• Title/Summary/Keyword: 순도

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Study on the Long-term Thermal Stability by DSC & ARC and its ISCO behaviors with different AP Quality (DSC, ARC, ISCO를 활용한 다양한 순도를 가진 AP의 장기 열적안정성 연구)

  • Kim, Seunghee;Kwon, Kuktae;Lee, So Jung
    • Journal of the Korean Society of Propulsion Engineers
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    • v.22 no.2
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    • pp.59-65
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    • 2018
  • We conducted an isothermal slow cook-off(ISCO) test for an aluminized explosive containing AP. The sample bulged before the run-away reaction, and therefore we were unable to obtain the ISCO data. However, these phenomena did not occur for a certain AP grade, which means that the quality of the AP exerted a significant effect on the thermal stability of the explosive formulation. In this study, we investigated the thermal stability difference between a good and bad AP grade. First, we characterized the thermal properties of all APs by Differential Scanning Calorimeter(DSC) and correlated them to the ISCO phenomena. In addition to the DSC study and ISCO test, we also investigated and calculated the SADT and self-heating rate by the ARC of the different AP qualities to interpret the thermal stability of the explosive formulation. Moreover, we investigated the impurity of the AP and a preparation method to remove the included impurity and crystallization. Finally, we implemented qualification methods to identify the quality of AP by DSC using a high-pressure crucible.

Preparation and Characterization of Highly Pured Water-soluble Chitosan Oligosaccharides as Biomaterials (생체재료로서의 고순도 수용성 키토산 올리고당의 제조와 특성)

  • Park, Jun-Kyu;Choi, Changyong;Nam, Joung-Pyo;Park, Seong-Cheol;Park, YungHoon;Jang, Mi-Kyeong;Nah, Jae-Woon
    • Polymer(Korea)
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    • v.38 no.1
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    • pp.85-92
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    • 2014
  • To develop water-soluble chitosan as an effient gene delivery carrier, chitosan oligosaccharides (COSs) with various molecular weights (MW) were studied for gene transfection agents. MWs of COSs fractionated by ultrafiltration techniques were identified as narrow MW distributions with the average MW ranging from 1 to 10 kDa through gel permeation chromatography (GPC) measurement depending on the applied ultrafiltration membranes. Their structural characterizations were analyzed by FTIR spectrophotometer and $^1H$ NMR. The degree of deacetylation was determined by UV spectroscopy showing the degree of deacetylation above 90%. The relative cell viabilities were maintained over 100% (10 mg/mL), independent of the MW of the fractionated COSs. The fractionated COSs of 10 mg/mL concentration with narrow MW distributions showed non-cytotoxicity in Caco-2 cells.

Evaluation on the Whitening Effect of Nypa fruticans wurmb Extracts (해죽순 추출물의 미백활성 평가)

  • Kim, Il-Chool
    • Journal of the Korean Applied Science and Technology
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    • v.39 no.3
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    • pp.462-470
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    • 2022
  • The purpose of this study was to investigate the role of the Nypa fruticans extracts as a cosmetic additive. The tyrosinase inhibitory effects showed 52.0% at 1,000 ㎍/mL concentration. A cell viability test, measured on melanoma cell (B16F10) hot water extract of nypa fruticans showed 84.8% at 100 ㎍/mL concentration. The protein expression inhibitory effects of nypa fruticans extracts were measured by western blot at 25, 50, 100 ㎍/mL concentration and the β-actin. Results showed that the expression inhibition rates of the MITF, TRP-1, TRP-2, tyrosinase protein were decreased by 70.7%, 83.3%, 45.7%, 45.9% at 100 ㎍/mL concentration, respectively. It was concluded that nypa fruticans extracts had the whitening effects and thus could be applied for cosmetics as a natural ingredient.

