• Title/Summary/Keyword: 시료채취

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지하수의 채취 및 전처리 방법에 따른 TOC 농도변화

  • 조수영;윤윤열;이길용;김용재
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.413-416
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    • 2004
  • TOC(total organic carbon)분석은 폐수 및 강수의 오염특성을 평가하기 위한 도구로서 BOD(biochemical oxygen demand), COD(chemical oxygen demand) 와 함께 사용되어 왔다. TOC 측정시간은 10분 정도로 BOD(5~6일), COD(2~3시간)에 비해 아주 짧은 시간에 측정할 수가 있으며, 전처리과정이 단순하고 정확도도 높은 것으로 알려져 있다. 본 연구는 지하수의 잠재오염성을 밝혀내기 위한 도구로 TOC를 활용하여 신뢰성 있는 분석 값을 얻기 위해서 시료의 채취, 보관, 측정까지의 최적 조건을 도출하는데 목적을 두었다. 아울러 시료 채취 후 일정 경과 시간에 따른 TOC의 변화를 관찰하였다. 시료채취 용기, 채취 후 산성화, 보관방법 및 기간에 대한 실험 결과, 대상 변수에 따라서 TOC의 농도변화에 커다란 차이점을 볼 수 있었다. TOC 농도가 낮은 지하수시료의 측정에서는 빛을 차단시킨 불투명 유리병을 사용해야만 하고 채취 즉시 산도를 높여(pH<2)주며 4$^{\circ}C$ 이하에서 보관하여야 한다. 지하수중 TOC 측정시료는 가능한 보관 기간에 있어서 채수 후 24시간 이내에 측정하는 것이 좋으나 1) 본 연구에서는 채취현장과의 거리를 고려하면 현실적으로 불가능하므로 기간에 따른 TOC 변화를 30일까지 측정, 조사하였다.

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Suggestions for river bed material sampling criteria (하상재료 Sampling 기준에 대한 제안)

  • Cho, Hong-Je;Lee, Kyeong-Won;Lee, Jea-Ho;Park, Jong-Won
    • Proceedings of the Korea Water Resources Association Conference
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    • 2011.05a
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    • pp.206-210
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    • 2011
  • 하상재료 조사 결과는 하천 계획과 개발의 기초 자료로 사용한다. 그러나 우리나라에는 하천 특성을 반영한 적절한 하상재료 조사 및 분석 방법을 제시하지 못하고 있다. 따라서 태화강 도시하천 연장 5km 구간에서 높은 밀도로 시료채취를 시행한 후 하상재료의 분석 결과를 토대로 국내 하천 실정에 맞는 하상 재료 조사 및 분석 방법을 제안하고자 한다. 대상구간 5km에 대하여 250m 간격으로 시료 채취 간격을 설정하고, 하천의 중심 및 좌 우안의 시료를 채취하였으며, 심도별로 시료를 분리하여, 시료의 공간적 분포 특성을 판별할 수 있도록 하였다. 한편, 시료의 입도 분포와 유기물질 함량과의 관계, 입도 분포와 거리와의 상관관계를 분석하였다. 분석결과로부터 향후 시료채취의 적절한 간격과 시료채취의 적절한 깊이를 제안할 수 있다. 연구 성과는 하천 관련 계획이나 개발에서 실용적인 방법으로 활용할 수 있다.

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Development of Automatic Smear Equipment for Measuring Surface Radioactivity Contamination (표면방사선 오염도 측정용 자동 스미어장치의 개발)

  • Tack, Han-Ho;Kang, Shin-Chool
    • Journal of Korea Society of Industrial Information Systems
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    • v.16 no.4
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    • pp.37-44
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    • 2011
  • This paper was development of surface contamination automatic smear sampling for measuring radioactive contamination in radiation controlled area of nuclear facility. In indirect method a smear paper are used manually. Activity on the smear paper is affected by varying the pressures applied, by the smearing time, by the difference of ares sampled during smearing. By means of these there are erroneous. In the future the apparatus will be developed as a portable apparatus measuring smear activity automatically by adding radiation detection instrument.

A Comparison Study of Aerosol Samplers for PM10 Mass Concentration Measurement (PM10 질량농도 측정을 위한 시료채취기의 비교 연구)

