• Title/Summary/Keyword: 압축성형공정

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Development of Inorganic Binder Using Ash from Sewage Sludge Incinerator I (하수슬러지 소각재를 이용한 무기바인더 개발 I)

  • Lee, Hyun-Joo
    • Journal of Korean Society of Environmental Engineers
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    • v.36 no.12
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    • pp.843-850
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    • 2014
  • This study investigated to recycle ash produced in the sewage sludge incinerator using reduction/stabilization. Nonsintering process was performed by binding cement, geobond and sand mixed with sewage sludge ash (SSA). Results showed that unconfined compressive strength could be obtained components of sewage sludge ash. it exceeded more than double score of the 22.54 Mpa ($229.7kg/cm^2$) Korean standard. chemical ingradients of the sewage sludge ash was mainly composed of $SiO_2$, $Al_2O_3$, $Fe_2O_3$, CaO and others, which were similar to those of the each binders consisting cement and geobond. microstructure of solidified speceimen for the different admixture was related to the compressive strength according to SEM analysis. optimum mixing range of the sewage sludge ash to inorganic binder was found to be 10~40% which can widly safely regulate the confined compressive strength. This study revealed the sewage sludge ash can be partial replacement of the inorganic binder for recycling.

Study on the Microstructure and Mechanical Properties of High Volume Fraction TiB2-Al1050 Metal Matrix Composites (고체적률 TiB2-Al1050 금속복합재료의 미세조직 및 기계적 특성 연구)

  • Ko, Seongmin;Park, Hyeonjae;Lee, Yeong-Hwan;Shin, Sangmin;Lee, Donghyun;Jo, Ilguk;Lee, Sang-Bok;Lee, Sang-Kwan;Cho, Seungchan
    • Composites Research
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    • v.32 no.1
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    • pp.1-5
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    • 2019
  • In this study, Al1050 composites reinforced with uniformly dispersed, high volume fraction $TiB_2$ particles were fabricated by liquid pressing process and analyzed to microstructure, mechanical properties. Hardness, ultimate tensile strength and compressive yield strength of the 56 vol.% $TiB_2$-Al1050 composite increased to 10, 4.5 and 9.8 times, respectively, compared with those of the Al1050 due to dispersion hardening effect of uniformly dispersed $TiB_2$ in the Al matrix.

새로운quinolone계 항균제의 경구용제제화 연구

  • 이규현;윤두선;홍종호;홍지웅;심영기;전인구
    • Proceedings of the Korean Society of Applied Pharmacology
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    • 1994.04a
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    • pp.308-308
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    • 1994
  • 열분석 (DSC, TG/DTA)을 통해 Q-35는 A, B, C의 세가지 다형이 존재함을 알수 있었으며 이중 상대습도에 따른 흡습성의 변화가 적고, 가습에 의해 다형전환이 일어나지 않는 C형이 제제에 유리하다고 사료된다. 또한C형은 분쇄, 연합 및 타정에 의한 다형의 전환이 없었다. Q-35의 용해도는 물, 메탄올, 에탄올에 각각 0.30.3.55,6.31mg/m1 이었으며 PH5이상에서는 급격히 용해도가 감소하고 산성에서는 용해도가 크게 증가하는 양상을 나타냈다. 적층시험, 배합시험을 통해 선정한부형제의 표준 처방 혼합물로 정제를 저조한 결과Q-35의 성형성은 양호하였고 Q-35의 함량이 증가함에 따라 붕해시간이 다소 지 연됨을 알수 있었다. 그러나 Q-35원료는 유동성이 적어 직타법이 적합하지 않았으며, 습식 과립압축법에 따라 저조한 정제의 붕해시간은 5-9분, 15분 후 용출은 91.$\pm$5.0% 이었다. Q-35정제를 4$0^{\circ}C$, 4$0^{\circ}C$ ㆍ 75%RH에서 6개월, 6$0^{\circ}C$에서 3개월 보존후 함량을 측정한 결과 각각 100.0, 98.7, 98.9%이었으며 그밖의 항목에서도 안정한 결과를 얻어 Q-35정제는 온도 및 습도어 안정한 것으로 사료된다. 대량생산 연구결과 Q-35의 결정수가 이탈되지 않도록 건조, 코팅 공정 중 정제의 온도를 5$0^{\circ}C$ 이하로 유지시켰다.

