• Title/Summary/Keyword: 시료채취방법

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Nitrate Volatilization Associated with Fine Particles($PM_{2.5}$) Measurement (미세입자($PM_{2.5}$) 측정시 유발되는 질산염 휘발)

  • 강병욱;이학성
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2000.11a
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    • pp.81-82
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    • 2000
  • 미국 EPA에서 $PM_{2.5}$를 새로운 대기환경기준으로 설정함에 따라 $PM_{2.5}$를 측정하기 위한 새로운 Reference method가 설정되었다. 새로운 $PM_{2.5}$측정방법(Reference method)은 2.5$\mu\textrm{m}$ cut-diameter를 가진 cyclone을 통하여 16.7 L/min 유량으로 24시간동안 테프론 필터에 시료를 채집하는 것으로 규정하고 있다. 최근에 국내외에서 $PM_{2.5}$에 대한 활발한 연구가 수행되고 있으며 이들 연구의 대부분이 현재 미국 EPA의 $PM_{10}$ Reference method인 Dichotomous 샘플러를 이용하여 테프론 필터에 시료를 채취하고 있다 (중략)

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Dating of Resin Collection from Korean Red Pine (Pinus densiflora) at Mt. Worak and Investigation on the Tree' s Healing Ability using the Tree-ring Analysis Method (나이테 분석법을 이용한 월악산 소나무 송진채취 시기 및 상처회복능력 조사)

  • Lee, Yo-Seop;Seo, Jeong-Wook
    • Journal of Korean Society of Forest Science
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    • v.111 no.2
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    • pp.242-250
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    • 2022
  • Here we aimed to date the year and season of the resin collection from Korean red pines at Worak mountain and investigate the natural healing ability of the wounds using the tree-ring analysis technique. We determined the dating of the resin collection based on the synchronization between the ring-width time series from the wound surface of the experimental trees and the local master chronology, which is the mean time series from the sound surface on the opposite side of the wounds. For the dating of resin collection, we selected thirteen Korean red pines with resin wounds. For the investigation on the annual healing ability of the wounds, we sampled three dead trees out of 13 trees as disks. Through the comparison of the individual ring-width time series from the wounds with the local master chronology, it was verified that the resin collection was undertaken between the spring of 1962 and the autumn of 1975. The mean healing length of the wounds was 15.8 cm over the preceding 42 years, making their annual mean healing 0.38 cm. Through our study we successfully verified the healing ability of the wounded Korean red pines for the resin collection as well as the undocumented resin collection history.

남해 서부 연안 지역 지하수의 수리지구화학: 해수침투에 대한 예비 고찰

  • 신광섭;윤성택;허철호;이상규
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2002.04a
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    • pp.258-261
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    • 2002
  • 남해 서부 연안 지역 지하수의 해수 침투 영향을 광역적으로 파악하기 위하여, 186개소의 지하수 시료를 random하게 채취하고 수리지구화학 연구를 수행하였다. 전체 시료 중 23.6%에서 500$\mu\textrm{m}$/cm을 초과하는 높은 EC값을 나타내어 상당한 정도의 해수 영향을 반영해 주었다 또한, 해수 영향 판단의 또 다른 파라메터로 사용되는 Cl/HCO$_3$ 몰비 역시 전체 시료의 23%에서 1.3 이상의 값을 나타내었다. 한편, 대표적으로 해수침투 영향 및 인위적 오염의 영향을 각각 반영하는 것으로 알려진 Cl과 NO$_3$의 농도에 관한 누적도수분포도(cumulative frequency curve)를 작성하여 배경수질군과 오염영향군을 구분 짓는 배경치(background concentration)를 구한 결과, 각각 Cl : 22.4 mg/1 및 NO$_3$= 23.4 mg/1로 나타났다. 이 두 파라메터의 농도 분포를 활용하여 샘플링된 지하수 시료를 크게 4개의 그룹으로 나눌 수 있었다. 그 결과, 자연적 또는 인위적 기원이 오염이 배제된 그룹 1은 전체 시료의 32%, 자연적 오염(해수 영향)을 반영하는 그룹 2는 전체의 15%, 인위적 오염의 영향을 반영하는 그룹 3은 전체의 7%, 해수 영향 및 인위적 오염을 동시에 반영하는 그룹 4는 전체의 46%로 나타났다 그룹 4 중 Piper diagram 상에서 Na-Cl 유형으로 점시되어 해수 영향을 강하게 반영하는 일부 시료와 그룹 2의 시료를 합쳐 보면, 전체 지하수 시료의 약 23%에서 해수의 영향을 반영하고 있다. 따라서, 여러 지구화학 방법에 의한 해수 영향 판단 결과는 서로 잘 일치하고 있음을 알 수 있다. 결국, 지구화학적 파라메터를 종합적으로 활용함으로써, 연안 지역 해수침투의 효과적인 파악은 물론 예측 및 방지, 복구에 효과적으로 사용될 수 있을 것으로 판단된다.

