• Korean Journal of Food Science and Technology
• /
• v.37 no.3
• /
• pp.352-359
• /
• 2005

Uncertainty involved during determination of vitamin C content in infant formula was quantified by indophenol titration method. Uncertainty sources in measurand, such as purity, weight, final volume of standard, volume of standard solution used for titration, sample weight, final volume of sample, extraction solution used for titration, titration of extraction solution and standard solution by indophenol solution were identified and used as parameters for combined standard uncertainty based on Guide to the expression of uncertainty in measurement (GUM) and Draft EURACHEM/CITAC Guide. Uncertainty parameters of each source in measurand were identified as resolution, reproducibility and stability of chemical balance, standard material purity, repeatability, reproducibility, end point of titration, 1 mL pipet, 5 mL autopipet, and 100 mL mass flask. Each uncertainty component was evaluated by types A and B and included to calculate combined uncertainty. Analytical test result for traceability under laboratorial conditions using Certified Reference Material (CRM) test was certified as $108.4{\pm}1.7mg/100g$, which was within CRM certification range of $114.6{\pm}6.6mg/100g$. Uncertainty test result of vitamin C content of 5 g sampling was $56.7{\pm}2.44mg/100g$. Uncertainty could be reduced by identification of uncertainty sources and components related with vitamin C determination by indophenol titration method and by decreasing uncertainty sources and components.

• Korean Journal of Plant Resources
• /
• v.20 no.5
• /
• pp.461-465
• /
• 2007

In this study, changes in the overall antioxidant properties and chemical constituents including total phenolics and vitamin C of R. occidentalis fruit during ripening are studied. The antioxidant activity was measured by the free-radical scavenging activity(DPPH method) and reducing power(potassium ferricyanide method). Although, the weight and diameter of R. occidentalis fruit were increased with the progress of ripening, antioxidant activity and total phenolics were decrease during ripening. The highest free-radical scavenging activity(at $125{\mu}g/m{\ell}$) and reducing power(at $100{\mu}g/m{\ell}$) in fruit were 61.67% and 0.71, respectively. Total phenolic content and vitamin C content in fruit of 5 days after fruit set were $220.73{\mu}g/g$ and $540.45{\mu}g/g$, respectively. A linear correlation(r=0.9761) was shown between free-radical scavenging activity and total phenolic content.

• Applied Biological Chemistry
• /
• v.43 no.1
• /
• pp.39-45
• /
• 2000

The stability of vitamin A, $B_1,\;B_2,\;B_6$, C in aqueous multivitamin solutions was carried out by means of estimation of reaction velocity and the results are described in this paper. The stability of vitamin A, $B_1$ and C due to thermal degradation method in aqueous multivitamin solutions was evaluated at 40, 50, 60 and $70^{\circ}C$ up to 40 days. The shelf-lives of vitamin A, B₁ and C in this preparation, calculated using the Arrhenius equation, were 1493, 449 and 639 days at $25^{\circ}C$ respectively. Examination was made on the effect of initial concentration of vitamin $B_2$$(C_0)$ on light fading of vitamin $B_2$ in aqueous multivitamin solutions and it was found that the fading progressed according to the following formula : $-{\frac {dc}{dt}}=K_c\;{\frac C{C_0}}$ where Kc is apparent light-fading rate constant relate to $C_0$. Photodecomposition of vitamin $B_6$ in aqueous multivitamin solutions was apparently first order kinetics and was stable in polyethylene>brown color>glass container to sunlight. Photodecomposition of vitamin $B_6$ in four seasons also investigated.

• Journal of Bio-Environment Control
• /
• v.6 no.4
• /
• pp.264-269
• /
• 1997

This study was conducted to evaluate appropriate selenate ion concentration for the production of high functional vegetables. Sodium selenate was treated 0, 2, 4, 6 and 8mg/$\ell$ using herb nutrient solution developed by European R & D Vegetable Center in Belgium. Low level of Na2se04 concentration increased the growth of wormwood, but high selenate concentration decreased the growth. Total chlorophyll content was increased by sodium selenate. The higher selenate ion concentration in the nutrient solution, the more total chlorophyll content was. The vitamin C content in wormwood was high at 2 and 4mg/$\ell$ treatment, showing good growth, at higher concentration, however, the vitamin C content decreased. At 4mg/$\ell$ selenate ion concentration, essential oil content of wormwood was best. But higher selenate ion concentration decreased essential oil content. The uptake of Se by the plant increased with the increase of selenate ion concentration.

