• Proceedings of the Korea Water Resources Association Conference
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• 2008.05a
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• pp.933-937
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• 2008

유사(sediment)란 지각의 풍화작용에 의해 생성되어 유수나 바람 등에 의해 침식, 이송, 퇴적된 물질을 말하며, 일반적으로 하천유사(fluvial sediment)를 말한다. 유사의 크기는 작게는 미세한 점토입자부터 크게는 자갈에 이르기까지 매우 다양하며, 하천에서의 소류사량과 부유사량을 포함한 총유사량의 추정은 하천유사 문제의 기본이며 하천내의 수리구조물의 설계 및 유지관리, 하천개수 및 하도의 안정, 홍수터 관리, 저수지의 설계 및 운영 등 수자원 개발 및 관리를 위한 하천계획에 필요한 기본적 요소 중 하나이다. 본 연구에서는 중소하천에서의 실측을 통한 유사산정을 위해 대상하천에서 각 유량에 따른 부유사를 채취하여 시료분석을 통한 결과와 대상하천의 수리특성을 분석하여 총유사량의 산정 및 분석을 하였다. 이를 위하여 대상하천에 대하여 알맞은 측정조사지점을 선정하여 15회에 걸쳐 현장측정을 시행하였으며, 현장 측정시 유량측정을 위한 수위 및 유속을 측정하였고, 부유사농도 및 부유사입도분석을 위한 시료를 채취하여 실내 실험시 SS분석 및 BW관 분석을 시행하였다. 대상하천의 현장실험 측정성과와 수리특성을 기초자료로 하여 각 회차에 걸친 총유사량의 산정을 하였으며, 총유사량의 산정은 총유사량 추정 방법들인 직접 실측에 의한 방법, 간접계산에 의한 방법, '실측+계산'에 의한 방법 중 신뢰도가 높으며 경제성이 높은 '실측+계산'에 의한 방법과 간접계산에 의한 방법을 사용하는 공식으로 산정하였다. 결과들의 비교와 대상하천의 수리특성들에 대한 연구를 통해 적정공식을 선정하고 공식의 선정 원인에 대한 연구를 시행하였다.

• Journal of the Korean Geotechnical Society
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• v.17 no.4
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• pp.259-267
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• 2001

실내시험으로 구한 점토의 공학적 성질은 샘플링, 운반, 저장, 그리고 성형과정 동안에 발생하는 시료의 교란으로 인해 원지반의 성질과 다르게 측정된다. 본 연구에서는 양산점토에 대한 삼축압축시험($CK_{o}$ UC) 결과를 이용하여 샘플링 방법에 따른 교란의 정도를 평가하였다. 실험에 사용된 시료는 76mm 튜브샘플러, 76mm 피스톤샘플러, 블록샘플러로 채취되었으며, 시료의 교란정도를 평가하기 위해 각 시료에서 측정된 체적변형률, 비배수 전단강도, Secant Youngs modulus, 그리고 파괴시 간극수압계수를 비교하였다. 시료의 교란정도를 평가하는 것 이외에도 SHANSEP 방법을 이용하여 수행한 $CK_{o}$ U 삼축압축시험 결과를 이용하여 양산점토에 대한 정규화 전단강도($C_{u}$ /$\sigma$$_{vc}$ )와 OCR 관계를 규명하였다. 또, 피에조콘 관입시험, 딜라토메타 시험, 그리고 현장 베인시험결과를 이용하여 구한 양산점토의 비배수 전단강도를 삼축압축시험 결과와 비교하였다.

• Journal of the Korea Institute of Building Construction
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• v.23 no.2
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• pp.143-152
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• 2023

In this research, the microwave oven drying method was investigated as a potential accurate testing approach for determining the water content of fresh concrete. To do so, water content estimation formulas employed in three prominent oven drying test methods were selected, and the calculation principles for each equation, along with potential error factors arising during the actual testing process, were considered. Moreover, a concrete test was conducted to validate the possible error factors. Consequently, it was confirmed that estimation errors in the water content of fresh concrete can occur due to sample deviations arising during the wet screening process for creating mortar specimens or deviations in the coarse aggregate sampling quantity during the sample collection process.

