• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.9
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• pp.943-951
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• 2014

The tip geometries of the pyramidal and conical indenters used for micro/nano-indentation tests are not sharp. They are inevitably rounded because of their manufacturability and wear. In many indentation studies, the tip geometries of the pyramidal indenters are simply assumed to be spherical, and the theoretical solution for spherical indentation is simply applied to the geometry at a shallow indentation depth. This assumption, however, has two problems. First, the accuracy of the theoretical solution depends on the material properties and indenter shape. Second, the actual shapes of pyramidal indenter tips are not perfectly spherical. Hence, we consider the effects of these two problems on indentation tests via finite element analysis. We first show the relationship between the Poisson's ratio and load-displacement curve for spherical indentation, and suggest improved solutions. Then, using a possible geometry for a Berkovich indenter tip, we analyze the characteristics of the load-displacement curve with respect to the indentation depth.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.12
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• pp.1453-1463
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• 2013

In this study, we investigated the effect of the indenter geometry on the crack characteristics by indentation cracking test and FEA. We conducted various cohesive finite element simulations based on the findings of Lee et al. (2012), who examined the effect of cohesive model parameters on crack size and formulated conditions for crack initiation and propagation. First, we verified the FE model through comparisons with experimental results that were obtained from Berkovich and Vickers indentations. We observed whether nonsymmetrical cracks formed beneath the surface during Berkovich indentation via FEA. Finally, we examined the relation between the crack size and the number of cracks. Based on this relation and the effect of the indenter angle on the crack size, we can predict from the crack size obtained with an indenter of one shape (such as Berkovich or Vickers) the crack size for an indenter of different shape.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.2
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• pp.129-137
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• 2013

A force calibration of a nanoindenter and a 3D morphology observation of indenters were carried out in this study. A microbalance calibrated with standard weights was used for measuring the loads generated by a nanoindenter. The indentation load could be calibrated from the ratio of measured and generated loads and the first contact load also could be detected from the microbalance data. By analyzing atomic force microscopy images of two indenters, curvature radii of apexes were determined by $19.71{\pm}3.03$ and $1043.94{\pm}50.91$ nm, respectively, for the nearly new indenter A and the severly worn indenter B. Corresponding bluntness depths were estimated by 1.22 and 64.56 nm for the both indenters by overlapping their profiles on the perfect pyramidal shape. In addition, nanoindentation curves obtained from a fused silica reference material with the both indenters showed a depth difference corresponding to the bluntness depth difference along the indentation depth axis. By shifting amounts of the bluntness depths along the horizontal axis, whole nanoindentation curves overlapped on themselves and resulted in nanohardness values consistent within 1.11 % without considering the complex indenter area function of each indenter.

• Proceedings of the Korean Reliability Society Conference
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• 2011.06a
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• pp.125-130
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• 2011

발전 설비는 기대 수명동안의 안정성을 확보하기 위하여 해당 규격에 부합하도록 설계하여 건설된다. 하지만 가동 중 다양한 복합 환경에 노출됨에 따라 구조물을 이루고 있는 재료의 열화 현상이 가속화되어 예기치 못한 파손이 발생할 수 있다. 기계적 물성은 재료의 기계적 거동을 나타내는 주요 척도가 되며 이는 신뢰성 및 안전과 직결된다. 하지만 기존의 역학물성을 측정하는 대부분의 시험법들은 특정 크기의 시편을 요구하고 파괴적인 시험법이기 때문에 가동 중 시설물에 적용하기가 불가능하였다. 이러한 한계점을 극복하고자 비파괴적이고 정량적인 시험이 가능한 연속압입시험법이 최근 각광받는 시험법으로서 많은 연구자들에 의해 연구되고 있다. 이 시험법은 시험 대상물의 형상에 제약을 받지 않으며 시험 절차가 매우 간단하다는 장점을 가진다. 또한 대상의 국소 부위에 시험할 수 있어 취약 부위 판별이 가능하다. 본 연구에서는 대표응력-대표변형률 기법을 통하여 인장물성을 평가하고, 압입 하중 차이를 이용하여 소재에 존재하는 잔류응력을 평가하는 기법을 소개한다. 또한, 연속압입시험을 이용하여 실제 발전소 파이프의 취약부위로 알려진 용접부에 대하여 인장물성 및 잔류응력을 측정함으로써 실제 산업체의 신뢰성 평가가 적용할 수 있음을 확인하였다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.1
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• pp.81-90
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• 2012