• Food Science and Preservation
• /
• v.14 no.6
• /
• pp.591-597
• /
• 2007

The quality characteristics of semi-dry red pepper (SDRP) (Capsicum annuum L.) were compared with raw and dry red pepper (DRP). Raw red pepper was divided into pieces and the semi-drying treatment involved air-drying at $65^{\circ}C$. The study focused on describing the characteristics of semi-dry red pepper in comparison with dry red pepper. Factors considered were reduced drying period, ASTA color, capsanthin, capsaicinoids, free sugars and vitamin C content. ASTA color, capsanthin, capsaicinoids, free sugars and vitamin C content of SDRP were higher in SDRP than in DRP for 15 g or less water per 100 g. Red pepper powders made using the semi-drying method showed the highest amount of glucose and vitamin C. Capsanthin content in SDRP (151.6155.9 mg/100 g) was significantly higher than for DRP (133.4 mg/100 g). The capsaicinoid content of SDRP was about 13-25% higher than in DRP. The ASTA values (148.7159.3) for SDRP were much higher than for DRP (139.5). The vitamin C and free sugar content of SDRP was 40-76% and 20-40% higher, respectively, than for DRP. and $20{\sim}40%$, respectively, by SDRP compared to DRP.

• Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
• /
• 2003.10a
• /
• pp.142.2-142
• /
• 2003

손바닥 선인장(Opuntia ficus indica)은 중심자목 선인장과에 속하는 다년생 초본으로 열매는 서양배 모양이며 많은 종자가 들어있고 다량의 점질물을 함유하고 있다. 손바닥 선인장 열매(prickly pear pulp)는 14.5%의 고형분 함량을 가지고 있으며, 0.21%의 단백질, 0.12%의 지방, 0.44%의 회분, 0.19%의 pectin 이외에 미량의 비타민 A와 C 그리고 여러 종류의 무기질을 포함하고 있다. 주요 당류로서 sucrose(68.7%), fructose(18.0%) 및 glucose(12.8%)를 함유하고 있으며, 점질다당류의 구성분인 mannose 가 0.5% 포함되어 있다. 손바닥 선인장 열매는 높은 혈중 콜레스테롤, 염증 및 비만 등의 치료에 유용한 것으로 알려져 있다. 본 연구에서는 손바닥 선인장 열매 추출물의 기능적 특성을 반응표면분석에 의해 모니터링 하였다. 그 결과 환원당 함량은 최대값이 33.39 mg%로 추출온도 69.87$^{\circ}C$, 추출시간 68.84 min및 시료에 대한 용매비 16.29 ml/g일 때였다. 총 플라보노이드 함량은 추출온도 89.7$0^{\circ}C$, 추출시간 170 min 및 시료에 대한 용매비 17.07 ml/g일 때 2,03 mg%로 최대값을 나타내었다. 펙틴 함량은 추출온도 96.54$^{\circ}C$, 추출시간 135.28 min및 시료에 대한 용매비 20.02 nWg일 때 최대값 82.04 mg%를 나타내었으며, 비타민 C 함량은 추출온도 61.8$0^{\circ}C$, 추출시간 101.98 min 및 시료에 대한 용매비 12.14 ml/g일 때 최대값이 3.76 mg%였다.

• Journal of the Korean Society of Food Culture
• /
• v.19 no.2
• /
• pp.209-216
• /
• 2004