Effect of Young Phragmites communis Leaves Powder on Lipid Metabolism and Erythrocyte Antioxidant Enzyme Activities in High-Fat Diet Fed Mice (갈대순분말이 고지방을 급여한 마우스의 지질대사 및 적혈구 항산화방어계에 미치는 영향)

  • Lee, Jin;Jeong, Joo-Yong;Cho, Young-Sook;Park, Seok-Kyu;Kim, Kwang-Jin;Kim, Myung-Joo;Lee, Mi-Kyung
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.39 no.5
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    • pp.677-683
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    • 2010
  • This study investigated the effect of young Phragmites communis (Pc) leaves on lipid profiles, lipid metabolism and erythrocyte antioxidant defense system in high-fat diet fed mice. Three groups of mice were fed different diets for 8 weeks: normal diet (Normal), high-fat diet (High-fat; 37% calories from fat) and high-fat diet supplemented with 1% Pc (wt/wt, HF-Pc). Body weight, daily food intake and energy intake tended to decrease by Pc supplement in high-fat fed mice. Pc supplementation significantly lowered plasma triglyceride and total cholesterol concentrations compared to the high-fat control group. Pc also lowered hepatic and heart cholesterol contents, whereas it significantly increased fecal excretion of triglyceride and cholesterol compared to the high-fat control group. Pc significantly inhibited fatty acid synthase, 3-hydroxy-3-methylglutaryl CoA reductase and acyl-CoA:cholesterol acyltransferase activities compared to the high-fat control group. Erythrocyte superoxide dismutase and catalase activities were also significantly higher in the high-fat group than in the normal group, however Pc supplementation reversed these changes. The Pc supplementation significantly lowered erythrocyte lipid peroxidation level compared to the high-fat control group. Accordingly, these results suggest that Pc improves lipid metabolism and erythrocyte antioxidant defense system in high-fat diet fed mice.

Weed Occurrence in Apple Orchard in Korea (우리나라 사과원(園)의 잡초식생(雜草植生)에 관(關)한 분석(分析))

  • Jung, J.S.;Lee, J.S.;Choi, C.D.
    • Korean Journal of Weed Science
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    • v.17 no.2
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    • pp.147-156
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    • 1997
  • The survey of weed population in apple orchard was conducted to investigate basic information on weed flora and its ecology at 27 locations in 1996. The weed species observed include 7 species of grasses, 60 species of broadleaves and 2 species of sedges, and the ratio of annual weed vs perennial weed was 64 : 36. Major dominant weed species by frequence were Chenopodium album, Capsella bursa-pastoris, Digitaria sanguinalis, Rorippa islandica, Alopecurus aequalis and Erigeron canadensis. While, on the basis of dry weight, the most dominant weeds were C. album followed by E. canadensis, A. aequalis, R islandica and R indica. The dominant weed species in middle-north Kyeongbuk region were C. bursa-pastoris, C. album, R indica and R islandica, were E. canadensis, Persicaria hydropiper, A. aequalis and Arenaria serpylliforia in Chungbuk region and were A. aequalis, E. canadenris and R islandica in Honam region.

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Change in tooth length and angulation on panoramic radiographs taken at different labiolingual and buccolingual inclinations (치아의 순(협)설 경사도 변화에 따라 파노라마 방사선 사진에 나타난 치아 길이 및 각도 변화)

  • Choi, Gab-Lim;Lim, Sung-Hoon;Kim, Jae-Duck;Kim, Kwang-Won
    • The korean journal of orthodontics
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    • v.37 no.2 s.121
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    • pp.114-124
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    • 2007
  • Objective: The purpose of this study was to examine how the mesio-distal angulation and the length of each tooth changes on panoramic radiograph at different bucco-lingual inclinations. Methods: After constructing an acrylic model based on the mean arch of 30 adults with normal occlusion, the wire was placed in the center of the teeth on the acrylic model. First, the wire was implanted in normal angulation and inclination and a panoramic radiograph taken. After changing the inclination from $I-5^{\circ}\;to\;I+15^{\circ}\;by\;5^{\circ}$, a panoramic radiograph was taken again and the mesio-distal angle and wire length on the panoramic radiograph were assessed. Results: When the wire was implanted at the normal angulation and inclination, the length measured in the panoramic radiograph was magnified $111{\sim}117%$ from the original length in the anterior region and $121{\sim}125%$ in the posterior region. Only the central and lateral incisors showed significant length differences when the inclination was changed from $l-15^{\circ}\;to\;I+15^{\circ}$ at fixed angulation. When the inclination was changed from $l-15^{\circ}\;to\;I+15^{\circ}$, the angulation of most teeth on panoramic radiograph appeared to be more disto-angulated than in reality, and the lateral incisor and canine showed the largest difference. Only $l-15^{\circ}\;to\;I+15^{\circ}$ groups of premolars and $I+15^{\circ}$ group of molars showed more mesio-angulation than in reality. As the labio(bucco)lingual inclination of all teeth were decreased, tooth angulation in the panoramic radiograph appeared to be more disto-angulated. Conclusion: The labio-liugual inclination of teeth should be considered because it affects panoramic image of teeth, such as length of incisors and angulation of other teeth.

