• Title/Summary/Keyword: 수직 이방성

Search Result 219, Processing Time 0.025 seconds

Effects of Annealing Temperature on the Properties of Solid Phase Epitaxy YIG Films (열처리온도가 고상에피택시 YIG박막의 특성에 미치는 영향)

  • Jang, Pyung-Woo
    • Journal of the Korean Magnetics Society
    • /
    • v.13 no.6
    • /
    • pp.221-225
    • /
    • 2003
  • Effects of annealing temperature on the crystalline and magnetic properties of YIG films grown by solid phase epitaxy. The eptiaxy films were made by annealing Fe-Y-O amorphous films in the air at 550-1050 $^{\circ}C$ which were sputtered on GGG (111) substrates in a conventional rf sputtering system. Crystallization temperature of Fe-Y-O amorphous films on GGG (111) substrate was between 600 and 650 $^{\circ}C$ which is much lower than that Fe-Y-O powder prepared by sol-gel method. Excellent epitaxial growth of YIG films could be conformed by the facts that the diffraction intensity of YIG (888) plane was comparable with that of GGG (888) plane and full width at half maximum of YIG (888) rocking curve was smaller than 0.14$^{\circ}$ when films were annealed at 1050 $^{\circ}C$. It could be seen that it is necessary to anneal the films at higher temperature for an excellent epitaxy because lattice parameter of YIG films were smaller and the peak of YIG (888) plane is higher and narrower with increasing annealing temperature. Films annealed at higher temperature shows M-H loop with perpendicular anisotropy which was due to 0.15% lattice mismatch between YIG and GGG.

Effect of Ear and Near-side Single Circular Pit Depth and Bulk Stress on Magnetic Flux Leakage at ferromagnetic Pipeline (강자성 배관 외.내부 면의 단일 원형 홈의 깊이와 부피응력이 누설자속에 미치는 영향)

  • Ryu, Kwon-Sang;Park, Young-Tae;Atherton, D.L.;Clapham, L.
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.23 no.3
    • /
    • pp.263-269
    • /
    • 2003
  • Magnetic flux leakage (MFL) signals were used for corrosion inspection of buried oil and gas pipeline. 3D finite element analysis was used to examine the effects of far and near-side pit depth and tensile stress on MFL signals. Anisotropci materials were used, and the effects of simulated tensile stress on MFL were investigated. The axial and radial MFL signals depended on far and near-side single pit depth and on the bulk stress, but the circumferential MFL signal did not depend on them. The axial and radial MFL signals increased with increasing pit depth and the bulk stress, but the circumferential MFL signal was scarcely changed.

Magnetic & Crystallographic Properties of Patterned Media Fabricated by Nanoimprint Lithography and Co-Pt Electroplating (나노임프린트 패터닝과 자성박막도금을 이용하여 제작한 패턴드미디어용 자기패턴의 자기적 및 결정구조특성에 관한 연구)

  • Lee, B.K.;Lee, D.H.;Lee, M.B.;Kim, H.S.;Cho, E.H.;Sohn, J.S.;Lee, C.H.;Jeong, G.H.;Suh, S.J.
    • Journal of the Korean Magnetics Society
    • /
    • v.18 no.2
    • /
    • pp.49-53
    • /
    • 2008
  • Magnetic and crystallographic properties of patterned media fabricated by nanoimprint lithography and Co-Pt electroplating were studied. Thin films of Ru(20 nm)/Ta(5 nm)/$SiO_2$(100 nm) were deposited on Si(100) wafer and then 25 nm hole pattern was fabricated by nanoimprint lithography on substrate. The electroplated Co-Pt nano-dots have the diameter of 35 nm and the height of 27 nm. Magnetic dot patterns of Co-Pt alloy were created using electroplated Co-Pt alloy and then their properties were measured by MFM, SQUID, SEM, TEM and AFM. We observed single domain with perendicular anisotropy for each dot and achieved optimum coercivity of 2900 Oe. These results mean that patterned media fabricated by nanoimprint lithography and electroplating have good properties in view of extending superparamagnetic limit while satisfying the writability requirements with the present write heads.

