• 한국주조공학회지
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• 제10권6호
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• pp.528-537
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• 1990

7XXX aluminum alloy powders produced by the self-manufactured rotating disc atomizer were investigated to determine the influence of the atomization parameters on the particle size distributions in air atmosphere. The particle size distributions are almost always bimodal with the dominant mode on the large particle size. Average powder size of 7XXX aluminum alloy is $74/{\mu}m~125/{\mu}m$ when melt is poured with the rate of 9g /sec at 730$^{\circ}C$ on a rotating disc of 30㎜ diameter at 6300rad/sec. The mass of finer particle increased when disc diameter, angular velocity, pouring temperature increased and pouring rate decreased. The powder shapes of bimodal change from acicular to tear-drop and from tear-drop to ligament with increasing powder size. Powder shape was determined by the atomization mechanism and oxidation in liquid state. Microstructure of powders appeared to be cell and cellular dendrite. The SDAS of Al-7.9wt%Zn-2.4wt%Mg-1.5wt%Cu-0.9wt%Ni Powders is $0.8{\mu}m~1.0{\mu}m$ for the powders of $size＋44{\mu}m~53{\mu}m$ and $1.6{\mu}m∼1.8{\mu}m$ for the powders of $size＋105{\mu}m~125{\mu}m$, repectively.

• 한국재료학회지
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• 제26권9호
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• pp.472-477
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• 2016

Microstructure evolutions of thermosetting resin coating layers fabricated by electrostatic spray deposition (ESD) at various processing conditions were investigated. Two different typical polymer systems, a thermosetting phenol-formaldehyde resin and a thermoplastic polyvinylpyrrolidone (PVP), were employed for a comparative study. Precursor solutions of the phenol-formaldehyde resin and of the PVP were electro-sprayed on heated silicon substrates. Fundamental differences in the thermomechanical properties of the polymers resulted in distinct ways of microstructure evolution of the electro-sprayed polymer films. For the thermosetting polymer, phenol-formaldehyde resin, vertically aligned micro-rod structures developed when it was deposited by ESD under controlled processing conditions. Through extensive microstructure and thermal analyses, it was found that the vertically aligned micro-rod structures of phenol-formaldehyde resin were formed as a result of the rheological behavior of the thermosetting phenol-formaldehyde resin and the preferential landing phenomenon of the ESD method.

• 한국전기전자재료학회논문지
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• 제14권7호
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• pp.539-545
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• 2001

Undoped and Co$^{2+}$ $\alpha$-Ga$_2$S$_3$ thin films were grown by spray pyrolysis method. It has been found that these thin films have a monoclinic structure and direct optical energy gap and indirect were located to 3.477eV and 3.123 eV at 10K respectively. In the photoluminescence due to a D0A(donor-acceptor) pair recombination were observed at 502 nm and 671 nm for the $\alpha$-Ga$_2$S$_3$ thin film, where is excited by the 325 nm-line of He-Cd laser. These peaks are identified to be corresponding to the electron transition between the energy levels of Co$^{2+}$ ion sited a the T$_{d}$ symmetry point in the $\alpha$-Ga$_2$S$_3$;Co$^{2+}$ thin film. film.

• 대한기계학회논문집
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• 제18권9호
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• pp.2404-2412
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• 1994

A mathematical model has been developed for predicting kinematic, thermal, and solidification histories of atomized droplets during flight. Liquid droplet convective cooling, recalescence, equilibrium-state solidification, and solid-phase cooling were taken into account in the analysis of the solidification process. The spherical shell model was adopted where the heterogeneous nucleation is initiated from the whole surface of a droplet. The growth rate of the solid-liquid interface was determined from the theory of crystal growth kinetics with undercooling caused by the rapid solidification. The solid fraction after recalescence was obtained by using the integral method. The thermal responses of atomized droplets to gas velocity, particle size variation, and degree of undercooling were investigated through the parametric studies. It is possible to evaluate the solid fraction of the droplet according to flight distance and time in terms of a dimensionless parameter derived from the overall energy balance of the system. It is also found that the solid fraction at the end of recalescence is not dependent on the droplet size and nozzle exit velocity but on the degree of subcooling.

• 대한기계학회논문집B
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• 제23권10호
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• pp.1310-1319
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• 1999

High-pressure swirl injectors have usually been employed in Gasoline direct injection engines due to their spray characteristics and the feasibility of their control. Thus the microscopic characteristics of high-pressure swirl spray were investigated by PDA. The correlation between axial and radial velocities and the correlation between droplet size and axial velocity were examined with different axial and radial positions. Two dimensional droplet velocity and its number distribution with size-classified droplets were illustrated. The mean droplet velocity and its SMD were also analyzed at the center of spray, the position having maximum mean axial velocity, and the spray periphery using time dividing method. Finally, the structure of high-pressure swirl spray was presented with the size distribution and velocity profile of droplets.