Anti-inflammatory effect of barley leaf ethanol extract in LPS-stimulated RAW264.7 macrophage (LPS로 자극한 RAW264.7 대식세포에서 보리순 에탄올 추출물의 항염증 효과)

  • Kim, Mee-Kyung;Kim, Dae-Yong
    • Food Science and Preservation
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    • v.22 no.5
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    • pp.735-743
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    • 2015
  • This study investigated the anti-inflammatory activity of barley leaf extract in lipopolysaccharide (LPS)-stimulated RAW264.7 cells and hairless mice. Pre-treatment with barley leaf extract significantly inhibited the protein expression of inducible nitric oxide synthase (iNOS) and cyclooxygenase-II (COX-II) in a dose-dependent manner in LPS-stimulated RAW264.7 cells. Barley leaf extract also significantly inhibited the secretion of inflammatory cytokines, such as tumor necrosis factor-${\alpha}$ (TNF-${\alpha}$), interleukin-$1{\beta}$ (IL-$1{\beta}$), and interleukin-6 (IL-6). Moreover, phosphorylation of mitogen-activated protein kinases (MAPKs) and nuclear translocation of nuclear factor-kappa B (NF-${\kappa}B$) were strongly suppressed by barley leaf extract in LPS-stimulated cells. In hairless mice, barley extract significantly decreased the pathological phenotypes of contact dermatitis, such as erythema, edema, and scabs. These results indicate that barley leaf extract has an anti-inflammatory effect and therefore a possible role in the treatment of inflammatory diseases or in functional cosmetics.

Design and Construction of the Sprout Trimmer for a 3-Wheel Riding Type Cultivating Vehicle (3륜 승용관리기용 순 지르기 작업기 설계 제작)

  • Choi, Il Soo;Choi, Yong;Lee, Beom Seob;Ji, Keum Bae;Yun, Young Tae;Yoo, Soo Nam
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2017.04a
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    • pp.75-75
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    • 2017
  • 3륜 승용관리기는 4륜 승용관리기에 비하여 작업기를 복부에 장착함으로 작업의 정밀도, 편이성, 관측의 용이성 향상과 함께 지상고 제고, 차폭 조절, 조향 등의 성능 개선을 기할 수 있다. 국내에서는 3륜 승용관리기용 복부 장착 부속작업기가 거의 개발되어 있지 않으며, 특히 두류 재배에 있어서 일관기계화 작업을 위한 관리작업기의 개발이 매우 필요한 실정이다. 콩의 순 지르기 작업은 콩이 지나친 생육을 한 경우 미리 줄기의 윗부분을 제거하는 저심처리를 해주면 곁가지들의 왕성한 생육을 유도하여 많은 꼬투리를 얻고 쓰러짐도 줄어들어 수량을 높일 수 있다. 순 지르기 작업은 보통 낫이나 배부식 예취기를 이용하여 작업함으로 노동력이 많이 들고 작업부담이 심하여 개선이 필요한 실정이다. 따라서 본 연구는 3륜 승용관리기에 적합한 복부장착형의 순 지르기 작업기를 설계 제작하였다. 3륜 승용관리기용 순 지르기 작업기는 승용관리기의 복부 PTO에서의 구동력 전달을 위한 연결 조인트, 중간축, 기어 전동기구, 구동축으로 구성된 동력전달부, 2 조의 원판형 작업 날, 다양한 조간거리에 적응을 위한 조간조정 나사부, 3륜 승용관리기에의 부착을 위한 프레임 및 부착보조 작업기 이동용 바퀴장치 등으로 구성 설계 제작하였다. 원판형 칼날은 시판 중인 예취기의 외경 305 mm, 칼날 톱니 수 90개의 초경 비트 부착 날을 사용하였다. 작업 날의 승강높이는 150~540 mm 범위로 조절하도록 하였다. 조간거리의 조절범위는 수동나사에 의하여 660~860 mm 범위로 무단조절 할 수 있도록 하였다. 순 지르기 작업기는 3륜 승용 관리기 복부의 평행링크에 부착되므로 작업기의 이동 및 부착 편이를 위하여 이동용 바퀴를 설치하였다. 제작된 순 지르기 작업기의 크기는 길이${\times}$${\times}$높이가 $514{\times}1138{\times}810mm$, 중량은 약 100 kg으로 제작되었다.

