• Title/Summary/Keyword: 시료 채취

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Artifacts Frequently Encountered in Electron Micrographs (생물시료의 전자현미경 시료 제작 및 관찰 과정에서 발생되는 인공물)

  • Park, Chang-Hyun;Cho, Kang-Yong;Uhm, Chang-Sub
    • Applied Microscopy
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    • v.35 no.1
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    • pp.1-13
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    • 2005
  • Fine photographs are essential in the electron microscopy. Artifacts can be introduced during all steps of electron microscopy; specimen processing, observation and printing. Every caution is necessary to avoid the artifact formation. In this review, the authors discussed the causes of various artifacts and suggested the solution to help the correct tissue handling and electron microscopic observations.

한강 수계에서의 희토류원소 분포도의 유역별/계절별 분포도 변화

  • Lee Seung-Gu;Lee Gwang-Sik;Lee Dong-Ho;Kim Yong-Je
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2006.04a
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    • pp.263-265
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    • 2006
  • 희토류원소 분포도를 이용하여 하천본류의 화학조성에 미치는 각 지류 및 주변 암석들의 영향을 조사하기 위해 한강본류, 남한강, 북한강의 상류 및 하류에서 하천수를 계절별로 채취하여 분석하였다. 한강수내 희토류원소 자료를 PAAS (Post Archean Australian Shale)로 규격화한 분포도 특성은 다음과 같이 요약된다. 첫째, 한강의 모든 물시료는 Eu의 정(+)의 이상과 Ce의 부(-)의 이상을 갖고 있다. 둘째 절대농도에 있어서 하기에 채취된 모든 한강 시료는 다른 절기의 시료들보다. 함량이 높다. 셋째로 전반적으로 중희토류(HREE)가 경희토류(LREE)보다. 부화되어 있다. Eu의 이상을 가지고 비교해 볼 때, 한강 본류는 남한강쪽보다는 북한강쪽의 영향을 더 많이 받는 것으로 나타났다. 본 연구결과, 하천의 본류에 보다. 많은 영향을 주는 지류를 판단함에 있어서 희토류원소의 분포도자 유용하게 활용될 수 있음을 확인할 수 있었다.

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Analytical Quality Control of Environmental Pollutants in Water (수질측정분석의 정도관리)

  • 이인선
    • Journal of Environmental Health Sciences
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    • v.19 no.1
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    • pp.13-23
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    • 1993
  • I. 서론 : 생활수준의 향상과 더불어 삶의 질을 향상시키고 사람을 포함한 생태계에 미치는 오염물질을 관리하기 위하여는 정확한 오염현황 자료가 필요하다. 환경에 영향을 미치는 오염물질 농도는 매우 낮기 때문에 이들 물질을 측정분리하기 위하여는 측정분석 요원의 측정기술 능력, 측정장비, 측정분석에 소요되는 시약 및 초자, 기타 실험실 분위기와 측정요원의 근무여건 등이 최적의 상태로 상호 조화를 이루어야 정확한 측정자료를 얻을 수 있다. 정확한 측정자료를 얻기 위하여는 모든 측정과정이 포함된 측정분석 정도관리가 필요하며 측정결과에 영향을 미칠 수 있는 시료채취, 운송 및 보관, 측정분석 그리고 측정결과의 정리단계에서 오차요인을 제거하는 노력이 필요하다. 본 고에서는 측정분석 과정 중 오차요인을 많이 포함하고 있는 환경시료 채취방법, 환경시료 전처리방법 그리고 측정분석 정도관리 방법에 대한 고찰을 통하여 수질측정분석 정도를 향상시킬 수 있는 방안을 강구하고자 한다.

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Geochemical Study on the Alluvial Aquifer System of the Nakdong River for the Estimation of River Bank Filtration (강변여과수 개발을 위한 낙동강 충적층 지하수의 지구화학적 특성연구)

  • 김건영;고용권;김천수;김형수;김성이
    • The Journal of Engineering Geology
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    • v.13 no.1
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    • pp.83-105
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    • 2003
  • Geochemical studies on the alluvial aquifer system near the Nakdong River were carried out for the basic investigation of the estimation of artificial recharge for the river bank filtration. In-situ data do not show any distinct difference between the pumping well and river. Most of waters belong to $_3$ and Ca-$SO_4$ types and show high Mn concentration. In the borehole installed with Multi-Ca-HCOPacker (MP) system, Na, Ca, Mg, $HCO_3$ contents of the groundwater are increased with depth increasing. Cl and $SO_4$ contents of the groundwater show the lowest values at the bottom level (18m depth) and Mn content is very high at the middle level (13.5 m depth) of MP system. There is no distinct difference in the ${\delta}^{18}O$ and D values and tritium content between MP, borehole and surface water samples. The sulfur isotope data indicate that the possible sulfur source is dissolution of sulfate mineral from sedimentary rock. Strontium isotope ratio shows a little differences between the pumping well and observation borehole samples. Nitrogen isotope data indicate that the nitrogen of water samples is originated from fertilizer or organic materials.

