• Title/Summary/Keyword: 소둔

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Crystal structures and magnetic properties of Mn-Al-M (M=Cu, Fe) alloys (Mn-Al-M(M=Cu, Fe) 합금계의 결정구조 및 자기적 성질)

  • Choe, Won-Gyu;Go, Gwan-Yeong;Yun, Seok-Gil
    • Korean Journal of Materials Research
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    • v.5 no.1
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    • pp.22-35
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    • 1995
  • In this study, crystal structures and magnetic properties of as-ast, annealed and rapidly solidified Mn-A1-M( M=Cu, Fe) alloys have been investigated. In $Mn_{0.56}Al_{0.44}$ alloys, the largest fraction of $\tau$ phase and values of magnetic properties was obtained in Mnl, i6Alo or alloy. And this alloy was used as the basic composition. In $Mn_{0.56-X}M_{X}Al_{0.44}$ alloys, when annealed, $\tau$- and $\beta$-Mn phase appeared at x< 0.08, $\tau$- and $\kappa$ phase at 0.10 $\leq x \leq$ 0.12 and $\kappa$- phase only at 0.15 $\leq x \leq$0.20 . When rapidly solidified, specimens showed similar phases as when annealed except that $\varepsilon$ phase appeared at x=0.04. In Mnu FexAlo 44 alloys, asyast specimens showed $\tau$-, $\beta$-Mn and $\gamma_2$- phase at x<0.08 and K and $\beta$-Mn phase at x>0.10. When rapidly solidified, Mn-Fe-Al specimens showed $\varepsilon$-, $\gamma_2$- and small amount of $\tau$- and $\kappa$ phase at x<0.08 and $\kappa$- phase only at 0.$\leq x \leq$0.20. All the alloys investigated were ferromagnetic. The Curie temperature of annealed specimens and rapidly solidified of Mno 5sAlu 44 alloy were -650K and -644K. Spontaneous magnetization( UII of annealed and rapidly solidified specimens were 40-45 (emu/g) and 50-52(emu/g), respectively. Remanent (M,) to saturation magnetization( Ms) ratio was -0.7. M, of rapidly solidified specimen was about 48(emu/g). Magnetic properties of $Mn_{0.56}Al_{0.44}$ alloys were found to be determined by the relative fraction of ferromagnetic r- and K- phase. When M= Cu and x=0.15, maximum as($\sigma_{0.0}$) was obtained by about 64.3 emu/g), and when M=Fe and x=0.15, 66.4( emu/g). The Curie temperature decreased as x increased.

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Research Trend of Soft Magnetic Composite Materials with High Energy Efficiency (고에너지효율 연자성 복합 분말 소재의 연구개발 동향)

  • Kim, Hwi-Jun
    • Journal of the Korean Magnetics Society
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    • v.21 no.2
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    • pp.77-82
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    • 2011
  • The use of soft magnetic materials have been increasing in the various industrial fields according to the increasing demand for high performance, automatic, miniaturing equipments in the recent our life. In this study, we investigated the effect of factors on the core loss and magnetic properties of electrical steel and soft magnetic composites. Furthermore, we reviewed the major efforts to reduce the core loss and improve the soft magnetic properties in the two main soft magnetic materials. Domain purification which results from reduced density of defects in cleaner electrical steels is combined with large grains to reduce hysteresis loss. The reduced thickness and the high electrical conductivity reduce the eddy current component of loss. Furthermore, the coating applied to the surface of electrical steel and texture control lead to improve high permeability and low core loss. There is an increasing interest in soft magnetic composite materials because of the demand for miniaturization of cores for power electronic applications. The SMC materials have a broad range of potential applications due to the possibility of true 3-D electromagnetic design and higher frequency operation. Grain size, sintering temperature, and the degree of porosity need to be carefully controlled in order to optimize structure-sensitive properties such as maximum permeability and low coercive force. The insulating coating on the powder particles in SMCs eliminates particle-to-particle eddy current paths hence minimizing eddy current losses, but it reduces the permeability and to a small extent the saturation magnetization. The combination of new chemical composition with optimum powder manufacturing processes will be able to result in improving the magnetic properties in soft magnetic composite materials, too.

은상대(殷商代)의 질병(疾病)과 치료(治療)