• Analytical Science and Technology
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• v.23 no.3
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• pp.261-268
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• 2010

This study was performed to evaluate the PCBs-containing wastes using official test method. Ninety samples of transformer oil and various solid waste were collected to assess the analytical results. In the analysis of PCBs-containing wastes, the PCBs levels were detected in the range of 7.6 mg/kg to 23.8 mg/kg for transformer oils, $0.02\sim0.54\;{\mu}g/100cm^2$ for plat solid wastes, and 0.01~0.071 mg/kg for amorphous solid waste. In the cupper wire waste of the transformer with oil concentration level of 23 mg/kg, the analytical result exceed PCBs regulation level of 0.04 mg/kg. The new proposed analytical method for PCBs containing waste can be forced to effective management of the wastes.

• Proceedings of KOSOMES biannual meeting
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• 2007.05a
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• pp.21-26
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• 2007

The Protocol adopted in Sep. 1997 included the new Annex VI of MARPOL 73/78, which entered into force on 19 May 2005. Revision for the accept MARPOL Annex VI with make public on 29 Dec. 2005 and enforce on 29 Jun. 2006. For all that not installation at oil terminal or if installed do not used. The purpose of this study is to research and evaluate the methods of sampling and analysis, and the pollution measure of existed VOCs during the bulk liquid cargo operation at vessels. As the sampling instrument of VOCs, Tedlar bag has the effect of decrease in concentration by the chemical reaction and absorption, and the method using the solvent extraction has error cause because of the extraction, the absorption tube has error by the breakthrough. But canister is the best sampling instrument because of having no sampling mistake. The study on VOCs emission is not sufficient for the research on the pollution cause and the analysis data on the HAP during the bulk liquid cargo operation at vessels. Hence, monitoring on the management hazardous VOCs need to be continued during the cargo operation at vessels and VOCs management field must be study for the make progress at a good pace for reason of crew's health.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2005.06a
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• pp.151-157
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• 2005

For the treatment of regulatory clearance of the soils, a procedure for the radionuclides and radioactivity concentration analysis is under development. A strategy for soil sampling including random sampling after homogenization and standardization was set up. Statistical representativeness is considered for not only sampling strategy but also sample size. In this study, designed sample size was designed with confidence interval and error bound of soil using the pilot samples which were taken following the sampling strategy.

• Korean Journal of Soil Science and Fertilizer
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• v.38 no.1
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• pp.32-37
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• 2005

The procedure of soil sampling for on-farm quick test of soil nitrate is very important to improve practical application without weighing or drying soil. To improve application of test strip reflectometer as a quick on-farm analytical procedure for the estimation of soil nitrate concentration, three sampling methods such as gravimetric sampling (GS), particle density sampling (PDS) and bulk density sampling (BDS) for on-farm analytical procedure were investigated with twelve soils of 45 to $281mg\;kg^{-1}$ nitrate nitrogen concentration. The nitrate nitrogen concentrations measured from different soils were compared with two analytical methods, ion electrode method as a standard laboratory analysis (SLA) and test strip reflectometer at three moisture conditions, viz. air dried soil, 20 and 40% of maximum water holding capacity (MWHC). Nitrate nitrogen concentration measured by test strip reflectometer was significantly correlated with that of SLA, and the coefficients of variation (CV) were in the range of 3.5 to 10.9%. These CV values less than 10.9% were thought to be acceptable for the measurement of soil nitrate as an on-farm real time analytical procedure. The nitrate nitrogen concentration by BDS for test strip reflectometer as well as ion electrode method was more similar to that of SLA compared with those by GS and PDS especially in case of moist soils. This result suggests that the BDS is more useful than GS and PDS in case of on-farm analytical procedure of soil nitrate for moist soils. Further the practical measurement by BDS could be improved by substituting the bottle cap with a larger container.