The indentation test, which is one of the testing methods for evaluating the mechanical properties of materials, can be applied to the evaluation of creep properties. Many studies related to the indentation creep test, however, have just focused on the characteristics of the steady-state creep, so there are wide discrepancies between the uniaxial test and the indentation test. To obtain accurate creep properties, it is therefore important to consider the effects of transient creep. In the present work, the Ogbonna et al.'s work on the spherical indentation test including the transient creep was expanded and applied to the conical indentation creep test. The characteristics of the transient creep were analyzed via finite element simulations and compared with those obtained through spherical indentation. Other effects, such as elastic strain, indenter shape, contact area, and representative strain, which have not been considered properly in prior studies on the creep test, are also discussed.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.9
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• pp.1081-1086
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• 2012

This study deals with hardness evaluation for spot welding by using an instrumented indentation technique to improve the quality of the inspection methodology. First, an instrumented indentation test and a Rockwell hardness test were performed for normal and abnormal spot welding. The hardness to indentation force-displacement curve obtained using each of the tests was compared. Furthermore, an analysis was conducted using the hardness obtained by the instrumented indentation technique. A quality control standard based on reliability was this evaluated for spot welding.

• Composites Research
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• v.22 no.2
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• pp.24-29
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• 2009

This study aims to investigate the residual strength of sandwich composites with Al honeycomb core and carbon fiber face sheets after the quasi-static indentation damage by the experimental investigation. The 3-point bending test and the edge-wise compressive strength test were used to find the mechanical properties, and the quasi-static point load was applied to introduce the simulated damage on the specimen. The damaged specimens were finally assessed by the 3-point bending test and the compressive strength test. The investigation results revealed the residual strength of the damaged specimens due to the quasi-static indentation. The both test results showed that the residual strength of the damaged specimen was decreased according to increases of the damaged depth.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.244-244
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• 2003

나노인덴테이션은 시편에 압자를 침투시켜 재료의 기계적 특성을 파악할 수 있는 경도시험법이다. 압입범위를 나노미터범위로 조절할 수 있어 기존에 접근할 수 없었던 극 미소부분에로 응용이 넓어지고 있다. 경도시험시 재료의 탄성 및 소성 작용에 의해 재료는 변형되고, 표면변화 관찰을 통해 표면아래 부분에서 이루어지고 있는 거동을 예측할 수 있다. 이러한 관점에서 나노인덴테이션 시험시에도 발생하는 파일업과 싱크인 현상에서 재료가 나노미터 범위에서 어떠한 양상으로 변형을 하는지를 고찰하는 것은 의미가 있을 것이다. 본 연구에서 파일업과 싱크인의 양상을 파악하고 그 양을 정량화하기 위하여 가공경화양에 따른 표면변화와 압입하중 변화에 따른 표면변화를 관찰하였다. 어닐링한 봉상 알루미늄을 압축변형을 0%, 5%, 20%, 40%, 50% 로 변형시켜 가공경화를 일으켰고, 표면은 전해연마하여 나노압입시험이 가능하도록 하였다. 각각의 시편을 나노인덴테이션 압입하중을 변화시켜 재료에서 하중 변화에 따라 나타나는 표면변화를 관찰하였고, 위의 각 조건에서 파일업양을 정량화 하였다. 연구결과에 대해 ANSYS 유한요소분석 프로그램을 사용하여 재료의 변형양상을 시뮬레이션 하였고, 실제 실험데이터와 비교 분석하였다.

• Journal of the Korean Society for Nondestructive Testing
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• v.26 no.5
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• pp.306-314
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• 2006

Instrumented indentation technique is a new way to evaluate nondestructive such mechanical properties as flow properties, residual stress and fracture toughness by analyzing indentation load-depth curves. This study evaluated quantitatively the flow properties of steels and residual stress of weldments. First, flow properties can be evaluated by defining a representative stress and strain from analysis of deformation behavior beneath the rigid spherical indenter and the parameters obtained from instrumented indentation tests. For estimating residual stress, the deviatoric-stress part of the residual stress affects the indentation load-depth curve, so that by analyzing the difference between the residual-stress-induced indentation curve and residual-stress-free curve, the quantitative residual stress of the target region can be evaluated. The algorithm for flow property evaluation was verified by comparison with uniaxial tensile test and the residual stress evaluation model was compared to mechanical cutting and ED-XRD results.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.2
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• pp.158-162
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• 2004

Reliability of welded structures in power plant facilities is very important, and their reliability evaluation requires exact materials properties. But, the conventional PQR (Procedure Qualification Record) can hardly reflect the real material properties in the field because the test is only done on specimens with simulated welding. Therefore, a continuous indentation technique is proposed in this study for simple and non-destructive testing of in-field structures. This test measures the indentation load-depth curve during indentation and analyzes the mechanical properties such as the yield strength, tensile strength and work hardening index. This technique has been applied to evaluate the tensile properties of the weldment in the main steam pipe and hot reheater pipe in power plants under construction and in operation.