• Title/Summary/Keyword: 시효 처리

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Ti-50.lat.% Ni 합금의 변태거동에 미치는 시효처리의 영향

  • 박성범;류부형;우흥식
    • Proceedings of the Korean Institute of Industrial Safety Conference
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    • 2003.10a
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    • pp.107-112
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    • 2003
  • 형상기억합금(shape memory alloy; SMA)은 소성가공을 통하여 원하는 형태로 변형시킨 이후에도(현재로서는 최대 10%미만의 변형) 일정조건의 열을 가하면 원래의 형상으로 복원되는 합금을 말한다. 형상기억효과는 고상(solid state)에서의 금속조직이 오스테나이트(austenite: 이하 A 또는 B2상)로부터 마르텐사이트(martensite: 이하 M 또는 B19'상)로, 다시 역으로 마르텐사이트에서 오스테나이트로의 변태에 기인되는 것으로 밝혀지고 있으며 이러한 변태는 온도유기변태(temperature induced transformation)와 응력유기변태(stress induced transformation)로 분류할 수 있다.(중략)

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Strengthening mechanisms of 304 stainless steel during strain aging (304 스테인리스강 시효처리 시 강화기구 고찰)

  • Lee, S.H.;Choi, C.Y.;Nam, W.J.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.382-384
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    • 2009
  • Strengthening mechanisms of metastable austenitic stainless steel, containing $\alpha'$-martensite phase, during strain aging was investigated. The variations of volume fraction of $\alpha'$-martensite phase, hardness of $\alpha'$-martensite phase, hardness of austenite were examined.

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A study of the tensile bond strength between Polyetherketoneketone (PEKK) and various veneered denture base resin (Polyetherketoneketone (PEKK)과 다양한 의치상용 전장 레진 간의 인장결합강도에 관한 연구)

  • Park, Yeon-Hee;Seo, Jae-Min;Lee, Jung-Jin
    • The Journal of Korean Academy of Prosthodontics
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    • v.60 no.3
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    • pp.231-238
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    • 2022
  • Purpose. This study aimed to investigate the effect of different veneering methods on the tensile bond strength between polyetherketoneketone (PEKK) and denture base resins. Materials and methods. A total of 80 PEKK T-shaped specimens were fabricated and the primer (Visio.link) was applied after airborne-particle abrasion with 110 ㎛ alumina oxide powder. According to the veneering method, the specimens were divided into four groups (n = 20) to be veneered with the gingival colored packable photopolymerized composite resin (SR Adoro); flowable photopolymerized composite resin, (Crea.lign); heat-polymerized resin (Vertex); and self-polymerized resin (ProBase Cold). Each group was divided into two subgroups (n = 10) according to the artificial thermal aging. After the tensile bond strength measurement via universal testing machine, the fracture sections of all specimens were observed. Two-way ANOVA and Tukey's HSD post hoc test were used for the statistical analysis (α = .05). Results. The results of the two-way ANOVA showed statistically significant differences in the tensile bond strength according to the veneering method and artificial thermal aging of denture base resins (P<.001). The highest tensile bond strength showed in the packable photopolymerized resin group before and after the artificial thermal aging. The lowest tensile bond strength showed in the heat-polymerized resin group. The mixed and adhesive fracture showed in all groups. Conclusion. The veneering method and artificial thermal aging can influence in the tensile bond strength between the resin and PEKK. The artificial thermal aging can reduce the tensile bond strength.

Evaluation of Mechanical Property for Pb-free Solder/Ni Plate Joints with Artificial Aging Time (인공시효시간에 따른 Ni 기판 Pb-free 솔더접합부의 기계적 물성평가)

  • Park, So Young;Yang, Sung Mo;Yu, Hyo Sun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.5
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    • pp.467-471
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    • 2015
  • Thus far, solders used in electronics remain lead-based. Pb-free solutions in electronic components and systems are receiving increased attention in the semiconductor and electronics industries. Pb-free materials currently in used are Sn-37Pb, Sn-4Ag and Sn-4Ag-0.5Cu/Ni plate joints. In this study, solder alloys were used at high temperatures for artificial aging processing that was performed at $150^{\circ}C$ for 0hr, 100hr, 200hr, 400hr, 600hr and 1000hr. The SP test was conducted at $30^{\circ}C$ and $50^{\circ}C$. As a result, the maximum shear strength of all the specimens decreased with the increase in artificial aging time and temperature of the SP test. In addition, Pb-free solders showed higher total fracture energy compared with Sn-37Pb at high temperatures. The mechanical properties of Sn-4Ag-0.5Cu solder/Ni plate joints remained in excellent conditions in electronic parking systems at high temperatures.

Wire electrical discharge machining of titanium alloy according to the heat treatment conditions (열처리 조건에 따른 티타늄합금의 와이어 방전가공)

  • 김종업;왕덕현;김원일
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.930-933
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    • 2001
  • Titanium Alloys used in this experiment has an good corrosion resistance and specific strength, and is the new material developed for medical supplies living goods. In this study the rolled titanium alloy is done by annealing, solution heat-treatment and aging and then is worked by wire EDM. With changing the process conditions, the process properties of surface hardness, surface roughness, shape of process surface and the analysis of ingredients are measured through experiment repeating main cut and finish cut. It is confirmed to gain good measure values as increasing the number of processing of wire EDM. In this experiment the phenomena of processing is studied and the appropriate process condition is proposed.

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Effect of Heat Treatment on Mechanical Properties of STD11 and STS3 (공구강의 열처리 조건에 빠른 기계적 성질)

  • 박지환;이종권;류근걸;이윤배
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.5 no.3
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    • pp.204-209
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    • 2004
  • Using STD11 and STS3 as a mold set, accuracy of a mold product could be improved by heat treatment. Results of Charpy impact test and measurement of retained austenite in STS3 and STD11, STD11 was superior than STS3 in effect of sub-zero treatment and stability of working and measure. Decrease of retain austenite by sub-zero treatment in STS3 did not occured.

