• Journal of the Korean Society of Manufacturing Process Engineers
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• v.12 no.6
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• pp.3-9
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• 2013

Aluminum Oxide($Al_2O_3$) ceramics are excellent candidates for such applications due to their outstanding mechanical, thermal, and tribological properties. However, they are difficult to machine using conventional mechanical methods. Carbon fillers, such as carbon nanotubes(CNT) and graphene nanoplatelets(GNP)can be dispersed in a ceramic matrix to improve the mechanical and electrical properties. In this study, CNT and Graphene reinforced hybrid ceramic composites were fabricated using the spark plasma sintering method at a temperature of $1,500^{\circ}C$, pressure of 40 MPa, and soaking time of 10min. Besides this, the material properties such as microstructure, crystal structure, hardness, and electrical conductivity were analyzed using FE-SEM, XRD, Vickers, and the 4-point probe method. A micro machining test was carried out to compare the effects of the material properties and the machining performance for CNT and Graphene reinforced ceramic composites.

• Tribology and Lubricants
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• v.24 no.5
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• pp.269-274
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• 2008

Carbon nanotube composite is considered to be a good candidate material for composite material because of its excellent mechanical property and low density under high temperature as well as good wear and frictional properties. In this study, tribological characteristics of carbon nanotube aluminum composite were evaluated using pin-on-disk wear tester. Spark Plasma Sintering method is more effective than Hot Pressing method in terms of wear and friction. The composite with 1% CNT has the lowest friction and wear characteristic.

• Journal of the KSME
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• v.35 no.9
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• pp.816-828
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• 1995

냉동공조용 열교환기의 종류, 특징, 기술개발 동향, 전망 등에 대해 요약한 결과를 정리하면 다 음과 같다. (1) 암모니아 냉매가 다시 각광을 받음에 따라 응축기의 형식도 크게 변하고 있다. 이러한 변화로 핀 튜브를 사용한 횡형, 금속용착형 플레이트 식, 플레이트 핀 식의 응축기들이 암모니아 용으로 적용되기 시작하고 있다. (2) 암모니아 냉동장치는 현재에도 많이 적용되고 있으나 대부분 중앙 집중식 천정증발기나 강관 제 유닛 쿨러를 사용하고 있다. 그러나 최근 기술의 발전과 더불어 알루미늄 관 알루미늄 핀 증발기가 개발됨에 따라 암모니아 냉매도 프레온 냉매와 마찬가지로 건식, 분산식으로 적용되게 되었으며 이 분야의 기술개발이 요청된다. (3) 열교환기의 연구 방향은 에너지 절약, 공간 절약에 기여하면서도 성능향상을 이룩할 수 있는 기술개발, 그리고 소음이 적은 기기 제조 기술이 요망된다. 또한, 착상에 대한 기술적 대책, 근 본적 대책에 대한 대비가 요망되며, 기존 냉매에 대한 대체 냉매용 최적 열교환기에 대한 적극적 연구가 요망된다. (4) 제한된 에너지 자원, 지구환경, 열악한 우리나라의 에너지 사정 등을 고려할 때 냉동공조용 열교환기의 성능 향상에 대한 국가와 일반 소비자들의 기대는 더욱 증가하리라 예상된다. 이들 요구를 만족시키기 위해서는 냉동공조용 열교환기의 성능 향상, 열교환기의 제작에 필요한 자 원의 절약, 생산성 향상, 설치장소와 관련한 효율적인 공간활용, 열교환기 자체 소음의 최소화 등의 방면에 착실한 연구 개발이 있어야 할 것이다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.11
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• pp.1010-1015
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• 2008

In this study, the characteristics of aluminum tube hydroformed products at different extrusion type and heat treatment conditions were investigated. For the investigation, as-extruded, full annealed and T6-treated Al 6061 tubes at different extrusion type were prepared. To evaluate the hydroformability, free bulge test was performed at room temperature to $300^{\circ}C$. Also mechanical properties of hydroformed products at various pre- and post-heat treatments were estimated by hexagonal prototype hydroforming test at $250^{\circ}C$. And the tensile test specimens were obtained from hexagonal prototype hydroformed tube. As a results, hydroformability of full annealed tube is $5{\sim}8%$ higher than that of extruded and T6-treated tube. The tensile strength and elongation of T6-post heat treated indirect extrusion tube were more than 330MPa and 12%, respectively. However, T6 pre treated hydroformed product represents high strength, 330MPa and low elongation, 8%. Therefore, Hydroformability of Al6061 tube showed similar value for both extrusion types. However flow stress of direct tube showed $20{\sim}50MPa$ lower value than indirect tube.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.17 no.2
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• pp.127-137
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• 2019

Zr electrorefining is demonstrated herein using Zirlo tubes in a chloride-fluoride mixed molten salt in the presence of $AlF_3$. Cyclic voltammetry reveals a monotonic shift in the onset of metal reduction kinetics towards positive potential and an increase in intensity of the additional peaks associated with Zr-Al alloy formation with increasing $AlF_3$ concentration. Unlike the galvanostatic deposition mode, a radial plate-type Zr growth is evident at the top surface of the salt during Zr electrorefining at a constant potential of -1.2 V. The diameter of the plate-type Zr deposit gradually increases with increasing $AlF_3$ concentration. Scanning electron microscopy-energy-dispersive X-ray spectroscopy (SEM-EDX) and X-ray photoelectron spectroscopy (XPS) analyses for the plate-type Zr deposit show that trace amount of Al is incorporated as Zr-Al alloys with different chemical compositions between the top and bottom surface of the deposit. Addition of $AlF_3$ is effective in lowering the residual salt content in the deposit and in improving the current efficiency for Zr recovery.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2016.11a
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• pp.185-185
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• 2016