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Hydrothermal Preparation of Artificial Stone Plate from Stone Powder Sludge (수열양생법에 의한 석분 슬러지로부터 인조석판재의 제조)

  • 김치권;배광현
    • Korean Journal of Crystallography
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    • v.12 no.4
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    • pp.216-221
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    • 2001
  • Artificial stone plates were hydrothermally prepared in order to utilize the stone powder sludge which were generated from stone quarry . Calcium hydroxide and silica were added to sludge of which main phases were quartz and alumina, and the effect of vapour pressure, reaction time and added amount on the properties of plates were investigated. The compressive strength, water absorp-tion and apparent specific gravity of the plates, which were prepared from the mixture of 70% stone sludge, 20% calcium hydroxide and 10% silica for 3 hours at the conditions of pressing pressure of 200kg/㎠ and vapour pressure of 20 kg/㎠, were 614kg/㎠, 0.48%, 1.88 respectively. It was also possible to produce various colours and appearances by adding inorganic pigments.

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Extrusion Process Analysis of Al/Cu Clad Composite Materials by Finite Element Method (유한요소법을 이용한 Al/Cu 층상복합재료의 압출공정해석)

  • 김정인;강충길;권혁천
    • Composites Research
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    • v.12 no.5
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    • pp.87-97
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    • 1999
  • A clad material is a different type of the typical composites which are composed of two or more matericals joined at their interface surface. The advantge of cald material is that the combination of different materials can satisfy both the need of good mechanical properties and the other demand of user such as electrical properties instantaneously. This paper is concerned with the direct and indirect extrusion processes of copper-clad aluminum rod. Extrusion of copper-clad aluminum rod was simulated using a commercially available finite element package of DEFORM. The simulations were performed for copperclad aluminum rod to predict the distributions of temperature, effective stress, effective strain rate and mean stress for sheath thicknesses, die exit diameters and die temperatures.

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Development of a CAE Tool for P/M Compaction Process and Its Application (금형압축성형공정 해석용 CAE 프로그램 개발 및 적용)

  • Chung Suk-Hwan;Kwon Young-Sam
    • Journal of Powder Materials
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    • v.11 no.5
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    • pp.399-411
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    • 2004
  • Crack generation during die compaction and distortion during sintering have been critical problems for the conventional pressing and sintering process. Until now, trial and error approach with engineers' industrial experiences has been only solution to protect the crack generation and distortion. However, with complexity in shape and process it is very difficult to design process conditions without CAE analysis. We developed the exclusive CAE software (PMsolver/Compaction) for die compaction process. The accuracy of PMsolver is verified by comparing the finite element simulation results with experimental results. The simplified procedures to find material properties are proposed and verified with iron based powder and tungsten carbide powder. Based on the accurate simulation result by PMsolver, the optimal process conditions are designed to get uniform density distribution in a powder compact after die compaction process by using a derivative based optimization scheme. In addition, the effect of non-uniform density distribution in a powder compact on distortion during sintering is shown in case of the fabrication of tungsten carbide insert.

Compression D/B for Liquid Segregation Control in Semi-Solid Forming Process and Its Application (반용융 성형공정에 있어서 액상편석제어를 위한 압축 D/B 및 응용)

  • 정경득
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.06a
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    • pp.15-32
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    • 1999
  • A relationship between stress and stain is very important to design a die to avoid defects of products during semi-solid forming process. Since the liquid will be of eutectic composition in alloys liquid segregation will result in significant or undesirable situation. The materials used in this experiment are A 357. A390, Al2024 alloys that is fabricated by the electro-magnetic stirring process from Pechiney in France. The compression test was performed by induction heating equipment and MTS. In order to prevent the liquid segregation these measured temperature would be useful to control of strain rate during compression test. The liquid segregation is controlled as change of the strain rate and solid fraction during the compression process, The characteristics of flow between solid and liquid phase considering liquid segregation is examined through the above experiments. In the case of medium and high volume fractions of solid the distribution of strain rate is calculated by using compression test data of semi-solid materials (SSM). The thixoforming experiments with the designed die are carried out successfully. The die filling patterns of SSM for variation of die temperature and pressing force have been investigated. The hardness of the thixoformed scroll products is evaluated in terms of the microstructure for each position.