  • Yang, Dong-Suk
    • Journal of Korean Medical classics
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    • v.19 no.4
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    • pp.226-240
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    • 2006
  • 1899년재상대후기적왕궁유지안양소둔발현료갑골문(年在商代後期的王宮유址安陽小屯發現了甲骨文). 갑골문시목전능근거적최가고적고대자료(甲骨文是目前能根據的最可고的古代資料). 십오만다편적갑골문중유흔다유관질병적내용(十五萬多片的甲骨文中有흔多有關疾病的內容). 근거갑골문가고찰질병적원인(根據甲骨文可考察疾病的原因), 질병적치료(疾病的治療), 질병적종류(疾病的種類). 갑골문적질병복사중가이관찰도수(甲骨文的疾病卜辭中可以觀察到首),목(目),이(耳),설(舌),치(齒),골등삼십다종질병(骨等三十多種疾病). 근현대인적질병종류상차불다(근現代人的疾病種類相差不多). 질병적치료자시의관(疾病的治療者是醫官), 궁명규소질신(宮名叫小疾臣). 재래무야시실제상적의관료(再來巫也是實際上的醫官了), 인병료무통과무술래치병(人病了巫通過巫術來治病). 상대시중국오천년역사상최미신적시대(商代是中國五千年歷史上最迷信的時代), 일체사정도향상제혹시조선점복(一切事情都向上帝或是祖先占卜), 안점복적결과래행동(按占卜的結果來行動). 생병적시후야시일양(生病的時候也是一樣), 단시만만지도(但是慢慢知道), 점복불시치병적호판법(占卜不是治病的好辦法), 소이도상대후기질병복사점점소료(所以到商代後期疾病卜辭漸漸小了). 재갑골문질병복사중적병인유상왕(在甲骨文疾病卜辭中的病人有商王), 왕비(王妃), 왕자(往者), 왕신(王臣), 기중대다수시유관상왕적질병적정황(基中大多數是有關商王的疾病的精況). 치료방법수선유약래치병(治療方法首先有藥來治病); 제이침래치료(第二鍼來治療); 제삼애구래치료(第三艾灸來治療);제사안마래치료(第四按摩來治療), 제오아과중유발치치료(第五牙科中有拔齒治療); 제육유접골적치료(第六有接骨的治療). 유갑골문중적질병복사가간출상대적질병종류(由甲骨文中的疾病卜사可看出商代的疾病種類), 치료방법(治療方法), 가이설상대적의학수평상당고(可以設商代的醫學水平相唐高), 저양적능력능구공고전국시대적의술(這樣的能力能구鞏固戰國時代的醫術), 작료한대능사출(作了漢代能寫出)"신농본초경(神農本草經)", "황제내경(黃帝內徑)"등명저적기초(燈明抵敵基礎), 동시장중국적중의학적시원추도상대적학절적근거(同時將中國的中醫學的始源推到商代的학切的根据).

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A Study on Reductive Furnace for Copper Annealing Using Catalytic Combustion (촉매연소를 이용한 동 열처리용 환원로에 관한 연구)

  • Jeong, Nam-Jo;Kang, Sung-Kyu;Song, Kwang-Sup;Cho, Sung-June;Yu, Sang-Phil;Ryou, In-Su
    • 한국연소학회:학술대회논문집
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    • 2001.11a
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    • pp.83-89
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    • 2001
  • Most technologies of reduction process used in the heat treatment of existent metal products are related to metals applied to bolts and parts of automobiles, and nonmetal such as copper. Heating conditions and reduction gases produced in above processes depend on types of products to be treated thermally but heating systems employ electricity commonly and the reduction gases are separated into additional production equipment and a gas dryer and inefficiently provided into the system. Electrical heating system has the advantage of convenient temperature-control but is not economical because of disadvantages of high electricity-running cost and extra installation cost of a transformer. Accordingly, development of the system which has economical heating mode in which provision of reduction gas and heating conditions are unified is necessary for improvement of economy and efficiency in current reduction processes. This study aimed to develop a new advanced heat treatment furnace using catalytic combustion. thereby minimizing the cost during heating, supplying heat and reductive gas at the same time and controlling operating condition freely by changing electrical heating system to heating system by the gas combustion and regeneration of wasted heat.

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Effects of Strain Annealing Grain Size on the Magnetic Properties of Extra-Low Carbon Steel (극저탄소강판의 자성에 미치는 변형소둔 결정립도의 영향)

  • An, S.K.;Jeong, W.S.;Park, J.U.
    • Journal of the Korean Society for Heat Treatment
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    • v.19 no.4
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    • pp.208-218
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    • 2006
  • The effects of the grain size on the magnetic properties in extra-low carbon steel after strain annealing were investigated. Two kinds of sample were prepared. One is the annealed sheet, which was annealed at $670^{\circ}C$ and $850^{\circ}C$ for various time periods after cold rolling. The other is the strain annealed sheet, which was temper rolled by 0.4% and subsequently strain annealed at the temperature ranging between $670^{\circ}C$ and $850^{\circ}C$ for various time periods. The grains after strain annealing became more coarse than those after primary annealing. The grains were coarsened due to the strain induced grain boundary migration (SIGM). It was found that the permeability tended to be increased and coercivity tended to be decreased with the increase of grain size. The optimum magnetic properties was achieved after strain annealing at $850^{\circ}C$ for 30 minites. Under this condition, the coercivity was measured to be 0.6 and the permeability was measured up to be 13000.

Development of Low Annealing treatment omission steel by new rolling process (새로운 압연Process 구축을 통한 연화소둔 열처리생략강개발)

  • Kim B. H.;Choi K. S.;Heo C. Y.;Kim K. W.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.08a
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    • pp.27-36
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    • 2004
  • Contemporary objectives for steel rod rolling processing are increasingly complex and often contrasting i.e. obtaining a desired product with optimum combination of properties such as strength, toughness and formability at lower cost. Low-alloy steel rods have been produced with several heat treatments for drawing and forging processes at room temperature. In order to reduce these heat treatments much of the researches concerning of high temperature mechanical behavior of steel rods have been conducted at wire rod mill of POSCO. In this present work, optimizations of rolling temperature and cooling rate for JS-SCM435 are performed to eliminate softening heat treatment(Low Temperature Annealing) for drawing process. The results from the optimization changed the microstructure of rods after rod rolling from Bainite with high tensile strength of 1000Mpa to Pearlite and Ferrite with appropriate strength of 750Mpa that is equivalent tensile strength after softening heat treatment.

