• Proceedings of the Korean Fiber Society Conference
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• 1995.04a
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• pp.10-10
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• 1995

• Journal of Adhesion and Interface
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• v.10 no.4
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• pp.162-168
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• 2009

As a preliminary study of optimum composite properties under cryogenic temperature, the comparison of interfacial properties of carbon or glass fibers reinforced epoxy composites was evaluated at ambient and intermediate low temperature, i.e., 25 and $-10^{\circ}C$ by using micromechanical techniques. Under tensile and compressive loading conditions, their mechanical modulus at low temperature was higher than that atambient temperature. Interfacial shear strength (IFSS) at ambient and low temperatures was compared to each other, depending on epoxy matrix toughness and apparent modulus at the interface. The IFSS was much higher at low temperature than that at room temperature because of the increased epoxy matrix modulus. Statistical distributions of tensile strengths of glass and carbon fibers were evaluated for different temperature ranges, which is dependent upon fiber's inherent flaws and rigidity.

• Composites Research
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• v.19 no.4
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• pp.7-14
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• 2006

Interfacial shear strength between epoxy and carbon fiber has been analyzed utilizing the microbond specimen with an epoxy micro-droplet adhered onto single carbon fiber. The interfacial shear stress distributions along the fiber/matrix interface were calculated by finite element analysis using three kinds of finite element models such as droplet model, circular-crosssection model and pull-out model. Conclusions were obtained as follows. (1) Interfacial shear stress distribution showed that larger stresses were concentrated in the fiber/matrix interface for microbond test than for pull-out test. Thus, debonding at the fiber/matrix interface during microbond test was liable to occur at low load level. (2) Microbond test showed higher interfacial strength which was caused by various effects of micro-droplet geometry and size as well as stress concentration in the region contacting with the micro-vise tip.

• Composites Research
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• v.16 no.4
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• pp.74-79
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• 2003

Comparison of interfacial properties and microfailure mechanisms of oxygen-plasma treated poly(p-phenylene-2,6-benzobisoxazole(PBO. Zylon) and poly(p-phenylene terephthalamide)(PPTA, Kevlar) fibers/ epoxy composites were investigated using micromechanical technique and nondestructive acoustic emission(AE). Interfacial shear strength(IFSS) and work of adhesion, Wa of PBO or Kevlar fibers/epoxy composites increased by oxygen-plasma treatment. Plasma-treated Kevlar fiber shooed the maximum critical surface tension and polar term, whereas the untreated PBO fiber showed the minimum value. Microfibril fracture pattern of plasma-treated Kevlar fiber appeared obviously. Based on the propagation of microfibril failure toward core region. the number of AE events for plasma-treated PBO and Kevlar fibers increased significantly. The results oi nondestructive AE were consistent well with microfailure modes by optical observation in microdroplet and two-fiber composites tests.

• Journal of Power System Engineering
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• v.7 no.1
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• pp.25-33
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• 2003

섬유강화 복합재료의 계면 강도는 강화재와 메트릭스간의 계면특성, 강화용 섬유의 표면처리 및 섬유간의 거리 등에 많은 영향을 받는다. 본 연구에서는 섬유간의 거리가 섬유강화 복합재료의 계면특성에 미치는 영향을 고찰하기 위해, E glass fiber/epoxy 복합재료의 시험편을 제작하고, 섬유의 표면처리 및 섬유파괴가 이웃하는 섬유파괴에 영향을 미치는 거리에 대해 고찰하였다. E glass fiber/epoxy 복합재료의 계면 전단강도는 섬유간 거리 $0{\sim}50{\mu}m$ 사이에서는 섬유의 표면처리와는 관계없이 섬유간 거리가 증가할수록 증가하였고, 섬유간 거리 $50{\mu}m$ 이상에서는 섬유간거리에 관계없이 계면전단강도는 일정하였다.

• Composites Research
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• v.12 no.6
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• pp.53-64
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• 1999

Microstructural morphology and bending strengths of moulded composites of thermotropic liquid crystalline polymer(LCP) and polyamide 6 (PA6) have been studied as a function of epoxy fraction. Injection-moulding of a composite plaque at a temperature below the melting point of the LCP fibrils generated a multi-layered structure: the surface skin layer with thickness of $65\;-\;120{\mu\textrm{m}}$ exhibiting a transverse orientation; the sub-skin layer with an orientation in the flow direction; the core layer with arc-curved flow patterns. The plaques containing epoxy 4.8vol% exhibited superior bending strength and large fracture strain. With an increase of epoxy fraction equal to and beyond 4.8vol%, geometry of LCP domains was changed from fibrillar shape to lamella-like one, which caused a shear-mode fracture. An analysis of the bending strength of the composite plaques by using a symmetric layered model beam suggested that addition of epoxy component altered not only the microstructural geometry but also the elastic moduli and strengths of the respective layers.

