• Title/Summary/Keyword: 알루미나 세라믹

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졸-겔 법에 의한 알루미나 한외여과막의 제조 및 특성에 관한 연구

  • 최양희;김은옥;최재호;이용택
    • Proceedings of the Membrane Society of Korea Conference
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    • 1991.04a
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    • pp.40-42
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    • 1991
  • 최근에 분리 농축 그리고 정제 등의 분야에서 세라믹 분리막은 내열성, 내약품성 및 우수한 기계적 강도와 같은 특성으로 인해 기존의 유기고분자막으로는 사용할수 없던 영역까지 그 응용 범위를 확대시키고 있다. 이러한 세라믹 분리막 중 기공크기가 0.1-0.001 $\mu$m 정도로 미세한 한외여과막의 경우, 최근에는 주로 졸-겔법을 이용하여 제조되는 것으로 보고되고 있는데, 이는 졸-겔법이 기존 분리 공정과 비교하여 볼대 다음과 같은 장점이 있기 때문이다.

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취화재료(脆化材料)의 내취화(耐脆化) 구조(構造)

  • Sin, Dong-U;Hong, Cheong-Suk
    • Elastomers and Composites
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    • v.31 no.4
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    • pp.247-255
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    • 1996
  • 금속이나 고분자 재료에 비하여 세라믹스는 우수한 내열성과 고온 물성을 가지고 있음에도 불구하고, 잘 깨지는 특성과 제조시 많은 열량을 필요로 하는 단점 때문에 그 동안 고온 구조용 부품으로서 광범위하게 사용되지 못하였다. 본 연구에서는 polycarbosilane을 이용하여 C/C 복합체를 포함한 산화물 및 비산화물 세라믹 복합체의 저온 치밀화 제조 공정을 확립하였다. polympr precursor를 열처리하여 얻은 $Al_2O_3$와 SiC 장섬유를 대표적인 산화물, 비산화물 세라믹스인 알루미나와 탄화규소에 각각 보강하여 파괴에너지가 기존의 단체 세라믹스에 비하여 10배 이상 향상된 세라믹 복합체를 제조하였다. 복합체 제조시 polycarbosilane을 결합제로 첨가하였으며 polycarbosilane이 SiC로 전이되는 $1150^{\circ}C$에서 열처리하여 이론 밀도의 73% 이상을 얻었다.

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Application of Sol-Gel Coating Process in Pressureless Sintering of Si3N4 and Their Properties (알루미나 졸-겔 코팅 공정을 이용한 질화규소의 상압소결 및 물질 특성)

  • 임경란;임창섭
    • Journal of the Korean Ceramic Society
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    • v.31 no.1
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    • pp.69-73
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    • 1994
  • Si3N4 ceramics could be densified above 3.2g/㎤ with pressureless sintering at below 178$0^{\circ}C$ by coating Si3N4 and Y2O3 powder with an alumina sol. Substitution a portion of Al2O3 with AlN improved densification. Additional milling of the coated powder in large improvement in bending strength greater than 800 MPa (4-point).

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A Study on the Purification Process of Alumina by Powder Technics (알루미나 정제공정의 분체공학적 연구)

  • 백행남;서태수;곽중협
    • Journal of the Korean Ceramic Society
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    • v.25 no.6
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    • pp.655-664
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    • 1988
  • As a part of study to establish the industrial process for manufacturing high purity alumina powder which is largely used as fine ceramics, an adsorption method using a silica-containing material which can absorb to eliminate a major impurity, Na in aluminum hydroxide as a raw material has been studied. It is confirmed that the primary property of powder such as the particle size of raw material and that of silica-containing material plays a great important role in the purification process.

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A Study on Preparation of Alumina Membranes(2) (알루미나 한외여과막의 제조에 관한 연구(2))

  • 유재근;이응상
    • Journal of the Korean Ceramic Society
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    • v.31 no.4
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    • pp.359-366
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    • 1994
  • Tow types of supports were made using $\alpha$-Al2O3 powder and optimum conditions to prepare for supports were provided. Sol solution for coating was synthesized by sol-gel method with aluminum isopropoxide. Supports were coated and heat-treatemented, where the thickness of coating layer was controlled by dipping time. Flux and permeability of alumina membrane were measured by liquid and gas filtration apparatus and these were compared with the provided model. It was confirmed that the coating was done very well without micro~crack and defect.

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Study on the Alumina Extraction from Kaolin (고령토로부터 알루미나 추출에 관한 연구)

  • 맹중재;김철주;신병식
    • Journal of the Korean Ceramic Society
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    • v.17 no.1
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    • pp.35-41
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    • 1980
  • Alumina extraction from raw Hadong kaolin with sulfuric acid was studied to obtain relatively pure alumina. Factors as acid concentration, heating temperature and conditions of ammonium alum crystal formation from extracted solution are also surveyed and most of iron oxide in kaolin is eliminated in crystallization of ammonium alum. Pure crystal obtained from the extracted solution with ammonium sulfate is relatively free from iron containment in mother liquor. Alumina in ammonium alum crystal is converted to gibbsite form after complete hydrolysis in ammonia gas.

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Effect of Salt on Crystal Growth of Plate-like Alumina Particles by Molten-salt Method (Molten-salt 방법에 의해 합성되는 판상형 알루미나 분말의 입성장 거동에 미치는 Salt의 영향)

  • Kim, Bo Yeon;Lee, Yoon Joo;Shin, Dong-geun;Kim, Soo Ryong;Kwon, Woo Teck;Kim, Younghee;Choi, Duck Kyun
    • Korean Chemical Engineering Research
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    • v.53 no.5
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    • pp.603-608
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    • 2015
  • Alumina powder have been expanded its application in industry and required to control its morphology such as powder size and aspect ratio of single particle. It can be synthesized by molten - salt method which is possible to obtain various shapes of ceramic particles by controlling the growth direction because each crystal face has different growth rate. In this study, various combinations of salts such as NaCl, $Na_2SO_4$, $Na_3PO_4$ and their mixture were used for control the growth of plate like alumina particle from the initial stage of synthesis because salt having different ionic strength can control the growth direction of ceramic particle under its melting condition around $800{\sim}900^{\circ}C$, and growth behavior of plate-like alumina particle with different reaction conditions such as temperature and concentration on the crystal size and shape was studied.

Investigation of alumina(Al2O3) 3D nozzle printing process (알루미나(Al2O3)를 활용한 3D 노즐 프린팅 기술 연구)

  • An, Tae-Kyu;Han, Kyu-Sung;Kim, Ji-Hoon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.12
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    • pp.247-253
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    • 2019
  • 3D printing technology has attracted considerable attention because of its potential to fabricate the intricate design of ceramic products. In this study, ceramic 3D nozzle printing was introduced to manufacture complex alumina products with a ceramic pigment. The alumina paste was formulated by incorporating an elastomer to impart viscoelastic properties. Viscoelastic pastes play an essential role in ceramic 3D nozzle printing. The effects of the viscoelastic properties of the ceramic pastes on their printability were assessed using comprehensive rheological analysis, and various shapes were printed. As a result, the paste with a high yield stress showed better printability. In addition, a ceramic pigment was added to the developed pastes to increase the aesthetics of the printed ceramic structure. The printed ceramic parts were sintered in air at 1300 ℃. The stability of the ceramic pigment was confirmed even after high-temperature sintering.