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The Effect of Aging Treatment on the Microstructure and Mechanical Properties of Super Duplex Stainless Steel with W (W이 첨가된 슈퍼 2상 스테인리스강의 미세조직과 기계적성질에 미치는 시효처리의 영향)

  • Kim, Soo-Chun;Bae, Dong-Soo;Kang, Chang-Yong
    • Journal of Ocean Engineering and Technology
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    • v.23 no.4
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    • pp.52-57
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    • 2009
  • The effect of aging treatment on the microstructure and mechanical properties of super duplex stainless steel with W was investigated. The phase was precipitated mainly at the early stage of aging and a lower aging temperature under $750^{\circ}C$, but the phase was formed after long-term aging treatment between $600^{\circ}C$ and $900^{\circ}C$. The volume fraction of the phase increased with aging temperature up to $750^{\circ}C$ and then decreased up to $900^{\circ}C$. With an increase in the aging time, the volume fraction phase at the early stage of aging increased slightly, and then increased rapidly beyond a certain time. The rapid increase in the tensile strength and hardness and decrease in the elongation and impact toughness were measured with aging temperatures up to $750^{\circ}C$. On the other hand, the tensile strength and hardness decreased slightly, and the elongation and Charpy impact toughness were unchanged with aging temperatures over $750^{\circ}C$. The tensile strength and hardness increased rapidly at the early stage of aging, and then increased slowly beyond a certain time. The elongation and Charpy impact toughness decreased rapidly at the early stage of aging, and then remained unchanged beyond a certain time. The phase that formed at the early stage of aging and the lower aging temperature had a considerable effect on the elongation and Charpy impact toughness of the super duplex stainless steel with W.

Mechanical Properties and cytotoxicity of nitrided 630 Stainless by ion nitriding (플라즈마 이온질화에 따른 STS 630의 기계적 특성과 세포독성에 관한 융합적 연구)

  • Hwang, Gab-Woon
    • Journal of the Korea Convergence Society
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    • v.10 no.11
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    • pp.241-246
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    • 2019
  • In this study, we have examined the possibility to improve the material properties and biocompatibility of the 630 stainless steel for the application of medical instruments. The evaluation of mechanical properties and biocompatibility of the 630 stainless steel were studied by aging, nitriding, SEM measurement, Vicker's hardness, tensile strength and MTT cytotoxicity using IGF cells, respectively. The results showed that the tensile strength and Vicker's hardness of 630 stainless steel was increased with aging and ion nitriding time. The cytotoxicities of the 630 stainless decreased compared with the 420 stainless on MTT cytotoxicity using IGF cells. Ion nitriding of 630 stainless led to an enhanced application of medical instruments and biocompatibility performance.

Properties of Cu Pillar Bump Joints during Isothermal Aging (등온 시효 처리에 따른 Cu Pillar Bump 접합부 특성)

  • Eun-Su Jang;Eun-Chae Noh;So-Jeong Na;Jeong-Won Yoon
    • Journal of the Microelectronics and Packaging Society
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    • v.31 no.1
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    • pp.35-42
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    • 2024
  • Recently, with the miniaturization and high integration of semiconductor chips, the bump bridge phenomenon caused by fine pitches is drawing attention as a problem. Accordingly, Cu pillar bump, which can minimize the bump bridge phenomenon, is widely applied in the semiconductor package industry for fine pitch applications. When exposed to a high-temperature environment, the thickness of the intermetallic compound (IMC) formed at the joint interface increases, and at the same time, Kirkendall void is formed and grown inside some IMC/Cu and IMC interfaces. Therefore, it is important to control the excessive growth of IMC and the formation and growth of Kirkendall voids because they weaken the mechanical reliability of the joints. Therefore, in this study, isothermal aging evaluation of Cu pillar bump joints with a CS (Cu+ Sn-1.8Ag Solder) structure was performed and the corresponding results was reported.

Effect of Aging Treatment on the Mechanical Properties of Mg-6Al-xZn(x=0,1,2) Alloys Fabr~catedb y Squeeze Casting (용탕단조법에 의해 제조된 Mg-6AI-xZn(x0,1,2)합금의 기계적 성질에 미치는 시효처리의 영향)

  • Gang, Min-Cheol;Yun, Il-Seong;Kim, Gyeong-Hyeon;Kim, In-Bae
    • Korean Journal of Materials Research
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    • v.7 no.2
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    • pp.129-135
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    • 1997
  • This study has investigated the effects of aging treatment on thc nlechanical propcrries of blg-iiAl-x%nix - 0.1.2) alloys fabricated by the squeeze castmg process. The microstructurcs of as-squeeze cast were composed of pro eurectic $\alpha$ magnesium solid solution, super saturated $\alpha$ solid solution and $\beta(Mg_{17}AI_{12}$) compund. Agcd at both $200^{\circ}C$ and $240^{\circ}C$, Mg--6AixZn alloys showed the peak hardness due to the formation of $\beta(Mg_{17}AI_{12}$) precipitates. The tiiscontinuous precipitates of the lamella r\.pe are predominant at $200^{\circ}C$ aging tredrment. tvhilc. the finely dispersed continu ous precipitates were major type at $240^{\circ}C$ treatment. Mg-- GAI-xZn a1loi.s fabricated hy the squeeze casting process had the hetter combination of tensile strength and elongation compared to the conventionally cast alloys. As increascci zinc: contents. the tensile strength was increased 11y the soiid solutirin strengthening effect of zinc,.

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