• Polymer(Korea)
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• v.29 no.5
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• pp.481-485
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• 2005

In this work, the thermal and mechanical properties of vapor grown carbon nanofibers (VGCNFs)-reinforced difunctional epoxy (EP) composites were investigated in the presence of the 0, 0.1, 0.5, 1.0, and $2wt\%$ VGCNFs. The thermal properties of the VGCNFs/EP composites were studied by thermo-mechanical analysis (TMA) and dynamic mechanical analysis (DMA). The mechanical properties of the VGCNFs/EP composites were also examined by universal testing machine (UTM), falling impact test, and the friction and wear tests. From experimental results, the thermal and mechanical properties of the VGCNFs/EP composites were improved with increasing the VGCNFs contents. This was due to the increase of crosslinking structure of the composites, resulting in improving the mechanical interlockings between VGCNFs and epoxy resins in the present composite system.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1992.04a
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• pp.115-119
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• 1992

산업의 발전과 더불어 새로운 재료의 개발에 대한 요구가 날로 증가하고 있으며 이와 같은 요구에 부응하기위하여 각종의 신소재가 개발되고있다. 이들 신소재 중에서 섬유강화 복합재료는 높은 비탄성과 비강도특성 때문에 구조물의 경량화가 요구되는 우주선, 항공기 등에 주로 이용 되어 왔으며 최근에는 복합재료의 가격이 저렴해 지면서 이 재료의 높은 비탄성과 감쇠특성을 이용하고자 스포츠용품 및 기계 부품에도 섬유강화 복합재료의 이용이 증가 되고 있다. 항공기나 고속회전체의 부품을 복합재료로 제작하였을 경우 복합재료를 다른 금속이나 다른 복합재료부품에 접합(joining)시켜야 하는데 이 때문에구조물의 효율은 Joint에서 주로 죄우된다. Joint를 제작하기 위해서는 복합재료의 표면을 가공한 수 Adhesive를 이용하거나 Bolt로 체결하기 위해 구멍 뚫기 작업이 필요하여 드릴링을 하였을때 이 재료가 매우 연마성이 강하여 심한 공구마멸을 일으키며, 드릴의 입구와 출구쪽에서 각 ply들의 박리 현상이 발생하고, 드릴가공된 벽면으로부터 섬유 또는 레진의 탈락현상등이 발생하는 결점을 가지고 있다. 따라서 본 연구에서는 이러한 결점을 최소화하여 고정밀도의 높은 생산성을 얻기위한 가공기술에 대한 자료를 만들고 최적 절삭조건 및 복합재료가공용 드릴의 설계를 위한 지침을 제시하고자 고속도강 표준드릴을 사용하여 유리섬유 에폭시 복합재료및 탄소섬유 에폭시 복합재료의 드릴링 실험에서 절삭조건이 가공면 생성, 공구마멸, 절삭력에 미치는 영향에 대하여 조사하였다.

• Composites Research
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• v.28 no.1
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• pp.22-27
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• 2015

Although it is important to have high strength of each of fiber and matrix, interface between fiber and matrix is most important. If NaCl water penetrates the interface, that area will be weak. So experiment about increasing interfacial strength is in process. In this study, the change of properties by mechanical, interfacial and micromechanical tests was observed after NaCl and aging treatment. The changes in mechanical properties of glass fiber were investigated using single-fiber tensile test. Interfacial properties between glass fiber and epoxy resin were evaluated using nondestructive acoustic emission (AE) and micromechanical test applied to fatigue test. Through change of fatigue properties, relative interfacial properties were evaluate. In conclusion, glass fiber diameter decreased and the reduction of mechanical and interfacial was observed with NaCl solution and aging treatment.

• Journal of the Korean Applied Science and Technology
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• v.33 no.1
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• pp.168-175
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• 2016

The surface of glass fiber bundle was modified with functionalized silanes and phenolic resin to improve the tensile strength as well as the adhesion of glass fiber to matrix phenolic resin. The surface modification of reinforcing glass fiber can play a significant role in controlling whole composite characteristics. We applied surface modification of glass fiber with two different functionalized silanes, such as glycidyltrimethoxysilane(G-silane) and aminopropyltriethoxysilane (A-silane), and phenol formaldehyde(PF) resin in one pot or separated process under different coating compositions and temperatures. Thermal treatment temperature is very important factor to improve the mechanical properties of modified glass fiber. Modified glass fiber bundle treated at $170^{\circ}C$ showed the highest tensile strength of $10.05g_f/D$. Surface analyses by scanning electron microscope(SEM) and FT-IR spectroscopy were used to characterize the surface coatings on glass fiber bundles. Mechanical property changes as functions of treatment conditions and coupling agent types were also explained.