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Purity Improvement of Calcium Lactate and Calcium Citrate Prepared with Shell of Anadarac tegillarca granosa (꼬막 패각으로 제조한 젖산칼슘과 구연산칼슘의 순도 향상에 대한 연구)

  • Kang mee-Sook;Soh Gowan-Soon;Shin Dong-Hwa
    • Journal of Food Hygiene and Safety
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    • v.20 no.3
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    • pp.128-133
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    • 2005
  • Ash of Anadarac tegillarca granosa shell was used for preparation of calcium lactate and calcium citrate, and improvement of their purity was carried out by using ammonium chloride process (ACP) and ammonium nitrate process (ACP). Purity of calcium lactate and calcium citrate made by the reaction of ash of Anadarac tegillarca granosa shell with lactic acid solution and with citric acid solution was 94.35-96.72 and $87.58-93.06\%$, respectively. However, purity of calcium lactate and calcium citrate prepared with purified calcium carbonate pre-purified from the ash of Anadarac fegiliarca granosa shell using ACP and ANP method was 99.53-100.34 and $99.32-99.88\%$, respectively. The purity of these calcium products were higher than those of calcium lactate and calcium citrate made with ash of Anadarac tegillarca granosa shell. Whiteness of calcium lactate and calcium citrate prepared with purified calcium carbonate pre-purified using ACP and ANP method was 94.8-98.5 and 99.4-101.5, respectively. Whiteness of these calcium products was higher than that of calcium lactate (91.8) and calcium citrate (92.9) made with the ash of Anadarac tegillarca granosa shell. Therefore, we estimated that calcium lactate and calcium citrate prepared with purified calcium carbonate using ACP and ANP method could be used potentially as a food additive for calcium supplement.

Effect of Organic Materials and the Removal of Apical Shoot on Controlling Cucumber Downy Mildew (유기농업자재와 순지르기를 이용한 오이 노균병 방제)

  • Park, Jong-Won;Kim, Yong-Ki;Park, So-Hyang;Hong, Sung-Jun;Shim, Chang-Ki;Kim, Min-Jeong;Park, Jong-Ho;Han, Eun-Jung;So, Hyun-Gyu;Kim, Seok-Cheol
    • Korean Journal of Organic Agriculture
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    • v.24 no.4
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    • pp.919-929
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    • 2016
  • This study investigated the effect of organic materials (Bordeaux, Loess-sulfur) and the removal of apical shoot against downy mildew disease on cucumber cultivated in greenhouse. Five kinds of Bordeaux were made by adjusting mixing ratio of lime and copper sulfate in order to elucidate the optimal combination. The 4-6type Bordeaux was selected as the most effective combination for controlling cucumber downy mildew. Loess-sulfur showed inhibitory activity against cucumber downey mildew, but it was less effective than Bordeaux. It was confirmed that apical shoot cutting could reduce the incidence of cucumber downy mildew disease by 56.3%. When apical shoots of susceptible cucumber variety were cut at different leaf stages, disease incidence by early apical shoot cutting treatment was lower than that of late apical shoot cutting treatment. However in a resistant variety, 'Heukryungsamcheok', disease incidences of all cucumber apical shoot cutting treatments were lower than that of non-cutting treatment, but there was no differences between apical shoot cutting treatments due to low disease incidences. In addition, when organic materials and apical shoot cutting treatment were carried out in parallel, the combined treatments of organic materials and apical shoot cutting showed low disease incidence of cucumber downy mildew compared to untreated control. The lowest disease incidence of cucumber downy mildew was recorded in the combined treatment of 4-6type Bordeaux and apical shoot cutting. This study confirmed that apical shoot cutting can reduce the disease incidence of cucumber downy mildew and the combined treatment of apical shoot cutting and organic materials showed higher suppressive effect against cucumber downy mildew.