Displacement Analysis of an Excavation Wall using Inclinometer Instrumentation Data, Banyawol Formation, Western Daegu (경사계를 이용한 대구 서부지역 반야월층 굴착 지반의 변위 분석)

  • Ihm, Myeong-Hyeok
    • The Journal of Engineering Geology
    • /
    • v.23 no.1
    • /
    • pp.47-55
    • /
    • 2013
  • To analyze lateral displacement of excavation walls exposed during the construction of Subway Line 1 in the Daegu region, inclinometer measurement data for sites D4, D5, and Y6 are investigated from the perspective of engineering geology. The study area, in the Banyawol Formation, Hayang Group, Gyeongsang Supergroup, is in the lower part of bedrock of andesitic volcanics, calcareous shale, sandstone, hornfels, and felsite dykes that are unconformably overlain by soil. The rock mass around the D4 site is classified as RMR-V grade and the maximum lateral displacement of 101.39 mm, toward N34W, was measured at a bedding-parallel fault, at a depth of 12 m. The rock mass around the D5 site is classified as RMR-IV grade and the maximum lateral displacement of 55.17 mm, toward the south, was measured at a lithologic contact between shale and felsite, at a depth of 14 m. The rock mass around the Y6 site is classified as RMR-III grade and the maximum lateral displacement of 12.65 mm, toward S52W, was measured at an unconformity between the soil and underlying bedrocks, at a depth of 7 m. The directions of lateral displacement in the excavation walls are vector sums of the directions perpendicular to the excavation wall and horizontally parallel to the excavation wall. Lateral displacement graphs according to depth in the soil profile show curvilinear trajectories, whereas those in bedrock show straight and rapid-displacement trajectories.

Strength Design of Lightweight Composite Bicycle Frame (복합재료 라미네이트 경량화 자전거 프레임의 강도 설계)

  • Lee, Jin Ah;Hong, Hyoung Taek;Chun, Heung Jae
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.37 no.2
    • /
    • pp.265-270
    • /
    • 2013
  • Strength design for a lightweight bicycle frame made of carbon/epoxy composite laminates was studied using Tsai-Wu's failure criterion. For the design of bicycle frames, reducing the weight of the frame is of great importance. Furthermore, the frame should satisfy the required strength under specific loading cases. In accordance with the European EN 14764 standard for bicycle frames, three loading cases-pedaling, vertical, and level loadings-were investigated in this study. Because of the anisotropic characteristics of composite materials, it is important to decide the appropriate stacking sequence and the number of layers to be used in the composite bicycle frame. From finite element analysis results, the most suitable stacking sequence of the fiber orientation and the number of layers were determined. The stacking sequences of $[0]_{8n}$, $[90]_{8n}$, $[0/90]_{2ns}$, $[{\pm}45]_{2ns}$, $[0/{\pm}45/90]_{ns}$ (n = 1, 2, 3, 4) were used in the analysis. The results indicated that the $[0/{\pm}45/90]_{3s}$ lay-up model was suitable for a composite bicycle frame. Furthermore, the weakest point and layer were investigated.

Synthesis of nanosized WC powder by Chemical Vapor Condensation Process (화학기상응축법에 의한 WC 나노분말의 합성연구)