Studies on the Hydrolysis of Seaweed using Microorganisms and Its Application II. Screening of Microfloras Involved in Hydrolysis of Seaweed Tenella, Seaweed Fusiforme and Green Laver (미생물을 이용한 해조류의 가수분해 및 이용 II. 돌가사리, 톳 및 가시파래를 가수분해시키는 미생물군의 탐색)

  • 김해섭;배태진
    • The Korean Journal of Food And Nutrition
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    • v.15 no.3
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    • pp.257-266
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    • 2002
  • The purpose of this study is screening of microfloras involved in hydrolysis of seaweed tenella, seaweed fusiforme and green laver. This is a part of studies on the hydrolysis of seaweed using microorganisms. First, about two hundred microflora samples were obtained from mountain, rice field, dry field, sea, seaside and fish market in the vicinity of Yeosu. Thirty-three microflora samples were screened from the destruction of tissue in sea tangle and sea mustard. It was sufficient that results of the naked eye observation were obtained at eight microflora samples as a feces of bull, a decayed pine tree, a soil of dry field, the mud of the banks in a rice field, the water of a ditch in a rice field, the weed of the banks in a rice field, the water in a rice field and leaved in the air. Above all, extraction rate and contents of reducing sugar in extracts of seaweeds added a decayed pine tree(sample No. 8) and the water of a ditch in a rice field(sample No. 27) were showed high value. And the value of chemical analysis of the sample is much better in comparison with control. Accordingly the hydrolysis of seaweed using microorganisms in the inside of these microflora samples can be possible.

Reconsideration for Current Water Quality Monitoring System throughout Daily Observation (매일 관측을 통한 현행 수질 모니터링 시스템 주기에 관한 재고)

  • Bae, Hun-Kyun
    • Journal of Environmental Policy
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    • v.12 no.1
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    • pp.59-74
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    • 2013
  • The weakness of current water quality monitoring system was reviewed to manage Nakdong river's water quality. The current monitoring system has sampling periods lasting for a week to 10 days, but these-SAMpling periods may not accurately measure the real level of water quality. Therefore, daily sampling and analysis of water samples for nine factors was performed from May 1st 2011 to Sep. 30st 2011 to check the water quality changes at three-SAMpling points, Munsanri (the upper side of Kangjung-Koryung weir), Kangchang (the outlet of the Kumho River) and Samunjin (the lower side of Kangjung-Koryung weir). As demonstrated by the results, concentrations of all nine factors dramatically changed on a daily basis, so daily sampling and analysis of water quality samples may be needed instead of weekly sampling and analysis of water quality samples to ensure the proper management of the Nakdong River's water quality. However, daily observations for all water sampling points are not possible because costs and labors are limited, so that new methods which could support the current monitoring system should be developed.

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An Assessment of Air Sampling Location for Stack Monitoring in Nuclear Facility (원자력시설 굴뚝 내 공기시료채취 위치의 적절성 평가)

  • Lee, JungBok;Kim, TaeHyoung;Lee, JongIl;Kim, BongHwan
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.15 no.2
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    • pp.173-180
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    • 2017
  • In this study, air sampling locations in the stack of the Advanced Fuel Science Building (AFSB) at the Korea Atomic Energy Research Institute (KAERI) were assessed according to the ANSI/HPS N13.1-1999 specification. The velocity profile, flow angle and $10{\mu}m$ aerosol particle profile at the cross-section as functions of stack height L and stack diameter D (L/D) were assessed according to the sampling location criteria using COMSOL. The criteria for the velocity profile were found to be met at 5 L/D or more for the height, and the criteria for the average flow angle were met at all locations through this assessment. The criteria for the particle profile were met at 5 L/D and 9 L/D. However, the particle profile at the cross-section of each sampling location was found to be non-uniform. In order to establish uniformity of the particle profile, a static mixer and a perimeter ring were modeled, after which the degrees of effectiveness of these components were compared. Modeling using the static mixer indicated that the sampling locations that met the criteria for the particle profile were 5-10 L/D. When modeling using the perimeter ring, the sampling locations that met the criteria for particle profile were 5 L/D and 7-10 L/D. The criteria for the velocity profile and the average flow angle were also met at the sampling locations that met the criteria for the particle profile. The methodologies used in this study can also be applied during assessments of air sampling locations when monitoring stacks at new nuclear facilities as well as existing nuclear facilities.