To investigate physico-chemical changes of mashed red repper and red pepper powder during frozen storage, we analyzed the quality of samples after mashing, mashing and blanching, mashing and addition of vitamin C, mashing and addition of NaCl. The most important quality factor of red pepper is red color. $\alpha$ value of red pepper powder of Pochungchun was 31.51. These results showed that those processing methods were effective to preserve red color. Capsanthin contents of mashed red pepper treated with vitamin C were decreased 1.8% after 180 days of frozen storage. This decrease was the least, showing that addition of vitamin C helped retaining capsanthin contents. Capsaicin and dihydrocapsaicin contents in Pochungchun powder ore decreased 11.9 and 18.3% during frozen storage respectively. These results showed that capsaicin was more stable than dihycrocapsaicin during frozen storage. Generally capsaicin and dihydrocapsaicin in the Pochungchun red pepper frozen-stored after mashing were less decreased than red pepper powder, and addition of vitamin C to the mashed red pepper was the most effective to retain capsicin and dihydrocapsaicin than others. The content of vitamin C in the red pepper frozen-stored after masking and blanching was 12.0 mg/100g, compared with 44.0 mg/100g in the sample stored after only mashing. This suggested that blanching process destroyed vitamin C in the mashed red pepper. Addition of salt in the mashed red pepper showed the same inclination. But, addition of vitamin C to the mashed red pepper was decreased 32.9% compared with 69.0% in the mashed red repper during frozen storage. Theser results indicated that addition of vitamin C could retain vitamin C in the mashed red lopper.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.25 no.2
• /
• pp.199-204
• /
• 1996

부산시 사하구 관내 통합보건지역 주민 100여명을 대상으로 1995년 9월 1일부터 9월 30일까지 실시한 영양실태 조사의 결과를 요약하면 다음과 같다. 1) 헤모글로빈 함량은 평균 13.19g/100ml이었으나, 빈혈이 의심되는 조사대상자는 21%이었다. 혈청 알부민 함량은 4.08g/100ml, 총 단백질 함량은 7.81g/100ml로 나타났다. 2) 열량 섭취량은 권장량의 63.1~82.0%를 나타내었으며, 탄수화물, 지방, 단백질의 구성비율은 63.2~72.4% : 13.2~19.5% : 14.4~18.5%이었다. 단백질은 권장량의 79.4%~98.5%의 섭취량을 보였으나, 칼슘, 철, 비타민 $B_{1}$, 비타민 $B_{2}$, niacin, 비타민 C 등은 권장량보다 낮은 섭취를 보이는 주민이 많은 것으로 나타났다. 3) 조사 대상자의 18.5%가 점심을 결식하는 것으로 나타났고, 한끼 평균 4.0~9.3가지, 하루 평균 10.9~14.9가지의 식품을 섭취하고 있었다. 4) 해당 영양소의 결핍이 우려되는 수준인 영양권장량의 75% 미만을 섭취하고 있는 주민의 비율이 단백질이 34%, 칼슘 71%, 철분 47%, 비타민 $B_{1}$ 30%, 비타민 $B_{2}$ 30%, niacin 30%로 매우 높음을 알 수 있었다.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.33 no.9
• /
• pp.1573-1579
• /
• 2004

This study was conducted to develop intermediate material for new processed food from sweet pumpkin. Osmotic dehydration was carried out as pretreatment before drying. After the sweet pumpkins were pretreated under optimized osmotic dehydration conditions, they were dried by three drying methods (hot air drying, vacuum drying and cold air drying). The moisture contents of dried sweet pumpkin products by osmosis treatment (sucrose) and hot air drying, vacuum drying, and cold air drying were 14.48, 14.09 and 13.87%, respectively. Cold air drying preserved more vitamin C content and showed lower color difference than hot air drying and vacuum drying. As a result of microscopic analysis, cold air dried sweet pumpkin was observed regular tissue, while hot air and vacuum dried sweet pumpkins were observed a cell collapse following the loss of water.

• Korean Journal of Food Science and Technology
• /
• v.35 no.3
• /
• pp.493-498
• /
• 2003

Changes in amino acids content and antioxidative activity in the leaves of buchu (Allium tuberosum R.) at different harvesting times were investigated. Contents of protein, lipids and ash were the highest at the first harvest time, but decreased thereafter, whereas water content showed the reverse pattern. Amino acid contents were the highest at 2nd harvest time, major compositions being aspartic acid, alanine, and glutamic acid, which decreased thereafter. Antioxidative activities according to harvesting times also revealed the same pattern showing by the major nutrients. Correlation coefficients between antioxidative detecting methods in TEAC vs FRAP assay, FRAP vs DPPH assay, and TEAC vs DPPH showed 0.996, 0.992, and 0.987, respectively (p<0.001). The earliest-harvested buchu had the highest content of carotenoids, vitamin C, and total phenol, whereas the lowest of chlorophyll. Antioxidative effects of buchu, with vitamin C and total phenol contents have high coefficient correlations of 0.991 and 0.989, respectively.