  • ;;;Oleg V. Tolochko
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2002.04b
    • /
    • pp.45-45
    • /
    • 2002
  • 나노미터 크기의 결정립을 가지는 나노분말 및 나노복합분말의 제조와 특성에 관한 연구가 매우 활발하다. 나노복합분말의 제조방법에는 기상증발후 응축법, 화학응축법, 기계적합금법 등이 있으나, 고순도 및 균일한 크기분포의 분말과 응집되지 않은 분말의 제조 조건을 가장 잘 만족하는 방법은 화학기상응축법(Chemical Vapor Condensation; CVC)이다. 본 연구그룹 에서는 CVC밤법으로 이용하여 공구/금형재료에 가장 많이 사용되는 WC/Co 합금의 결정립을 n nm크기로 극미세화고자하는 연구을 진행하고 있다. 본 연구에서는 이들 WC/Co합금제조시 가장 중요한 출발분말인 나노크기 WC 분말의 제조와 그 특성에 관하여 연구하고자 하였다. 나노미터 WC분말을 제조하기 의한 전구체는 고상의 금속유기물인Tungstenhexacarbonyl$(W(CO)_6)$ 을 사용하였다. 수평관상로을 반응기로 사용하였으며, 노내의 온도을 500-110$0^{\circ}C$로 변화시 키면서 WC 분말을 합성하였다. 반응기 및 포집기 내부를 대기분위기, 상압의 Ar분위기, 진공 분위기로 변화시켜 압력 및 분위기의 영향을 조사하였다. 포집기는 상온 및 액체질소로 냉각 한 Chiller을 사용하였다. 형성분말의 상분석은 XRD로 조사하였으며, 형태 및 결정립크기는 TEM로 분석하였다. 반응온도 600 -1 OOO$^{\circ}C$의 온도범위에서 검은색의 WC 분말이 제조되었다. XRD 분석의 결과 로 제조된 분말은 상온에서 준안정상인 Hexagonal 구조의 $\gammar-WC_{1-x}$ 상이였으며, TEM 분석결 과 상압하에서는 약 30nm이하의 WC분말이 제조되었으며, 그 형태는 둥근 4각형의 모양을 지녔다. 감압하에서 진행한 경우 결정립의 크기는 8nm이하를 가졌다.곤가스로 산화를 방지하였고, 냉매로는 질소가스를 이용하였다. 제조된 분말을 기ㅖ적 분급법을 이용하여 분급하였고, 냉매로는 질소가스를 이용하였다. 제조된 분말을 기계적 분급ㅂ법을 이용하여 분급하였고, 압출에 이용된 분말은 250$\mu\textrm{m}$이하의 크기를 사용하였다. 또한 분말제조과정 중 형성되는 표면산화층을 제거하기 위하여 36$0^{\circ}C$에서 4시간동안 수소 환원처리를 행하였다. 제조된 분말은 열간 압출을 위하여 Aㅣcan에 넣고 냉간성형체를 만들고, 진공처리를 한 후 밀봉하여 탈가스처리를 하였다. 압출다이는 압출비가 각각 28:1과 16:1인 평다이(9$0^{\circ}C$)를 사용하여 각각 내경이 9, 12cm이고, 길이가 50, 30cm인 압출재를 제조하였다. 열간압출한 후의 미세조직을 광학현미경으로 압출방향에 평행한 방향과 수직방향으로 관찰하였고, 열간 압출재 이방성을 검토하기 위하여 X선 회절분석을 실실하여 결정방위를 확인하였다. 전기 비저항 및 Seebeck 계수 측정을 위하여 각각 2$\times$2$\times$10$mm^3$ 그리고 5$\times$5$\times$10TEX>$mm^3$ 크기의 시편을 준비하였다.준비하였다.전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all low in two aspects, named "the Nonsign

  • PDF

Synthesis of Nanoscale Sn-Pb Alloy Powders by Electrical Explosion of Wire (전기선폭발법을 이용한 Sn-Pb 나노분말의 합성)

