• Korean Journal of Soil Science and Fertilizer
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• v.28 no.2
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• pp.183-190
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• 1995

Various factors such as sampling height in the chamber, sampling interval, sampling time at daytime and the effects of pedoturbation on methane emission during chamber installation were evaluated using a simplified closed static chamber method to measure methane flux in paddy soils. Sampling height of the chamber for representative samples was 65cm. An additional DC fan was required to attain an even methane gradient in the chamber. Considering the change of methane concentration and air temperature in the chamber, sampling is recommended to finish within 30 minutes after starting sampling. The aim of setting DC fan in the chamber was to get the thermal equilibrium in the chamber as well as the representative samples. Suitable time to collect the gas samples representing the day's methane flux was 0900~1200 hours. Gas sampling was possible even after installation of small chambers if the elapsed time was more than 6 hours and supporting stand would be to be added to minimize pedoturbation.

• Journal of Environmental Impact Assessment
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• v.24 no.6
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• pp.607-618
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• 2015

Five years have passed since the first set of environmental samples was taken in 2011 to represent various ecosystems which would help future generations lead back to the past environment. Those samples have been preserved cryogenically in the National Environmental Specimen Bank(NESB) at the National Institute of Environmental Research. Even though there is a strict regulation (SOP, standard operating procedure) that rules over the whole sampling procedure to ensure each sample to represent the sampling area, it has not been put to the test for the validation. The question needs to be answered to clear any doubts on the representativeness and the quality of the samples. In order to address the question and ensure the sampling practice set in the SOP, many steps to the measurement of the sample, that is, from sampling in the field and the chemical analysis in the lab are broken down to evaluate the uncertainty at each level. Of the 8 species currently taken for the cryogenic preservation in the NESB, pine tree samples from two different sites were selected for this study. Duplicate samples were taken from each site according to the sampling protocol followed by the duplicate analyses which were carried out for each discrete sample. The uncertainties were evaluated by Robust ANOVA; two levels of uncertainty, one is the uncertainty from the sampling practice, and the other from the analytical process, were then compiled to give the measurement uncertainty on a measured concentration of the measurand. As a result, it was confirmed that it is the sampling practice not the analytical process that accounts for the most of the measurement uncertainty. Based on the top-down approach for the measurement uncertainty, the efficient way to ensure the representativeness of the sample was to increase the quantity of each discrete sample for the making of a composite sample, than to increase the number of the discrete samples across the site. Furthermore, the cost-effective approach to enhance the confidence level on the measurement can be expected from the efforts to lower the sampling uncertainty, not the analytical uncertainty. To test the representativeness of a composite sample of a sampling area, the variance within the site should be less than the difference from duplicate sampling. For that, a criterion, ${i.e.s^2}_{geochem}$(across the site variance) <${s^2}_{samp}$(variance at the sampling location) was proposed. In light of the criterion, the two representative samples for the two study areas passed the requirement. In contrast, whenever the variance of among the sampling locations (i.e. across the site) is larger than the sampling variance, more sampling increments need to be added within the sampling area until the requirement for the representativeness is achieved.

• Journal of the Korean Geotechnical Society
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• v.39 no.3
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• pp.17-27
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• 2023

In order to accurately determine soil characteristics, it is necessary to collect undisturbed samples, and it is important to collect these samples with minimal disturbance. In this study, a sampler that minimizes sample disturbance was developed by attaching a catcher to the tip, and its applicability was reviewed through in situ sampling, X-ray CT, and laboratory tests. Results confirmed that horizontal cracks are likely to occur when using the Shelby tube sampler, whereas these cracks can be suppressed when using the newly developed sampler. Moreover, consolidation and shear test results showed that the samples collected using the newly developed sampler showed higher maximum shear strength compared to those collected using the Shelby tube sampler.

• Journal of the Korean Geotechnical Society
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• v.19 no.4
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• pp.43-53
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• 2003

To get improved soil parameters in the laboratory tests, the effects of sample disturbance should be excluded as much as possible. A collaborative research between Dong-A University and PHRI (Japan) was conducted to investigate the effects of sample disturbance due to sampling techniques and samplers on Pusan clays. The results of unconfined compression and consolidation tests performed on the clay samples taken by them have been compared in terms of soil parameters and sample disturbance. As the result of the study, it was found that when the Korean sampler was used with a different technique of cleaning the borehole bottom and removing slime before inserting and penetrating the sampler tube, similar to the one commonly used in Japanese practice, the quality of samples could be greatly improved. Furthermore, the CRS test with the rate of 0.02%/min yielded larger values of consolidation parameters and better degree of sample disturbance than those of oedometer test, due to the difference in testing method.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 2000.04a
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• pp.311-312
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• 2000

최근 들어 환경대기중 휘발성유기화합물(Volatile Organic Compounds)에 대한 인식이 고조되면서 극미량 유기물질의 채취 및 분석기법에 대한 연구가 활발히 수행되고 있다. 미국의 경우, 1980년대 초부터 대기중 VOC에 대한 연구가 활발히 이루어져서 여러 종류의 VOC에 대한 시료채취 및 분석방법이 명시되어 있지만 우리나라에서는 VOC에 대한 전반적인 측정방법이 아직까지는 없는 실정이다. 미국에서 지정한 VOC의 시료채취방법 중에서 일반적으로 가장 널리 이용되고 있는 방법으로는 용기를 이용하여 유기화합물을 함유하고 있는 공기를 직접 채취하는 방법과 흡착관을 이용하는 방법을 들 수 있다. (중략)

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.671-676
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• 1998