  • Park, Ju-Myon;Koo, Ja-Kon;Jeong, Tae-Young;Kwon, Dong-Myung;Yoo, Jong-Ik;Seo, Yong-Chil
    • Journal of Korean Society of Environmental Engineers
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    • v.31 no.2
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    • pp.153-160
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    • 2009
  • A PM10 (aerodynamic diameter${\leq}$10 ${\mu}m$) sampler is used to quantify the potential human exposure to suspended particulate matter (PM) and to comply with the governmental regulation. This study was conducted to compare and evaluate the same PM10 cutpoint and different slopes between United States Environmental Protection Agency (USEPA) PM10 sampling criterion and American Conference of Governmental Industrial Hygienists/$Comit\acute{e}$ $Europ\acute{e}en$ de Normalization/International Organization for Standardization thoracic PM10 sampling criterion through theory and experiment. Four PM10 samplers according to the USEPA criterion and one RespiCon sampler in accordance with the thoracic PM10 criterion were used in the present study. In addition, one DustTrak monitor was used to measure real time PM10 mass concentrations. All six aerosol samplers were tested in a PM generation chamber using polydisperse fly ash. Theoretical mass concentrations were calculated by applying the measured particle size distribution characteristics (geometric mean = 6.6 ${\mu}m$, geometric standard deviation = 1.9) of fly ash to each sampling criterion. The measured mass concentrations through a chamber experiment were consistent with theoretical mass concentrations in that a RespiCon sampler with the thoracic PM10 criterion collected less PM than a PM10 sampler with the USEPA criterion. The overall chamber experiment results indicated, when a PM10 sampler was used as a reference sampler, that (1) a RespiCon sampler had a normalizing factor of 1.6, meaning that this sampler underestimated an average 60% of PM10 mass sampled from a PM10 sampler, and (2) a DustTrak real-time monitor using a PM10 inlet had a calibration factor of 2.1.

Air Sampling For Volatile Organics Using an Adsorbent (흡착제를 이용한 휘발성 유기물 채취)

  • ;L.R.Berrafato
    • Journal of Environmental Science International
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    • v.1 no.1
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    • pp.41-46
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    • 1992
  • To perform a long-term ambient sampling study at a residential site, an air sampler was constructed to collect 24-hour integrated air samples suitable for the volatile organic compounds (VOCs) analysis. It includes an esthetically acceptance due to proximity to homes, as fell as providing the required sampling specifications. The VOCs sampler accomodates four 5/8 "stainless steel(SS) traps packed with adsorbent(Tenax) and is capable of four flow rates in the range of 5 to 50 cc/min. Sintered metal filters(10 micrometer) were directly connected to the inlet of the trap adapters. Additional specifications include: 1) constructed of organically inert materials, 2) weatherproof, 3) battery operated, 4) collecting of VOCs at a breathing zone level, and 5) quiet operation with micro diaphragm pumps wrapped by the sponge. The pump/battery system was separated from the sampling shelter. Sound levels measured for this system were below permissible sound levels (NJDEP) at a residential site. The sampler has been successfully operated at both ground level in a residential area and on the roof of a one story elementary school.hool.

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A Study on the Sample Characteristics Obtained from Large Diameter Sampler and Piston Sampler (피스톤 샘플러와 대구경 샘플러로 채취한 시료의 특성에 관한 연구)

  • Kim, Young-Chin;Kang, Jae-Mo
    • Journal of the Korean GEO-environmental Society
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    • v.6 no.3
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    • pp.5-15
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    • 2005
  • A large diameter sampler that can take undisturbed samples from soft ground was developed by KICT. In order to compare the quality of samples taken by the sampler with those of the traditional piston sampler, a series of laboratory tests were performed. Samples were taken at different sites such as Incheon, Gimhae, Yangsan and Busan. The results showed that the values of unconfined compression strength, secant modulus, pre-consolidation pressure, undrained shear strength, and shear modulus exhibited higher in samples taken by the large scale sampler. Strains at shear failure and volumetric strains were low for the new sampler. It was proved from the comparison that better quality samples could be obtained by the KICT sampler.

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An Improved Soil Core Sampler (개량(改良)된 토양(土壤) 코어 시료(試料) 채취기(採取器))

  • Hwang, Jae Hong;Son, Yowhan;Kim, Jong Sung
    • Journal of Korean Society of Forest Science
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    • v.90 no.6
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    • pp.788-791
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    • 2001
  • An improved double-cylinder hammer-driven sampling device was designed to extract undisturbed soil cores. The improvements consist of 1) separation of hammer from the driving head, 2) a split inside cylinder, and 3) a plastic sample holder. Pushing the sampler deep into the soil before hammering would result in less compression of the sample. Core samples should be taken in soils of medium moisture content. The improved soil core sampler provides sufficiently accurate volumetric soil samples with original soil layers and soil cores of 40cm in length and 5cm in diameter.

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지하수 수질 감시 기법

  • 정상옥
    • Water for future
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    • v.27 no.3
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    • pp.20-24
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    • 1994
  • 지하수 자원의 효율적인 이용과 보전을 위하여 필수적인 합리적인 수질감시를 위하여 지하수 수질 감시 사업의 계획수립 방법, 감시정 설치 방법, 지하수 수질 시료채취 방법 및 대수층 시험방법 등에 대하여 간단하게 소개하였으며, 또, 감시정 설치와 시료채취시에 필요한 장비 및 소모품 목록과, 시료 채취 장비의 종류와 특징을 소개하였다. 앞으로 지하수 관련 분야에 종사하는 분들에게 조금이라도 도움이 되었으면 하는 마음이다.