  • ;;;;A. P. Ilyin;D. V. Tichonov
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2003.04a
    • /
    • pp.35-35
    • /
    • 2003
  • )를 금속와이어에 인가하면 저항발열에 의해 와이어가 미세한 입자나 금속증기상태로 폭발하는 현상을 이용한 것으로 기상합성법에 속한다고 할 수 있다. 선폭법은 다른 제조법에 비해 공정이 간단하여 생산비용이 저렴하며, 원재료의 조성을 갖는 분말의 합성과 금속간화합물, 융점차이가 나는 재료의 합금화 등이 가능하다. 인가에너지의 크기와 폭발 시 분위기를 제어함으로써 분말의 평균크기와 분포 제어 또한 가능하다. 본 연구는 러시아의 우수한 기초기술을 바탕으로 Pb-Sn계 합금은 전기폭발법으로 극미세분말을 제조하였으며, 분말의 형상, 상 화학조성의 변화를 조사하였다. 본 실험에 사용된 Sn-Pb계(All-Union State Standard 1499-70, 0.53mm)합금와이어는 자동시스템(1-0.6Hz)에 의해 챔버안으로 공급되었다. 이 때 임계폭발 와이어 길이는 50-80nm으로 실험을 행하였다. 챔버 압력은 1.4~2.0atm으로 유지하였다. 제조된 분말의 특성은 XRD, XRPES, SEM등을 이용하여 분말의 형상과 상, 화학조성, 표면분석을 행하였으며 DSC, TGA, BET분석을 통하여 온도변화에 따른 금속분말의 열량변화, 질량변화, 비표면적을 측정하였다. 제조된 Sn-Pb계 분말은 모두 평균 입도 117nm~220nm의 구형형상이었다. 이때 합금분말의 조성은 51.17~63.21 at%Sn, 35.47~46.37 at%Pb로 나타났다. 와이어에 인가되는 비에너지(W/Wc)가 감소된에 EK라 표면층의 Pb함량이 증가함을 보였다. 이는 와이어 내부 저항의 감소로 인한 공정시간의 지연과 Sn, Pb의 확산계수 차이에 의한 것으로 사료된다. 열분석 결과, Sn~Pb계 화합물의 융점은 167~$169^{\circ}C$로 관찰되었으며, $10^{\circ}C$/min로 $920^{\circ}C$까지 승은 하였을 때 17.1~18 wt%의 질량증가를 보였다.TEX>계 나노복합분말이 얻어짐을 알 수 있었다. 이 때 X션 회절피크의 line broadening으로부터 복합분말의 Fe 명균 결정립 크기는 24nm로 초미세 결정럽의 분말합금이었다. 포화자화값은 볼밀처리에 따라 점점 증가하여 MA 30시간에는 20.3emu/g로 포화됨을 알 수 있었다. 또한 보자력 Hc는 MA초기단계에 350e로 매우 낮으나 30시간 후에는 Hc값이 2600e로 매우 큰 값을 나타내었다. 이것은 환원반응결과 초기에 생성된 Fe의 결정립이 비교적 크고 결정결함이 적으나 볼밀처리를 30시간까지 행하면 Fe 결정렵의 미세화 빛 strain 증가로 magnetic hardening이 일어나기 때문인 것으로 사료된다.길이가 50, 30cm인 압출재를 제조하였다. 열간압출한 후의 미세조직을 광학현미경으로 압출방향에 평행한 방향과 수직방향으로 관찰하였고, 열간 압출재 이방성을 검토하기 위하여 X선 회절분석을 실실하여 결정방위를 확인하였다. 전기 비저항 및 Seebeck 계수 측정을 위하여 각각 2$\times$2$\times$10$mm^3$ 그리고 5$\times$5$\times$10TEX>$mm^3$ 크기의 시편을 준비하였다.준비하였다.전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all low in two aspects, named "the Nonsignificant group". And the issues were high risk perception in general setting and lo

  • PDF

Relationship between Groundwater Level Changes and Aquifer Characteristics during Pumping at a Radial Collector Well (방사형 집수정 취수시 대수층 특성에 따른 지하수위의 변화)

  • Choi, Myoung-Rak;Lee, Ho-Jeong;Kim, Gyoo-Bum
    • The Journal of Engineering Geology
    • /
    • v.29 no.3
    • /
    • pp.279-288
    • /
    • 2019
  • The groundwater drawdown at each monitoring well near a radial collector well along Anseong Stream, Korea, was measured and compared with the calculated drawdown using the mirror well concept. The drawdown calculation is performed by treating the collector well as a large vertical well in a homogeneous isotropic aquifer. The measured drawdown at each monitoring well is slightly different from the calculated value due to anisotropy in the hydraulic conductivity and aquifer thickness. The difference between the measured and calculated values at Well OW-7 is large, reaching approximately 48 cm, because a horizontal well is not installed along this direction. Sensitivity analysis of the hydraulic conductivity and aquifer thickness indicates that the hydraulic conductivity is more sensitive to groundwater level changes. Groundwater level changes become a concern when a radial collector well with a large pumping rate capacity is installed, which highlights the need to thoroughly investigate the aquifer characteristics in the surrounding area.

