• Journal of the Korean Society of Propulsion Engineers
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• v.20 no.1
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• pp.37-42
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• 2016

In this study, we examined the burning rate of the uncured propellant (with and without a curing agent application) in order to inspect the process of the HTPB solid propellant. The burning rate of the uncured propellant, that did not contain the curing agent, was approximately 9.7 mm/s at 1000 psi. In relation to the curing time, the burning rate was constant. The propellant, with the curing agent application, was approximately 8.1 mm/s showed a tendency of slowing as it burned. When the cure reaction rate was low, in accordance to the time, there were small changes in burn rate. However, when the cure reaction rate was high, the difference in burning rate was increased. The burning rate of a fully-cured propellant was approximately 6.8 mm/s, which appeared to be the lowest in order.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.4
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• pp.24-32
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• 2008

We made a new propellant formulation to improve the productivity of Base Bleed Unit(aka BBU) by reducing of the curing time. We made an experiment with new propellant formulation such as binder characteristics and manufacturing process. In addition, we already tested several basic characteristics and the final performance of the new propellant. According to the test report, it was not only satisfied with all requirements in the specification, but it also contributed to improve productivity and reduced 53% of the curing time.

• Applied Chemistry for Engineering
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• v.16 no.2
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• pp.292-295
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• 2005

The curing time of the phenolic resin for the processing of brake pad is very important factor for reducing the processing cost. The curing time could be investigated by examining the reaction time of the phenolic resin and hexamethylenediamine. The reaction time has been studied by FT-IR, Differential Scanning Calolimetric Analysis (DSC), and Thermogravimetric Analysis (TGA).

• Polymer(Korea)
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• v.38 no.2
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• pp.171-179
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• 2014

Low temperature cure prepregs are being developed for use in the preparation of large-structured fiber-reinforced polymer (FRP) composites with good performance. Cure behavior and chemorheology of low temperature cure epoxy resin system, based on epoxy resin, curing agent, and accelerators, were investigated to provide a matrix resin suitable for the prepreg preparation. Characteristics of cure reaction were studied in both dynamic and isothermal conditions by means of differential scanning calorimetry and rheometry. The low temperature cure epoxy resin system suggested in this study as a matrix resin was curable at $80^{\circ}C$ for 3 h, and showed the gel times of 120 and 20 min at 80 and $90^{\circ}C$, respectively. Thermal and mechanical properties of the cured sample were almost the same as high temperature cure counterparts.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.04a
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• pp.929-932
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• 2008

The unsaturated polyester(UP) and epoxy resin have a superior material properties and a chemical resistance using sewerage pipes rehabilitation. However, UP and epoxy have not a low temperatures harding, the requirement $8{\sim}11$ hours long times harding and heating system used by reinforcement liner. This study is to evaluate the effects of low temperature harding properties methyl methacrylate(MMA) monomer using expanded polystyrene(EPS) in addition of initiator and promoters. From the test result, viscosity tends to increase with increasing EPS contents. However, harding time change of the MMA resins which it follows in addition of the initiator and promoter.

• Composites Research
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• v.37 no.3
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• pp.215-218
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• 2024

Liquid crystalline thermosetting epoxy oligomer DD-A was synthesized with Diglycidyl ether of 4,4'-dihydroxy-α-methylstilbene (DGE-DHMS) and aniline in a ratio of 2:1 and cured with a catalytic curing agent, 1-Methyl Imidazole. The gelation times and vitrification times were measured to create Time-Temperature-Transition Diagrams with liquid crystalline phase changes. It was found that the gelation and vitrification times were decreased as the concentration of curing agent increased, and the vitrification curve showing a typical S-shape was confirmed.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2008.11a
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• pp.114-114
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• 2008

자동차 보수도료 경화는 주로 열풍방식을 사용하고 있지만 적외선 가열방식을 사용하면 품질이 향상 되고 에너지 절약 등의 이점이 있다. 따라서 자동차 보수도료의 경화용으로 사용할 적외선 방사체를 개발하였다. 자동차 보수도료의 적외선 흡수 스펙트럼과 적외선 방사체 방사 스펙트럼이 일치해야 도료의 경화효율이 우수해짐을 알 수 있었고 열풍방식과 비교하여 경화된 도막의 품질 및 경화시간에 대한 실험데이터를 분석하였다.

• Journal of the korean academy of Pediatric Dentistry
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• v.38 no.3
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• pp.229-236
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• 2011

ProRoot MTA(Dentsply Tulsa, U.S.A) which has similar component with Portland cement has setting expansion character and long setting time. Excessive expansion can cause fracture at the apical portion of the root and decreasing of volume stability. And the long setting time makes additional visits for crown restoration and slow setting process of this material can change physical properties itself. In this study, among requirements of root canal filling material(KS P ISO 6876) which is revised at 2008, we investigated the setting time and setting expansion. Objects are recently developed OrthoMTA(BioMTA, Korea), conventional ProRoot white MTA(Dentsply Tulsa, U.S.A) and White portland cement(Union, Korea). The results in setting expansion, OrthoMTA was $0.08{\pm}0.02%$, ProRoot white MTA and White portland cement were each $0.28{\pm}0.06$, $0.80{\pm}0.25%$(p<0.05). The results in setting time, OrthoMTA, ProRoot white MTA, White portland cement were each $307.78{\pm}3.83$ min, $150.44{\pm}2.35$ min, $235.33{\pm}9.07$ min(p<0.05).

• Journal of Adhesion and Interface
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• v.21 no.2
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• pp.65-70
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• 2020

Epoxy adhesive was mainly used to combine different composite materials. Epoxy adhesive was a typical thermosetting resin that can be bonded by changing from a linear structure to a three-dimensional network structure by curing reaction of epoxy and hardener. The curing conditions of epoxy adhesive were different with different types of hardener such as mixing ratio, curing time, and temperature. These curing conditions affected to the adhesive property of epoxy adhesive. In industry, it was difficult to proceed the applying epoxy adhesive and combining two parts immediately. The adhesive property decreased by humidity and pre-curing of epoxy adhesive in waiting time between two processes. In this paper, the glass fiber reinforced composite (GFRC) was combined with epoxy adhesive and adhesion property between epoxy adhesive and GFRCs was evaluated using single lap shear test. The different waiting times and humidity conditions were applied to epoxy adhesive in room temperature and adhesive property decreased as the waiting time increased. In small amount of humidity, the adhesive property increased because a small amount of moisture in the surroundings accelerated the curing reaction. In certain amount of humidity, however, the adhesion property decreased.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.233-233
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• 2009

기존 표면열처리기술에 단점인 대면적, 신속열처리를 위해 수중플라즈마 기술을 이용하여 표면경화와 경화 깊이층 제어를 실시였다. 수중플라즈마의 전원장치에 전압과 주기적인 전압과 시간을 달리하여 각각의 시편의 경도변화와 미세조직변화를 관찰하였다. 300V이상의 전압에서는 마르텐사이트가 관찰되었으며, 300V이하에서는 초석페라이트와 펄라이트가 혼합된상의 구조를 관찰할 수 있었다. 주기적인 전압과 시간을 달리하여 표면에서부터 $300{\mu}m$ 깊이만의 마르텐사이트로 형성시켜 경화 깊이층 제어가 가능하였다.