• The Journal of Engineering Geology
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• v.24 no.1
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• pp.111-122
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• 2014

For accurate laboratory evaluations of soil deposits, it is essential that the samples are undisturbed. An artificial ground-freezing system is the one of the most effective methods for obtaining undisturbed samples from sand deposits. The objective of this study is to estimate the shear strengths and the characteristics of elastic waves of frozen-thawed and unfrozen specimens through the undrained triaxial compression test. For the experiments, Jumunjin standard sands are used to prepare frozen and unfrozen specimens with similar relative densities (60% and 80%). The water pluviation method is used to simulate the fully saturated condition under the groundwater table. When thawing the frozen specimens, the temperature is measured every minute. After the specimens are completely thawed, undrained triaxial compression tests are conducted using the same procedures as for the unfrozen specimens. During the triaxial tests (saturation, consolidation, and shear phase), compressional and shear waves are measured. The results show that the freeze-thaw process has minor effects on the peak deviatoric stress and shear strength values, and that the process does not affect the internal friction angle. The compressional wave velocity increases with increasing B-value to 1800 m/s in the saturation phase, but tends to remain constant in the process of consolidation and shearing. The shear wave velocity decreases with increasing B-value in the process of saturation, but changes velocity in accordance with the change in effective stress in the processes of consolidation and shearing. The compressional wave velocity has similar values regardless of the freeze-thaw process, but values of shear wave velocity are slighly lower in frozen-thawed specimens than in unfrozen specimens. This study is a preliminary experiment for estimating the shear strength and characteristics of elastic wave velocity in undisturbed frozen specimens that have been obtained using the artificial ground-freezing method.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.8 no.2
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• pp.91-97
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• 2010

As nuclear power plants are getting older, interests on a decontaminating process are increasingly attracting more attention. Chemical decontamination is crucial to lower the production of radioactive waste and radiation dose rate. Prior to this, oxidizers and detergents for target material should be chosen so as to decontaminate major systems and components of a nuclear power plant chemically. In order to decontaminate it properly, it is crucial to have information about the chemical composition and crystalline structure of CRUD, analyzing its samples from the target or the decontamination system with components. However, there is no program which enables the extraction of samples directly from the object or the decontamination system with components carrying genuine radioactivity. Therefore, it is limited to samples from corrosion products carrying partial radioactivity as a resource. The composition of CRUD varies considerably depending on refueling cycle because it is closely related to the constituent of basic material. After settling a target, it is crucial to analyze and obtain analytical information about CRUD as a decontamination target. In this paper, various technologies for manufacturing simulated CRUD are introduced as alternatives to unattained samples. A metal oxide or metal hydroxide was used to synthesize simulated cruds having chemical compositions and crystalline stricture similar to the actual one by 12 different methods. CRUD 4(metal oxides in the autoclave vessel) and CRUD 10(metal oxides in a crucible after hydrazing pretreatment)were chosen as the best method for Type 1 and Type 2.respectively. As these CRUD can be synthesized easily without using any specialized equipment or reagents in a short time and in large quantities, they are expected to stimulate the development of decontaminating agents and processes.

• Environmental Analysis Health and Toxicology
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• v.20 no.2 s.49
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• pp.123-131
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• 2005

본 연구는 GC/MS를 이용하여 수질, 토양 및 저질 시료 중의 4-Nitrotoluene(4-NT)을 분석하는 방법을 확립하고자 하였다. 4-NT은 수질 시료(100mL)에서 n-hexane으로 추출하였으며, 토양 및 저질 시료(10g)에서는 먼저 메탄올로 추출한 후 hexane으로 다시 추출하여 농축시켜 분석하였다. 수질 시료 중의 4-NT의 회수율은 $99.1\%$ 이상이였으며 토양에서의 회수율(recovery)은 약 $110\%$를 보였고 재현성 (relative standard deviation)은 $11.99\%$ 이하였다. 검정곡선은 상관계수$(R^2)$값이 수질과 토양 모두에서 0.994이상의 좋은 직선성을 보여주었다. 본 연구에서 채취한 수질 43개 지역, 토양 35개 지역 및 저질 11개 지역의 모든 시료에서 4-NT은 검출한계 이하로 나타났다. 이 분석방법은 환경 중에 미량으로 존재하는 4-NT의 분석과 모니터링에 유용하게 사용할 수 있는 적합한 방법이라 사료된다.