아크릴계 수지(resin)에 인조 흑연과 탄소나노튜브(carbon nanotube)를 1:1 비율로 혼합한 충전제(filler)와 용제(solvent) 및 기타 첨가제(additives)를 혼합하여 방열도료를 제조하여 수직방향 열전도도를 상온에서 평가하였다. 충전제의 함량을 1, 2, 5 중량 %로 변화시키며 원료들을 준비하여 교반기로 혼합한 뒤 3단 롤 밀(three roll mill)로 분산공정을 진행하여 3 종류의 도료를 제조하였다. 제조한 도료를 가로 11 mm, 세로 11 mm, 두께 0.4 mm의 Al 5052 알루미늄 기판에 스프레이 코팅 방식으로 도포한 후 $150^{\circ}C$에서 30분 동안 열경화 건조 과정을 거쳐 샘플을 제작하였다. 측정 시료의 형상은 대략적으로 Fig. 1과 같다. 열전도도는 식 $k={\alpha}{\cdot}C_p{\cdot}{\rho}$를 사용해서 계산된다. 여기서 k는 열전도도($W/m{\cdot}K$), ${\alpha}$는 열확산계수($mm^2/s$), $C_p$는 비열($J/kg{\cdot}K$), ${\rho}$는 밀도($g/cm^3$)를 나타낸다. 열확산계수는 독일 NETZSCH 사의 Laser Flash Analysis 장비(모델명 LFA 457)를 사용하여 측정하였는데, 기판 뒤쪽에서 레이저를 조사하고 도료층 전면에서 적외선 온도센서를 통해 시간에 따른 온도 상승곡선을 구한 후, 두 물체의 계면에서의 접촉 열저항(contact thermal resistance)을 감안하여 장비에 내장되어 있는 소프트웨어로 열확산계수가 계산된다. 비열은 같은 회사의 DSC(Differential Scanning Calorimetry) 200 F3 장비를 사용해 측정했으며, 밀도는 부피와 질량을 측정한 값을 이용하여 계산하였다. 도료를 도포하지 않은 bare Al plate에 대해서는 쉽게 열확산계수, 비열, 밀도를 측정하여 열전도도를 구할 수 있다. 도료가 코팅된 샘플에 대해서는 도료층을 일부 떼어내 비열을 측정하고, 밀도를 구한 후, 도료층의 열전도도가 2-layer 법으로 장비 내장 소프트웨어로 계산된다, 이때 Al 기판의 열확산계수, 비열, 밀도는 미리 측정한 bare Al plate의 값을 적용하였다. 실험 결과를 Table 1에 정리하였다. 흑연과 탄소나노튜브를 혼합한 충전제를 함유한 아크릴 복합체 박막에서 측정된 열전도도는 보통 고분자 재료의 열전도도 값의 상한 영역에 육박하는 값이며, 충전제 함량이 증가할수록 열전도도가 증가하는 경향을 보이고 있다.

• Journal of the Korean Vacuum Society
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• v.16 no.5
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• pp.377-382
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• 2007

In this study, we report the synthesis of the single-walled carbon nanotubes(SWCNTs) using laminated catalyst(Al/Fe/Al) layer deposited by sputter on Si(001). SWCNTs are grown by thermal chemical vapor deposition (TCVD) method. As the results of scanning electron microscopy(SEM), high resolution transmission electron microscopy(HR-TEM) and Raman spectroscopy, we confirmed the SWCNTs bundles with narrow diameter distribution of $1.14{\sim}1.32\;nm$ and average G&D ratio of 22.76. Compare to the sample having Fe/Al catalyst layer, it can be proposed that the top-aluminum incorporated with iron catalyst plays an important role in growing process of CNTs as a agglomeration barrier of the Fe catalyst. Thus, we suggest that a proper quantity of aluminium metal incorporated in Fe catalyst induce small and uniform iron catalysts causing SWCNTs with narrow diameter distribution.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.314-317
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• 2007

Automotive rear subframe of aluminum tube was developed by using hydroforming process, based on the numerical analysis and physical tryouts. In the previous study, the effect of prebending was evaluated on the basis of forming limit diagram which had been obtained from free bulging, T-shape forming and cross-shape forming, using the developed tube hydroformability testing system. In order to get the sound products, appropriate internal pressure is to be imposed corresponding to the axial feeding. In this study, the loading path, the combination of internal pressure and axial feeding during the process, was optimized to ensure minimum thickness variation and dimensional accuracy, by using response surface method.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.364-367
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• 2001

Recently social demands of fuel economy and environmental regulation require the development of light materials and new manufacturing technologies. In this point, aluminum tube hydroforming, which is satisfied with good strength-to-weight ratio and recyclability, is new innovative concept. but, up to now the level of that is relatively low. In this paper, we studied formability of different aluminum tubes in different heat treatments under internal pressure and axial feeding, and mechanical properties of aluminum tubes before and after hydroforming.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.198-201
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• 2004

Aluminum alloys have high potential for weight reduction in automotive and other applications. But aluminum alloys have relatively low tubular hydroformability which can be enhanced by conducting the hydroforming at elevated temperatures. Hot working processes are commonly used in bulk forming such as forging and rolling, but still is rare in sheet metal forming like hydroforming. In this study hydroforming test at elevated temperatures is performed by special designed induction heating system to investigate the hydroformability of aluminum alloys. The high temperature formability characteristrics are obtained by 1?fitting forming test and circular bulging test and the effects of the process parameters such as feeding amount, internal pressure and temperatures on the tubular forming limits are mainly investigated.