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Influence of Alkali or Silane Treatment of Waste Wool Fiber on the Mechanical Properties and Impact Strength of Waste Wool/Polypropylene Composites (폐양모/폴리프로필렌 복합재료의 기계적 특성 및 충격강도에 미치는 폐양모섬유의 알칼리처리 또는 실란처리 영향)

  • Kim, Kihyun;Cho, Donghwan
    • Journal of Adhesion and Interface
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    • v.18 no.3
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    • pp.118-126
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    • 2017
  • In a natural fiber-reinforced composite material, many studies have been devoted to improving the interfacial adhesion between natural fiber and polymer matrix and the composite properties through various fiber surface modifications. In the present study, waste wool-reinforced polypropylene matrix composites were fabricated by compression molding and their mechanical and impact properties were characterized. As a result, the tensile and flexural properties and the impact strength of waste wool/polypropylene composites strongly depended on the treatment medium, alkali treatment with sodium hydroxide (NaOH) and silane treatment with 3-glycidylpropylsilane(GPS). The composite with waste wool by silane treatment exhibited higher mechanical properties and impact resistance than that by alkali treatment. The fracture surfaces of the composites support qualitatively the increased properties, showing the improved interfacial bonding between the waste wool and the polypropylene matrix.

A Study on the Isotropic Nd$_2$Fe$_{14}$B/Epoxy Bonded Magnets with High Characteristics (고특성 등방성 Nd$_2$Fe$_{14}$B/에폭시 본드자석의 연구)

  • 조태식;정원용
    • Polymer(Korea)
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    • v.26 no.1
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    • pp.98-104
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    • 2002
  • This study was investigated to fabricate the isotropic $Nd_2Fe_{14}B$/epoxy bonded magnets with high characteristics paroduced by compression molding. The magnetic characteristics of the bonded magnets were directly proportional to the density of the magnets and were enhanced by using raw $Nd_2Fe_{14}B$ magnetic powders, having the mean particle size of $200{\mu} m$.without additional milling process. The high characteristics of the bonded magnets were achieved at the following conditions: epoxy resin of 2.0 wt%, silane coupling agent of 0.8 wt%, curing agent of 0.7 wt% on the base of magnetic powders, and curing condition of $150^{\circ}C$/3 hrs. The bonded magnets at the optimum conditions indicated the high characteristics such as the density of 6.1 g/㎤, the remanent flux density of 7.1 kG, the maximum energy product of 9.7 MGOe, and the compressive strength of 17 kg/$mm^2$.

Adsorption Performance of Basic Gas over Pellet-type Adsorbents Prepared from Water Treatment Sludge (정수장 슬러지로부터 제조한 입상흡착제의 염기성 가스 흡착 성능)

  • Bae, Junghyun;Park, Nayoung;Lee, Choul Ho;Park, Young-Kwon;Jeon, Jong-Ki
    • Korean Chemical Engineering Research
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    • v.51 no.3
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    • pp.352-357
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    • 2013
  • In this study, the pellet-type adsorbents were prepared by extrusion using water treatment sludge. Effects of binder and calcination on physical and chemical properties of pellet-type adsorbents were investigated. The porous structure and surface characteristics of the adsorbents were studied using nitrogen adsorption, compression strength, scanning electron microscope, X-ray diffraction, and infrared spectroscopy of adsorbed pyridine. With increasing of binder content to 5 wt%, the compressive strength of pellet-type adsorbent could be improved more than three times, but the surface area reduced by 30%, and thus the breakthrough time of trimethylamine was shortened. The breakthrough time of the trimethylamine, a basic gas, could be increased more than three times through calcination, which seems to be due to generation of acid sites composed of Lewis acid and Br$\ddot{o}$nsted acid sites on the adsorbent surface.