• Economic and Environmental Geology
• /
• v.56 no.2
• /
• pp.115-123
• /
• 2023

We introduce a new 'image-mapping' in-situ U-Pb dating method using LA-ICP-MS, proposed by Drost et al. (2018), and show the characteristics and usability of this method through several examples of absolute age results determined by first applying it to samples from the Joseon Supergroup of the Early Paleozoic Era in Korea. Unlike the previous in-situ spot analysis, this in-situ U-Pb dating method for carbonate minerals can determine the absolute age with high reliability by applying the 'image-mapping' method of micro-sized domains based on micro-textural observation, as well as determine the absolute age of multiple geological 'events' that occurred after deposition. This was confirmed in the case of determining the syn-depositional age and the multiple post-depositional ages from carbonate minerals of the Makgol and the Daegi Formations. Therefore, if the 'image-mapping' in-situ U-Pb dating method is applied to determine the absolute age of various types of carbonate minerals that exist in various geological environments throughout the geologic era, it will be possible to secure new geological age information.

• The Journal of the Petrological Society of Korea
• /
• v.10 no.3
• /
• pp.133-147
• /
• 2001

Recently developing method of age determination using stepwise dissolution technique to expand the applicability of absolute age determination significantly is evaluated whether it is applicable to the Korean samples. The materials selected for the study are uranium-bearing black slates from Changni Formation of Ogcheon metamorphic belt, tourmaline separated from Naedeongni granite of Yeongnam massif, garnet and ilmenite separated from ilmenite-bearing anorthositic rock of Yeongnam massif, scheelites from Ogbang mine, and magnetite separated from Gyemyeongsan Formation of Ogcheon metamorphic belt. For the stepwise dissolution, various acid steps with different normalities and different durations were applied to leach the samples. The leachate from each step was analyzed to determine the Pb isotopic composition and concentrations of Pb and U using thermal ionization mass spectrometer. The black slates from the Changni Formation and the tourmaline from the Naedeongni granite reveal significant variation of Pb isotopic composition, which reveals the potential of such stepwise dissolution technique as a dating method. The behaviors of uranium and lead during the each stage of step leaching are different, which seem to reflect the differences in positions within the crystal lattices depending upon mineral species.

• The Korean Journal of Quaternary Research
• /
• v.34 no.1
• /
• pp.31-40
• /
• 2024

The Risø Research Institute in Denmark conducted the luminescence dating intercomparison project, which derives equivalent dose, annual dose, and absolute age results for each laboratory from the same sample, and compares the results between laboratories. This project was carried out from 2006 to 2012. In this project, 30 international laboratories worldwide participated, including the luminescence laboratory at the Korea Institute of Geoscience and Mineral Resources (KIGAM). As a result of the project's synthesis, the average value of the results generally shows an over-dispersion value between laboratories of about 13%. The equivalent dose value obtained through the provided quartz analyzed in KIGAM shows results almost identical to the final equivalent dose value of the project. On the other hand, the equivalent dose value obtained from self-extracted quartz analyzed in KIGAM shows a difference of about 0.9 Gy from the final result of the project, which is thought to be due to the difference in particle size of the separated quartz. This international joint research project is the first large-scale international joint study related to luminescence dating and is expected to have contributed to the reliability and use of luminescence dating internationally.

• 대한방사선방어학회:학술대회논문집
• /
• 2011.11a
• /
• pp.296-297
• /
• 2011

• Analytical Science and Technology
• /
• v.22 no.2
• /
• pp.136-140
• /
• 2009

To improve the carbon recovery yield of chemical pretreatment in soil and sediment for $^{14}C$ age dating using AMS (Accelerator Mass Spectrometry), we have developed ultrasonic method in chemical pretreatment to replace with stirring method which has been generally used in each step of humic acid extraction for soil and sediment samples. Extraction conditions such as ultrasonic power, temperature and reaction time have been optimized. Six times higher carbon recovery yield could be obtained from low carbon content samples using ultrasonic method. We also compared the dating results by AMS obtained using ultrasonic method with the ages of samples treated by the stirring method. It was found that this new method could be applied to the pretreatment process of low carbon content samples for AMS age dating without effects on the dated ages, and with highly improved carbon recovery yields.