Observation Test of Field Surface Reflectance Using Vertical Rotating Goniometer on Tarp Surface and Grass (수직 축 회전형 측각기 제작 및 야외 지표면 반사도 관측 시험: 타프와 잔디에서)

  • Moon, Hyun-Dong;Jo, Euni;Kim, Hyunki;Cho, Yuna;Kim, Bo-Kyeong;Ahn, Ho-Yong;Ryu, Jae-Hyun;Cho, Jaeil
    • Korean Journal of Remote Sensing
    • /
    • v.38 no.6_1
    • /
    • pp.1207-1217
    • /
    • 2022
  • Vegetation indices using the reflectance of selected wavelength, associating with the monitoring purpose such as identifying the progress of crop growth, on the vegetation canopy surface is widely used in the digital agriculture technology. However, the surface reflectance anisotropy can distort the true value of vegetation index related to the condition of surface, even though the surface property be unchanged. That causes difficulty to observe accurately crop growth on the monitoring system. In this study, a simple type goniometer was designed to measure the reflectance from the anisotropic surface according to various zeniths and azimuths of sun and viewing sensor in the field. On the tarp like as Lambertian surface, the reflectance of Blue, Green, Red, Near-Infrared band was similar to the tarps' reflectance properties. However, the reflectance was slightly overestimated in the cloudy day. The relative difference values of vegetation indices on grass were overestimated for the forward viewing and underestimated for the backward viewing. In addition, enhanced vegetation index (EVI) showed less sensitive according to the positions of sun and sensor viewing. Field observation with a goniometer will be helpful to understand the anisotropy characteristics on the vegetation surface.

A petrological study on the formation of geological heritage around Sangjogam County Park, Goseong, Gyeongsangnam-do (천연기념물 제411호 경남 고성 덕명리 공룡화석 산지 일원 병풍바위의 형성에 관한 암석학적 연구)

  • Kong, Dal-Yong;Cho, Hyeong-Seong;Kim, Jae-Hwan;Yu, Yeong-Wan;Jung, Seung-Ho;Kim, Tae-Hyeong;Kim, Jong-Sun;Jeong, Jong-Ok;Kim, Kun-Ki;Kwon, Chang-Woo;Son, Moon
    • Korean Journal of Heritage: History & Science
    • /
    • v.51 no.2
    • /
    • pp.78-91
    • /
    • 2018
  • Sangjogam, located in Goseong, Gyeongsangnam-do, was designated as Natural Monument #411, because of its diverse geological heritage, such as fossils, ripple marks, dykes, and columnar joints. In the area, Byeongpungbawi, with its beautiful columnar joints vertical to the bedding plane of the underlying sedimentary rocks and spectacular coastal view, was named after its overall shape reminiscent of a huge folding screen. The purpose of this study was to investigate the formation process of the columnar joints using the anisotropy of magnetic susceptibility (AMS) method. AMS measurements showed that the k1 and k3 values representative of directions of the long and short axes of a magnetic particle at each point strongly clustered, and the oblate magnetic foliation structure in Byeongpungbawi developed during sill-type intrusion rather than lava flow. In summary, Byeongpungbawi was produced by sill-type intrusion along the bedding plane of the underlying sedimentary layer, and the subsequent formation of columnar joints was accompanied by the cooling and contraction of intruding rhyolite magma. This study potentially provides a basic research tool in understanding the formation mechanism of columnar joints which are widely distributed in southern Korea.