roasting process. Alkylpyrazines and acids including propionic acid increased slightly during the period of manufacturing process of Ookjook tea. Furanic compounds originated from the thermal degradation of carbohydrates and alkypyrazines from aminocarbonyl reaction seemed to be the important contributors to the aroma of the Ookjook tea.

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Properties of the Variation of Fe and Mn in the Vicinity of Soil Affected by Forest Fire for the Development of Technics that Reduces Forest Fire-induced 2nd Damage from Gangwon Provinces, Korea (2차산불피해저감기술개발을 위한 강원도 산불지토양 중 Fe-Mn원소의 분포특성)

  • 오근창;양동윤;김주영;남욱현;윤정한
    • Economic and Environmental Geology
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    • v.35 no.3
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    • pp.285-297
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    • 2002
  • This study was carried out to prove the factor properties of the soil affected by a forest fire through the physical and chemical analysis and the data from the conclusion of those analysis are applied to the development of technics that reduces a forest fire-induced 2nd damage. The forest fire was in December 2000 at Gangreung city and Donghae city, Gangwon provinces, Korea. Soil samples were collected at upper layers (0-5 cm) and bottom layers (5-40 cm) in November 2001 from the burned and control sites. Values of pH in burned soils of the upper layers affected by forest fire are higher than those in control soils. Both the fragments of fire-burned plant and differences of geological properties are resulted in a class of soil. Contents of organic matters in burned soils are higher than those in control soils, exceptionally the contents of organic matters in burned soils that contain coaly shale are lower than those in control soils. Weathering indices in burned soils are higher than those in control soils and it concerned with loss of soil. Iron ions Fe(Fe$^{2+}$ or Fe$^{3+}$) are easily extracted from the burned soils by rainfall, but Mn ions are straightly exist in the burned soils by physiochemical adsorption of colloid. Through the sequential extraction in the burned soils and control soils, we are certificate the extraction of Fe ions and the disturbance of Mn ions from the burned soils. As a consequence of factor analysis in burned soil and control soil, we are certificate that the influence of forest fire results in a disturbance of positive correlation factors.

Change in Flavor Components during Microwave Roasting of Cocoa Mass (Cocoa Mass의 마이크로파 Roasting 중 향기성분의 변화)

  • 이은정;윤상현;노희진;박덕철;김상용;정명섭;오상석;김석신
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.29 no.3
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    • pp.384-388
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    • 2000
  • 본 연구는 cocoa mass를 마이크로파 roasting하여 그 향기성분의 변화를 pyrazine류를 중심으로 살펴보는 한편 상법으로 roasting한 경우와 비교하고자 하였다. 마이크로파 roasting은 110,120,130,140,15$0^{\circ}C$의 온도에서 20분 및 30분 동안 행하였고 상법의 경우는 14$0^{\circ}C$에서 30분간 roasting하였다. Roasting한 시료를 연속수증기증류추출법으로 추출하고 농축한 후 GC와 GC/MS로 향기 성분을 분석하였다. 마이크로파 roasting의 경우 5분만에 14$0^{\circ}C$에 도달한 후 그 온도를 잘 유지하였으나, 상법의 경우 25분이 경과되어서야 14$0^{\circ}C$에 도달되었다. Roasting 한 시료의 향기성분으로 2,6-dimethyl pyrazine, 2,3,5-trimethyl pyrazine, 2,3,5,6-teramethyl pyrazine, 5-methyl fufural, 2-methyl-6-propyl pyrazine 등이 확인되었다. Roasting 온도가 증가함에 따라 dimethyl-, trimethyl-, tetramethyl pyrazine류가 증가하였고, tetramethyl pyrazine은 15$0^{\circ}C$ 20분 roasting의 경우 현저하게 증가하였으나, 30분 동안 roasting한 경우 14$0^{\circ}C$에서 증가하였다가 15$0^{\circ}C$일 때는 감소하였다. 그러나 적정 roasting 지표인 di/tri, di/tetra pyrazine의 비율은 1 이하를 보임으로써 마이크로파 roasting이 cocoa mass의 향기 발현에는 부족한 것으로 나타났다.

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A communicational approach to mathematical process appeared in a peer mentoring teaching method (학생 중심 동료 멘토링 교수법에서 수학적 과정에 대한 의사소통학적 접근)

  • Choi, Sang-Ho;Ha, Jeong-Mi;Kim, Dong-Joong
    • Communications of Mathematical Education
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    • v.30 no.3
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    • pp.375-392
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    • 2016
  • The purpose of this study is to provide a philosophical reflection on mathematical process consistently emphasized in our curriculum and to stress the importance of sharing creativity and its applicability to the mathematical process with the value of sharing and participation. For this purpose, we describe five stages of changing process in a peer mentoring teaching method conducted by a teacher who taught this method for 17 years with the goal of sharing creativity and examine components of mathematical process and their impact on it in each stage based on learning environment, learning process, and assessment. Results suggest that six principles should be underlined and considered for students to be actively involved in mathematical process. After analyzing changes in the five stages of the peer mentoring teaching method, the five principles scrutinized in mathematical process are the principles of continuous interactivity, contextual dependence, bidirectional development, teacher capability, and student participation. On the basis of these five principles, the principle of cooperative creativity is extracted from effective changes of mathematical process as a guiding force.