REE Mineralization of Quy Hop Area in Nghe An Province, Northern Vietnam (베트남 북부 네안성 뀌홉지역 희토류 광화작용)

  • Lee, Jae-Ho;Jin, Kwang-Min;Heo, Chul-Ho
    • Journal of the Mineralogical Society of Korea
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    • v.31 no.3
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    • pp.193-213
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    • 2018
  • Soil geochemical exploration to check anomalies related to mineralization was carried out targeting around Quy Hop area within Nghe An province, Northern Vietnam. The interval of sampling are horizontal 250 m with 13 line and longitudinal 300 m with 25 line, resulting in 325 soil samples. Based on the result of soil geochemical exploration, the pitting survey was carried out targeting the grid point with high TREO content, resulting in 73 soil samples within 8 pits. The geology of the survey area are consisted of Ban Chieng biotite granite complex intruding Bu Khang formation comprising of schist, gneiss and limestone. In order to elucidate the source rock of monazite and xenotime confirmed from heavy sand, soil geochemical exploration was carried out. By ICP-MS result of soil samples, total REE oxide content of background amount is about 1.4 times of crustal abundance, depleting the light rare earth (about 0.2 times) and enriching the heavy rare earth (about 1.5 times). By ICP-MS result of pit soil samples, we identified TREO more than 1,000 ppm in 6 pits. It may be considered that REE ore bodies may develop in NE-SW direction, compared with the geochemical results of Quy Chau area.

A review of analytical method for volatile fatty acids as designated offensive odorants in Korea (악취성 유기지방산 성분의 분석기술)

  • Ahn, Ji-Won;Kim, Yong-Hyun;Kim, Ki-Hyun;Song, Hee-Nam
    • Analytical Science and Technology
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    • v.25 no.2
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    • pp.91-101
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    • 2012
  • A list of volatile fatty acids (VFA) including propionic acid, butyric acid, isovaleric acid, valeric acid, etc. is well known for offensive odorants. The analysis of odorant VFA is a highly delicate task due to high reactivity and unstable recovery rate. At present, analytical methods of VFA are recommended to include alkali impregnation filter method and alkali absorption method by the malodor prevention law of the Korea Ministry of Environment (KMOE). In this review, a survey has been made to explore various approaches available for the analysis of VFA to include both official methods of the KMOE and others. In light of the unreliability of those established analytical methods, it is highly desirable to develop some substituting methods for VFA. Among such options, one may consider such option as sorbent tube (ST) sampling and cryogenic trapping-thermal desorption technique. Moreover, procedures used for standard preparation, sampling steps, and instrumental detection stage are also evaluated. Application of container sampling (like Tedlar bag) is however not recommendable due to significant (sorptive) loss in sampling and in storage stage. In the detection stage, the use of GC/MS is recommendable to replace GC/FID due to the presence of diverse interfering substances. Thus, it is essential to properly establish the basic quality assurance (QA) for VFA analysis in air.

도계육의 시료 채취방법에 따른 세균의 검출량 비교

  • Yun, Hye-Suk
    • Bulletin of Food Technology
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    • v.18 no.1
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    • pp.127-135
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    • 2005
  • 상업적으로 시판되는 10주 미만의 식용 영계육을 처리하는 공정에서 25 그룹의 내장적출하지 않은 것 또는 내장적출한 도계육을 도계공정의 네지점에서 채취하였다. 도계 공정 각 지점의 계육으로부터 무작위로 선택된 부위에서 껍질을 잘라낸 것, 목의 껍질을 잘라낸 것, 셀룰로스 아세테이트 스폰지 재질의 스왑봉으로 계육을 스왑법으로 채취한 것, 또는 도계육을 통째로 세척한 세척액이다. 총균수, 대장균군, 대장균을 각 시료로부터 증균하였다. 사방 1 cm 안의 평균 로그값(log A)과 사방 25cm안에서 측정된 전체 측값치들의 로그값(N)은각 그룹 당 25개였다. 동일한 처리공정 단계에서 얻은 계육으로부터 얻은 같은 그룹의 세균의 측정값의 경우에, 무작위로 선택한 부위에서 잘라낸 껍질 또는 목에서 벗겨낸 껍질, 세척액 샘플에서 측정한 균수의 집합인 N의 세 값 또는 log A의 세 값은 <0.5 logunit 차이였다.그러나 스왑법으로 측정한 사방 1 cm안의 평균로그값(log A)과 사방 25 cm 안에서 측정된 전체측정치의 로그값(N)의 대략 절반이 다른 방법들로 측정한 동일한 측정항목의 값과 >0.5 log unit 까지 차이가 났다. 이런 결과로부터 도계육에서 무작위로 선택한 부위나 목에서 껍질을 잘라내는 방법, 또는 세척액 채취 등의 샘플링 방법은 도계육 표면의 단위영역 당 유사한 양의 세균이 검출될 것이라는 것을 나타낸다.

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