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Fabrication of bi-axially textured nickel tape (양 축 정렬된 nickel tape의 제조)

  • Kang, Seok-Min;Lee, Hee-Gyoun;Hong, Gye-Won;Kim, Hyoung-Seop
    • 한국초전도학회:학술대회논문집
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    • v.10
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    • pp.304-307
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    • 2000
  • 고순도 니켈분말을 사용하여 성형, 소결, 압연 및 중간소둔 공정을 통해 cube-texture를 갖는 니켈테이프를 제조하였다. 제조된 니켈테이프의 texture는 성형압력, 성형체의 소결 온도 및 시간, 냉간 압하율 및 중간열처리에 따라 달라지는 것을 관찰하였다. 200kgf/cm$^2$ 의 성형압력으로 제조한 성형체를 1000$^{\circ}$C의 온도에서 8시간열처리한 소결체를 100${\sim}$50 $_{\mu}$m로 압연된 tape을1000$^{\circ}$C 1시간 열처리 할 때 가장 우수한 texture를 가지는 tape을 제조할 수 있었다. 긴 니켈테이프를 제조하기 위해 50cm 길이의 mold에서 성형한 green-pellet을 불활성 분위기(Ar:96%-H$_2$:4%)에서 1000$^{\circ}$C, 8시간동안 열처리하여 소결하였다 400mm길이에 17${\sim}$20mm 두께의 소결체를 압연하여 100$_{\mu}$m두께의 긴 니켈 테이프를 제조하였다. 제조한 테이프의 texture는 소형으로 제조한 테이프에 비해 떨어졌으며 이는 압연 시 시료에 너무 큰 인장력을 가했기 때문으로 사료된다.

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The Improvement in Properties of $SnO_2-Si $ Heterojunction Solar Cells ($SnO_2-Si $ 이중접합 태양전지의 특성개선)

  • 이#한;송정섭
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.17 no.6
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    • pp.65-71
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    • 1980
  • The Sn O2-Si Heterojunction sola cells are Prepared by vacuum deposition of SnO2 on N- and P-type Si - wafers arts the effects of annealing on the Solar cell characteiistics are presented. The existence of optimumannealins temperature for maximum open-circuit voltage and short - circuit current of the solar cell is observed. The optimum tomperature, when low resistivity (7- 2.3 [$\Omega$.cm]) P-and N-type Si -wafers are used, is 500 [$^{\circ}C$] End 400 [$^{\circ}C$] when high resistivity[41-58 [$\Omega$.cm]) P-type Si-wafers are used.

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A Study of Annealing Heat-treatment for Ti(Grade 2) by Electrochemical Methods (전기화학적 방법을 이용한 Ti(Grade 2)재의 최적 어닐링 열처리에 대한 연구)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.90-98
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    • 2002
  • In this paper, the annealing heat treatments for the best corrosion resistant of Ti(Grade 2) were studied in a 3.5% NaCl solution by electrochemical methods. The annealing heat treatments were accomplished at 650, 700 and $750^{\circ}C$ with different time of 30min., 1hour and 2 hours in a vacuum condition. The obtained results are: 1) in the case of solution heat treated $930^{\circ}C$ for 2 hours in a vacuum and air, the corrosion potentials were -348.7 and -567. 1mV, and current densities 2.32 and $22.62\mu\textrm{A}$, respectively, 2) as increase both annealing heat treatment temperature 650, 700, $750^{\circ}C$ and time 30min., 1 hour, 2 hours, the corrosion potential were decreased, whereas corrosion current density increased, 3) in the case of cyclic polarization, the measured charges were increased as increasing solution heat treatment temperature and time, 4) on the bases of corrosion potential, current density and charge, the best annealing temperature and time were measured as $700^{\circ}C$ and 30min. for Ti(Grade 2) material.

The Present Status of Recycling Technology of Aluminum Can (알루미늄캔의 재활용(再活用) 기술현황(技術現況))

  • Lim, Cha-Yong;Kang, Suk-Bong
    • Resources Recycling
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    • v.9 no.2
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    • pp.3-10
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    • 2000
  • Used aluminum beverage can(UBC) is an important secondary resource. Domestic recycling rate of UBC should be increased from the standpoint of resource savings and environmental protection. Aluminum can to can recycling is divided into two steps. The first step was composed of the processes such as collection of used beverage cans, shredding, magnetic separation, de-lacquring, melting and casting. The second is remelting and casting, heat treatment, hot and cold rolling, annealing, and can making. With brief discussion about this recycling technology, this article covers aluminum can consumption, the present state of aluminum can recycling in Korea, Japan, USA, and Europe.

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