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The method for applying International Standards to Korean Industrial Standards in Construction fields - The standards of sampling and testing the fresh concrete - (건설분야에서 국내표준과 국제표준의 부합화 방안 - 콘크리트 시료채취와 시험방법에 대한 규격을 중심으로 -)

  • Lee Teck-wn;Kuk Chan-ho;Han Choong-hee
    • Korean Journal of Construction Engineering and Management
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    • v.2 no.4 s.8
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    • pp.107-116
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    • 2001
  • As the international trade has been increased, unified worldwide standards are getting more important and necessary. At the TBT(Agreement on Technical Barrier to Trade) of WTO(World Trade Organization) and the CTI meeting of APEC(Asia-Pacific Economic Cooperation), they made an agreement with applying International Standards to National Standards gradually. In addition, ISO (International Organization for Standardization) established the ISO/IEC Guide 21, a guideline for applying International Standards to National Standards. In these environment, Korean Industrial Standards has to be prepared for it. This paper introduce the comparison between Korean Industrial Standards and ISO Standards about the standards of sampling and testing the fresh concrete, based on ISO/IEC Guide 21 by ISO and the Applying guideline by Korean Agency for Technology and Standards, and then discuss the problem about applying them. The overall objective is to establish the applying guideline on construction fields, which is civil and building engineering part(KS F) of Korean Industrial Standards.

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Examination about evaluation method of odor active compounds in evaporator by using condensed water (응축수를 이용한 냉각기의 냄새원인물질 평가방법 검토)

  • Kim, Sun-Hwa;Kim, Kyung-Hwan;Jung, Young-Rim;Kim, Man-Goo;Kim, Jae-Ho;Park, Ha-Young;Ji, Yong-Jun
    • Analytical Science and Technology
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    • v.20 no.5
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    • pp.361-369
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    • 2007
  • Uncomfortable odor emitted from air conditioning system is the main cause of indoor air quality deterioration. To solve evaporator odor problems, odor active compounds, have to be identified then the quality of the product can be improved its quality. Because evaporator odor in exhaust gas has low odor intensity and discontinuity, it is very difficult to collect and analyze sample. In this study through the identification of odor compounds in condensed water, the evaluation of the eraporator was tested. Odor compounds were extracted from water by headspace-solid-phase microextraction (HS-SPME) method. The single odor was separated by GC/FID/Olfactometry (GC/FID/O) and odor active compounds were identified by GC/AED and GC/MS. Compared to air sample, result of sensory evaluation and the single odor compound appeared similarly. It was identified that odor active compounds have functional group containing oxygen such as alcohols and acids. Evaluation method of odor active compounds using condensed water in evaporator appeared effective on the side of simplicity of collection, low expanse and rapid analysis.

A Study of Seawater Sterilization for Ballast Water using solution plasma (수중방전에 의한 선박평형수 처리에 관한 연구)

  • Choe, Jong-Beom;Yang, Jeong-Hyeon;Kim, Yeon-Won;Gang, Jun;Lee, Myeong-Hun;Yun, Yong-Seop
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.141-141
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    • 2017
  • 국제해사기구(International Maritime Organization)는 선박 평형수로 인하여 발생하는 환경문제를 방지하기 위하여 지난 2004년 선박 평형수 관리 협약을 제정하였고, 2016년 핀란드의 비준함에 따라 2017년 9월 8일부터 발효될 예정이다. 이 협약에 대응하기 위하여 선박 평형수 처리기술이 개발되어 승인이 되었다. 이중 수중방전을 이용한 기술은 화학약품의 첨가 등이 없어 경제적이고 내부에서 발생하는 OH라디컬, 자외선, 충격파, 전기장, 오존 등에 다양한 요소들에 의하여 수처리가 가능하고, 중화를 위한 첨가제 등이 필요없어 친환경적이다. 본 연구에서는 부산 항만 근처연안에서 채취한 바닷물을 대상으로 수중방전을 이용한 방법을 연구하였다. 실험방법은 그림1과 같이 Point to Point 방식의 전극을 꾸몄고, 용액은 1L이며, 전압은 8kV, 30kHZ로 가해주었다. 광학분석장비(OES)를 이용하여 수중방전시 발생되는 빛 분석을 하였다. 실험결과 OES분석 결과 살균작용하는 OH 라디컬이 발생하는 것을 확인할 수 있었다. 또한 실험 도중 시료를 채취하여 $35^{\circ}C$ 48시간동안 배양하였다. 배양 결과 시간이 경과함에 따라 미생물의 개체가 그림 2와 같이줄어두는 것을 확인할 수 있었다.