• Journal of Conservation Science
• /
• v.28 no.3
• /
• pp.185-192
• /
• 2012

Issues of chronology on archaeological remains or relics have been a storm-center of controversy when various archaeological researches have been done. Sometimes there is a limit for figuring out issues of chronology by archaeological research. In that case, the field of natural science is often needed to work out issues of chronology. Among various subjects in natural science, archaeomagnetism plays an important role in dating archaeological remains for baked earth bearing relics. In particular, archaeomagnetism is of use for sites where directly excavated dating proxy is unavailable. Terrestrial magnetism changes along with the passage of time and leaves trace by many kinds of residual magnetization which could be called fossil of terrestrial magnetism. Archaeomagnetic dating method is used to assign a date to the archaeological remains in which baked earth is found by measuring the changes of terrestrial magnetism through the thermal remanent magnetization retained in baked earth. This study aims to constrain the age of fire at Buinsa, Daege, Korea using 27 samples that were collected from a layer of baked earth. Buinsa is famous for the place where kept the first edition of Tripitaka Koreana, which was lost in fire at the second invasion of mongolia. In addition, there is a record that there was revolt around this region in A.D.1203. According to archaeomagnetic dating, ages of A.D.1150~1200 and A.D.1130~1210 were assigned for the two building sites in Buinsa, respectively. To this end, it can be concluded that the layer of baked earth on the two building sites in Buinsa recorded the vestige of fire caused by revolt.

• Journal of the Korean association of regional geographers
• /
• v.11 no.1
• /
• pp.114-122
• /
• 2005

To find out the buried age of the relict dune sediments, a luminescence dating bas conducted for a relict dune from the Sindu dunefield on the Taean Peninsula. It shows that the deposition of the dune sands at 3m depth began about 690$\sim$730 years ago. From 3m to l.5m depth, the lower part of the dune bas remained stable, but a relict dune deposit appear at 1.3m depth. This part yields an age of about 68 years. The two samples that were collected from the lower part of the dune at depths of the 1.5 m and 3.0 m below the surface show a net accumulation rate of around 0.75 cm/y which is relatively slow for a coastal dune. The chronology obtained in this study demonstrates that a significant amount of sediments has been replaced or remobilized in the area over the past 1000 years, and there was at least a soil formation process during the same time period. These suggest that a new approach is necessary to identify the formation age of the so-called paleo-dune at the Sind dunefield.

• Journal of Radiation Protection and Research
• /
• v.36 no.2
• /
• pp.52-58
• /
• 2011

OSL dating for three hearths having the sequence of use and discard in No. 29 and 29-1 dwelling sites at Sogol cultural site was carried out. Resulting from the deconvolution of natural CW-OSL decay curve and thermal zeroing test, it was turned out that OSL signal was entirely composed of the heat- and light-sensitive fast component with high photoionization cross-section and all quartz OSL signals were thermally bleached under $300^{\circ}C$ which is the minimum temperature related to heating and cooking in Bronze age. After dose recovery test and plateau test, paleodose of each hearth sample was evaluated by using SAR method, and OSL age was determined from the ratio of paleodose to annual dose rate. For the purpose of the precision improvement of OSL age, Bayesian statistics was applied to each hearth's age and the archaeological sequence information. Finally, it could be concluded to the accurate use period of each hearth from the resultant OSL ages.

• The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
• /
• v.7 no.1
• /
• pp.1-7
• /
• 2002

Optical dating, using infrared stimulation of K-feldspar grains, was undertaken to determine the sedimentation rate of a recently deposited tidal flat on the western coast of Korea. Very low luminescence of the natural surface sample confirms that the materials we investigated were well bleached at deposition. The five IRSL ages obtained show a reasonable stratigraphic correlation with the expected sedimentation rate of approximately 50cm/100yr. In addition the recuperation effect due to thermal transfer was discussed. We conclude that the optical dating used here shows a great promise to determine the sedimentation rates of tidal flats.

• Nuclear Engineering and Technology
• /
• v.15 no.1
• /
• pp.23-32
• /
• 1983

In the previous studies on Rb-Sr geochronology, Gyeonggi Massif was known as the oldest rock in Korea Peninsula but the detailed sequence of geochronology was not studied yet. In the present study, some of whole rock isochrons considered here can be geochronologically grouped as follows: The ages of leucocratic gneisses at Yangpyeong, and augen and banded gneisses at Anyang show 2200 to 2300 m.y. which may represent the time of the Massif formation or an igneous intrusion. The age of the granite gneiss distributed in Yangpyeong area shows about 1400 m.y., which apparently represents the intrusion time of the gneiss. The age of the extremely altered metamorphic rock shows about 500 m.y., which may represent the time of a Caledonian orogenic event probably with hydrothermal activities. The other episodic ages of 800 to 900 m.y. which was widely observed through the Massif, may represent the ages of Precambrian igneous activities or regional metamorphism in the Massif. It seems to be reasonable that the ages of 120 to 270 m.y. show the times of Mesozoic and Late Palaeozoic Plutonisms in the Massif.