방사성 $\beta$핵종 중의 하나인 $^{14}$ C은 중수로에서 상대적으로 많이 방출된다. 본 연구에서는 국내 유일의 중수로 원전인 월성 원자력발전소에서 배기구를 통해 환경으로 방출된 $^{14}$ C을 감시하기 위한 두 가지 타입의 대기시료 포집기술을 개발하였다. 하나는 전원을 이용하는 능동시료포집법(active air sampling)이며, 다른 하나는 전원을 사용하지 않는 수동시료포집법(passive air sampling)이다. 시료분석의 재현성 측면에서는 능동시료포집법이 보다 나은 것으로 알려져 있으나 시료채취 장소의 제한성 등으로 인해 최근에 들어와 수동시료포집법의 사용을 선호하고 있다. 본 연구를 통해 두가지 시료 채취법에 대한 측정오차의 신뢰성을 검증하기 위해 동위원소 분별효과를 비교 평가해 본 결과, 측정상의 오차가 약 2% 정도로 나타나 시료채취가 간단한 수동시료포집법의 사용타당성 및 활용 가능성을 입증하였다.

• Journal of the Korean Geotechnical Society
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• v.16 no.5
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• pp.93-105
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• 2000

일정변형률압밀사시험의 효율성 및 적용성을 구체화하기 위해 인공시료 또는 한정된 지역에서 채취한 불교란 점성토 시료가 아닌 광범위한 지역에서 채취한 불교란 점성토 시료에 대해 시험을 실시하였다. 시료채취의 대상지역은 우리나라의 서해안에서 동해안에 이르는 13개 지역이며, 29개의 불교란 자연시료를 채취하여 일정변형률압밀시험을 113회 실시하였다. 또한, 비교하기 위해 표준압밀시험도 병행하였다. 시험결과로부터 얻어진 압밀정수에 대한 공학적 특성을 고찰하였고, 회기분석을 통해 통계식을 제안하였다. 두 시험법에 의해 산출된 압밀정수를 비교 분석한 결과 수압비가 20% 이내인 범위에서는 일정변형률압밀시험의 변형률 속도가 압밀시험의 정수에 미치는 영향은 거의 없는 것으로 나타났다. 압축지수 및 압밀계수는 일정면형률시험의 결과 값이 표준압밀시험의 결과 값보다 크게 산출되었으나 일관성을 보였다. 또한, 선행압밀압력에 있어서는 두 시험법에 Cassagrande의 방법을 적용할 경우 서로 일치하는 것으로 나타났다. 본 연구로부터 일정변형률압밀시험을 사용하여 표준압밀시험에 상용하는 상호관계식 개발의 타당성을 확인할 수 있었다.

• Journal of Soil and Groundwater Environment
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• v.8 no.2
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• pp.1-8
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• 2003

Two types of ground-water sampling techniques for CFCs (chlorofluorocarbons) analysis, the cold-welded copper tube method and flame-sealed borosilicate glass ampule method, were compared and evaluated. CFCs concentrations by the copper tube method showed a poor reproducibility among triplicates whereas those by the glass ampule method showed a good agreement and relative standard deviations of triplicates were less than 5%. The poor reproducibility of the copper tube method appears to be attributed to the incomplete sealing in connection between faucets of wellhead and the sampling apparatus. The copper tube method also showed higher CFCs concentrations than the glass ampule method, which is more pronounced for CFC-11 than for CFC-12. The plastic tubings and rubber gasket of faucets in case of the copper tube method possibly contaminated the samples with CFC-11 and CFC-12. The potential of CFCs contamination for the glass ampule method was eliminated by using stainless steel and Nylon only and by connecting the sampling equipment directly to the main discharge pipe of wellhead. The validity of the glass ampule method were also verified by detecting very low level of CFCs for the ground-water sample which is old enough to have negligible CFCs.

• Journal of Environmental Impact Assessment
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• v.25 no.6
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• pp.532-541
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• 2016

The National Environmental Specimen Bank (NESB) has been collecting broad leave samples to monitor environmental pollution from five different designated sampling areas. In order to ensure the reproducibility and comparability of the results, all the procedures from selecting trees and pooling leaves to make the representative sample are defined in the standard operation procedures(the SOP). The representative samples were subjected to the chemical analyses for some heavy minerals and Polycyclic Aromatic Hydrocarbons(PAHs). The uncertainty levels involved in each step of the SOP, that is, the sampling and the chemical analysis, were derived using the Robust ANOVA, which enables the relative comparison among the different levels of pollutants concentrations with confidence. Furthermore, the effect of the varying degrees of precipitation on the pollutants concentration of the leaves was also examined. Overall, the biological difference estimated from the duplicate samples was found to exceed the variation across the site, implying even aerial deposition over site. Samples from Gwanak Mt. showed highest heavy metal concentrations than the other sites. Washing off effect of the pollutants adhering in the form of particles on the leaf surface was found to be affected by the cumulative precipitation.

• 한국해양학회지
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• v.30 no.4
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• pp.365-370
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• 1995

A new piston-type Free-fall corer (FFC) was developed for the sampling of core sediments in aquatic environments. The corer, named "KORDI-FFC", is the modified sampler of the existing FFX with an open barrel gravity corer. It was rested successfully on the muddy bottom in the Chinhae Bay and on the sandy bottom (Mz=3$\phi$) in nearshore areas around the Cheju Island. Several merits found in the unstrument are; $\circled1$ operation on a small vessel without winch and cable, $\circled2$ low cost of construction, $\circled3$ little disturbance of surface sediments during the sampling, $\circled4$ short round-trip time of sampling, and $\circled5$ simultaneous performance of other research works during the lowering of FFC.