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NMHCs measurement using a cryogenic concentration system and application on gas samples (저온농축장치를 이용한 NMHCs의 측정법과 가스 시료에 적용)

  • Kim, Su Ha;Moon, Dong Min;Kim, Jin Seog
    • Analytical Science and Technology
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    • v.25 no.6
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    • pp.375-381
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    • 2012
  • In this study, we have developed a cryogenic concentration system for the analysis of non-methane hydrocarbons (NMHCs) in air sample. NMHCs with nmol/mol level of concentrations in the atmosphere were quantified by a comparative method with certified reference gas mixture. GC/FID with cryogenic concentration system operated in the range from $-67^{\circ}C$ to $180^{\circ}C$ was adopted. After cryogenic concentration, a fast desorption by heating could achieve a large amount of sample injection into the GC/FID. The linearity of the system was verified with the peak areas of NMHCs of the concentration amount of sample. The reproducibility is less than 10% and the limit of detection (LOD) is 0.1 nmol/mol. For the application of this system, we analyzed NMHCs in gas samples taken from air and soil in Daejeon, Seosan and Goheung.

Design and Evaluation of a Flow Rotate Divider for Sampling Runoff Plots. (토양 유실량 및 유출수량 측정을 위한 회전분할집수기의 평가)

  • Zhang, Yong-Seon;Park, Chan-Won;Lee, Gye-Jun;Lee, Jeong-Tae;Jin, Yong-Ik;Hwang, Seon-Woong
    • Korean Journal of Soil Science and Fertilizer
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    • v.41 no.6
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    • pp.374-378
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    • 2008
  • For the standard method of collecting the run-off, it is consumed the high cost and much effort to install and to manage this instrument. Because the all the soil and water from reservoir tank must be eliminate after their measurement of amount of soil loss and run-off and installed the reservoir tank at regular size in the experimental field. Therefore, objective of this study was to compare its efficacy between the standard method and a flow rotate divider for ontinuously collecting and measuring the soil loss and run-off in order to conveniently conduct the field experiment of the lysimeters. For collecting the sampling of soil loss and run-off from agricultural land with invariable ratio, a flow rotate divider was consisted with a 8 blades of round plate sloped in order to collect the invariable ratio of soil and water at lowest part from round plate by the law of gravity. For comparing its accuracy in the batch scale experiment, it shown that there was significantly a positive linear corelation ($r=0.997^{***}$) between flowing and sampling amounts with adjusting the range from 1 to $10L\;min^{-1}$ with flowing rate. In collecting ratio in the field experiment, it observed that the more its accuracy had, the more soil loss and run-off.

Seasonality of shellfish gathering using oxygen isotope analysis of Crassostrea gigas from the Gagok-ri shell midden site, Dangjin (산소동위원소 분석을 이용한 당진 가곡리 패총 굴 (Crassostrea gigas) 의 채집 계절 연구)

  • An, Deogim;Lee, Insung
    • The Korean Journal of Malacology
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    • v.30 no.1
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    • pp.1-8
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    • 2014
  • Oxygen isotope analysis was carried out on a oyster (Crassostrea gigas) from the neolithic age Gagok-ri shell midden site, Dangjin, Korea to determine the seasonality of shellfish gathering and site occupation. Isotope samples were taken from the hinge section of the left valve of the oyster. The isotope values of the shell range from -2.02‰ to -6.05‰ vs PDB. The isotope profile shows a seasonal temperature cycle, providing information related to seasonality of shellfish gathering. The isotope values towards the edge of the hinge are gradually increasing, suggesting progressively cooling and a fall period of shell gathering and site occupation. The result shows that the oxygen isotope analysis using oyster shell hinges can be used for archaeological seasonality studies.

A Technical Note on Monitoring Methods for Volcanic Gases (화산가스의 채취 및 분석에 대한 기술보고)

  • Lee, Seungyeol;Lee, Sangchul;Yang, Kyounghee;Jeong, Hoon Young
    • The Journal of the Petrological Society of Korea
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    • v.21 no.4
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    • pp.415-429
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    • 2012
  • The monitoring methods for volcanic gases are divided into remote sensing and direct gas sampling approaches. In the remote sensing approach, COSPEC and Li-COR are used to measure $SO_2$ and $CO_2$, respectively, with FT-IR for detection of a range of volcanic gases. However, the remote sensing approach is not applicable to Mt. Baegdu, where the atmospheric contents of volcanic gases are very low as a result of the strong interaction of volcanic gases with the nearby surface water and groundwater. On the other hand, the direct gas sampling approach involves the collection of volcanic gases from volcanic vents or fumaroles and the subsequent laboratory analysis, thus making it possible to measure even very low levels of volcanic gases. The direct sampling approach can be subdivided into the evacuated bottle method and the flow-through bottle method. In applying both methods, sampling bottles typically contain reaction media to trap specific volcanic gases. For example, NaOH solution(Giggenbach bottle), $NH_4OH$ solution, and acid condensates have been experimented for volcanic gas sampling. Once taken from vents and fumaroles, the samples of volcanic gases are pretreated and subsequently analyzed for volcanic gases using GC, IC, HPLC, titrimetry, TOC-IC, or ICP-MS. Recently, there has been the increasing number of evidences on the potential volcanic activity of Mt. Baegdu. However, little technical development has been made for the sampling and analysis of volcanic gases in Korea. In the present work, we reviewed various volcanic gas monitoring methods, and provided the detailed information on the monitoring methods applied to Mt. Baegdu.