• 광산업정보
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• 통권16호
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• pp.66-73
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• 2003

• 한국전기전자재료학회논문지
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• 제34권6호
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• pp.466-474
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• 2021

[011] poled ternary Pb(In_1/2Nb_1/2)O₃-Pb(Mg_1/3Nb_2/3)O₃-PbTiO₃ (PIN-PMN-PT) single crystals have been investigated for active materials for acoustic transducers because of their high piezoelectric properties in both shear and transverse modes. In order to use [011] poled PIN-PMN-PT single crystals for acoustic transducers, the characterization of full-matrix material properties is required. In this study, full sets of compliance, dielectric, and piezoelectric constants of [011] poled rhombohedral PIN-PMN-PT were measured by a resonance method. Dimensions and geometries of 12 samples were proposed for measuring 17 independent material constants of [011] poled rhombohedral PIN-PMN-PT single crystals. Two sets of samples with different PT concentrations, 0.24PIN-0.49PMN-0.27PT and 0.24PIN-0.46PMN-0.30PT, were fabricated and their material properties were measured. Measured impedance spectra and simulated impedance spectra of the samples were compared to check the accuracy of the measurements.

• 마이크로전자및패키징학회지
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• 제27권4호
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• pp.91-96
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• 2020

Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3계 압전 단결정의 유전특성과 압전특성을 전계 및 압축응력 인가 조건 하에서 33-모드 방식으로 측정하였다. 110~140℃ 영역에서 저온 rhombohedral 구조에서 고온 tetragonal 구조로의 상전이가 관찰되었으며, cubic 구조로 변화하는 큐리온도는 165℃ 정도로 나타났다. 압축응력 및 전계 변화에 따른 분극의 크기변화를 측정하였다. 전계인가 분극 곡선의 기울기로부터 비유전율을 계산하였고, 인가되는 응력의 크기가 증가할수록 계산된 비유전율의 크기는 증가하고, 인가되는 전계의 크기가 증가할수록 비유전율의 크기는 감소하는 경향성을 나타내었다. 압축응력 및 전계 변화에 따른 변위 거동을 측정하였으며, 곡선의 기울기로부터 압전상수를 계산하였고 압력인가에 따른 상전이를 확인하였다. 수중 또는 의료용 초음파 발진자로 실제 응용할 경우 선형성을 유지하여 구동이 가능하기 위하여 소자 기구물을 형성하는 단계에서 인가하게 되는 압축응력의 크기와 구동 전계의 DC 바이어스의 크기를 적절하게 설계할 필요가 있다.

• 한국전기전자재료학회논문지
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• 제37권4호
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• pp.412-419
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• 2024

Mn-doped Pb(In_1/2Nb_1/2)O₃-Pb(Mg_2/3Nb_1/3)O₃-PbTiO₃ (Mn:PIN-PMN-PT) single crystals, which exhibit improved phase transition temperatures and coercive field properties compared to Pb(In_1/2Nb_1/2)O₃-Pb(Mg_2/3Nb_1/3)O₃-PbTiO₃ (PIN-PMN-PT) single crystals, are expected to be utilized in high-power acoustic transducers. Bridgeman method, growing single crystals along the axial direction from melt, is most widely used method for single crystal growth with large size and high quality. However, single crystal boules grown by the Bridgeman method demonstrate a PT compositional variation, giving rise a distribution of crystal structure and material properties along the growing axis. To employ piezoelectric single crystals grown by the Bridgeman method for acoustic transducers, it is essential to investigate their overall property distribution. In this study, the compositional distribution and property variation of Mn:PIN-PMN-PT single crystals grown by the Bridgeman method was investigated. Measured compositional distribution of PT was from 29% to 32.5% in the Rhombohedral crystal region of the boule. Two types of specimen, [011]-poled Mn:PIN-PMN-29PT and Mn:PIN-PMN-32PT single crystals, were fabricated and tested to obtain full property variation at both ends of the Rhombohedral crystal region. The properties related to the 32 directional vibration mode and the properties related to high-power driving were measured to confirm the overall distribution of properties by composition.