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Performance Characteristics of PM10 and PM2.5 Samplers with an Advanced Chamber System (챔버 기술 개발을 통한 PM10과 PM2.5 시료채취기의 수행 특성)

  • Kim, Do-Hyeon;Kim, Seon-Hong;Kim, Ji-Hoon;Cho, Seung-Yeon;Park, Ju-Myon
    • Journal of Korean Society of Environmental Engineers
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    • v.32 no.8
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    • pp.739-746
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    • 2010
  • The purposes of this study are 1) to develop an advanced chamber system within ${\pm}10%$ of air velocity at the particulate matter (PM) collection area, 2) to research theoretical characteristics of PM10 and PM2.5 samplers, 3) to assess the performance characteristics of PM10 and PM2.5 samplers through chamber experiments. The total six one-hour experiments were conducted using the cornstarch with an mass median aerodynamic diameter (MMAD) of $20\;{\mu}m$ and an geometric standard deviation of 2.0 at the two different air velocity conditions of 0.67 m/s and 2.15 m/s in the chamber. The aerosol samplers used in the present study are one APM PM10 and one PM2.5 samplers accordance with the US federal reference methods and specially designed three mini-volume aerosol samplers (two for PM10 and one for PM2.5). The overall results indicate that PM10 and PM2.5 mini-volume samplers need correction factors of 0.25 and 0.39 respectively when APM PM samplers considered as reference samplers and there is significant difference between two mini-volume aerosol samplers when a two-way analysis of variance is tested using the measured PM10 mass concentrations. The PM10 and PM2.5 samplers with the cutpoints and slopes (PM10: $10{\pm}0.5\;{\mu}m$ and $1.5{\pm}0.1$, PM2.5: $2.5{\pm}0.2\;{\mu}m$ and $1.3{\pm}0.03$) theoretically collect the ranges of 86~114% and 64~152% considering the cornstarch characteristics used in this research. Furthermore, the calculated mass concentrations of PM samplers are higher than the ideal mass concentrations when the airborne MMADs for the cornstarch used are smaller than the cutpoints of PM samplers and the PM samplers collected less PM in another case. The chamber experiment also showed that PM10 and PM2.5 samplers had the bigger collection ranges of 37~158% and 55~149% than the theocratical calculated mass concentration ranges and the relatively similar mass concentration ranges were measured at the air velocity of 2.15 m/s comparing with the 0.67 m/s.

The Comparison Study on the Concentration of $NO_{2}$, HCHO by Passive Sampler and Direct Reading Instrument (확산형 시료 채취기와 직독식 기기에 의한 이산화질소와 포름알데히드 농도의 비교)

  • Kim, Gyeong-Jin;Park, Ji-Yeon;Kim, Hyeong-A;An, Gyu-Dong
    • Proceedings of the Korean Environmental Health Society Conference
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    • 2005.11a
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    • pp.106-109
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    • 2005
  • 확산형 시료 채취기와 직독식 기기(공정시험법, Nitrogen Oxides Analyzer Model; EC 9841, Ecotech, Australia)에 의한 $NO_2$, 농도를 비교하고, 능동시료채취기(공정시험법)와 확산형포집기에 의한 HCHO(포름알데히드) 농도를 비교하기 위해 서울 ${\cdot}$ 경기 또는 대전, 충남 ${\cdot}$ 북지역에 소재한 11개 시설(종합병원 4곳, 노인 병원 1곳, 보건소 1곳, 복지관 3곳, 보육시설 2곳)을 대상으로 수행하였다. 1. 포름알데히드의능동 포집법(공정시험법)에 의한 시료(n=87)의 평균농도는 $11.44{\pm}11.07ppb$이고, 확산형 시료 채취기 의한 시료(n=40)의 평균농도는 $11.91{\pm}7.37ppb$으로 비슷한 값이 나왔고, 통계적으로 유의하지 않았다(p=0.806). 2. 포름알데히드 능동 포집법에 의한 농도와 확산형 시료 채취기에 의한 농도와의 상관계수 r=0.404(p=0.037)로 나타나 이 두 가지의 방법은 특정시간 포름알데히드 측정에 사용하여도 어느 정도 비교하기에는 적합할 것으로 생각된다. 3. 이산화질소의 노출정도는 직독식 기기(공정시험방법)와 확산형 시료 채취기로 각각 1시간 (오전, 오후 각각 2회), 8시간 측정하였다. 공정시험방법(n=61)에 의한 1시간-시료 평균농도는$44.48{\pm}37.96ppb$이고, 확산형 시료 채취기(n=61)에 의한 1시간-시료 평균농도는 $3.58{\pm}2.07ppb$으로 통계적으로 유의하였다(p=0.000). 직독식 기기(n=61)에 의한 8시간-시료 평균농도는 $34.85{\pm}22.83ppb$이고, 확산형 시료 채취기(n=61)에 의한 8시간-시료 평균농도 $8.32{\pm}4.44ppb$으로 통계적으로도 유의하였다(p=0.000). 4. 이산화질소를 직독식 기기(공정시험방법)와 확산형 시료 채취기로 측정한 1시간-시료 농도의 상관계수 r=0.253(p=0.268)이고 8시간-시료 일 때 상관계수 r=0.367(p=0.102)로 나타나 확산형 시료 채취기를 직독식 기기(공정시험방법) 대체 사용방법으로 이용하기에는 적합하지 않다고 생각된다.

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