• 태양에너지
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• 제18권2호
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• pp.137-144
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• 1998

분무열분해법으로 $SnO_2$ 박막을 증착하여 기판표면의 온도에 따른 방향성과 결함을 조사하였다. 기판의 온도가 $300^{\circ}C$일 때부터 결정성 박막이 증착되었다. 기판의 온도가 $400^{\circ}C$까지 증가함에 따라 (200)면이 우선적으로 성장하였으며 결정립의 크기도 증가하였다. Sb를 첨가하지 않은 박막은 Sn과 O로 구성되어 있으며 산소공위를 포함한다. Sb를 첨가한 박막은 산소공위 외에 Sn 위치와 O 위치에 각각 치환된 Sb와 Cl을 가진다.

• 대한기계학회논문집B
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• 제26권7호
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• pp.1047-1054
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• 2002

To improve the fuel consumption and exhaust emission for gasoline engines, GDI(Gasoline Direct Injection) system was spotlighted to solve above requirements. Thus, many researchers have been studied to investigate the spray characteristics and the mixture formation of GDI injector. In this study, we tried to study the spray characteristics of a gasoline direct injector by using entropy analysis and PlV methods. The entropy analysis is based on the concept of statistical entropy, and it identifies the degree of homogeneity in the fuel concentration. The PlV method was adopted to determine the fluid dynamics information at the spray. From the applied results on a direct injection gasoline spray, we could find that the direct diffusion phenomena was a dominant factor in the formation of a homogeneous mixture at downstream of GDI spray especially under vaporizing ambient conditions, and mixing phenomena was also progressed by momentum exchange with induced air. In addition, the correlation between entropy and vorticity strength enabled to find their relation.

• 한국분말재료학회지
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• 제1권1호
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• pp.42-51
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• 1994

6061Al-SiCP metal matrix composite materials(MMCs) were fabricated by injecting SiCP particles directly into the atomized spray. The main attraction of this technique is the rapid fabrication of semi-finished, composite products in a combined atomization, particulate injection(10 $\mu\textrm{m}$, 40 $\mu\textrm{m}$, SiCP) and deposition operation. Conclusions obtained are as follows; The microstructure of the unreinforced spray formed 6061Al alloy consisted of relatively fine(50 $\mu\textrm{m}$) equiaxed grains. By comparision, the microstructure of the I/M materials was segregated and consisted of relatively coarse(150 $\mu\textrm{m}$) grains. The probability of clustering of SiCP particles in co-sprayed metal matrix composites increased it ceramic particle size(SiCP) was reduced and the volume fraction was held constant. Analysis of overspray powders collected from the spray atomization and deposition experiments indicated that morphology of powders were nearly spherical and degree of powders sphercity was deviated due to composite with SiCp particles. Interfacial bonding between matrix and ceramics was improved by heat treatment and addition of alloying elements(Mg). Maximum hardness values [Hv: 165 kg/mm2 for Al-10 $\mu\textrm{m}$ SiCp Hv--159 kg/mm2 for Al-40 $\mu\textrm{m}$SiCp] were obtained through the solution heat treatment at $530^{\circ}C$ for 2 hrs and aging at $178^{\circ}C$, and there by the resistance were improved.

• 동력기계공학회지
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• 제14권3호
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• pp.5-12
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• 2010

The purpose of this study is to analyze heterogeneous distribution of branch-like structure at downstream region of inner spray. The previous many studies about diesel spray structure have yet stayed in the analysis of 2-D structure, and there are very few of informations which are concerned with 3-D analysis of the structure. The heterogeneous distribution of droplets in inner spray affects the mixture formation of diesel spray, and also the combustion characteristics of the diesel engines. Therefore, in order to investigate 3-D structure of evaporative spray the laser beam of 2-D plane was used in this study. Liquid fuel was injected from a single-hole nozzle (l/d=5) into a constant-volume vessel under high pressure and temperature in order to visualize the spray phenomena. The incident laser beam was offset on the central axis. From the images analysis taken by offset of laser beam, we examine formation mechanism of heterogeneous distribution by vortex flow at the downstream of the diesel spray. As the experimental results, the branch-like structure formed heterogeneous distribution of the droplets consists of high concentration of vapor phase in the periphery of droplets and spray tip of branch-like structure. Also the 3-D spatial structure of the evaporative diesel spray can be verified by images obtained from 2-D measurement methods.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2015년도 추계학술대회 논문집
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• pp.352-352
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• 2015

PVD(Physical Vapor Deposition)법은 제작 조건에 따라 그 특성이 변하므로 원하는 재료 특성을 얻기 위해서는 모폴로지, 결정배향성 등에 따른 코팅막의 특성을 이해하는 것이 중요하다. 따라서 본 연구에서는 친환경 프로세스 방법인 PVD법 중 하나인 스퍼터링(Sputtering)을 이용하여 Al-Mg 막을 제작하였고, 제작된 막들에 대한 형성 메커니즘과 내식성 상관관계 해명을 위해 막의 조성분포, 표면 및 단면의 모폴로지 관찰 및 결정구조 분석을 진행하였다. 또한 염수분무 및 전기화학적 양극분극 시험을 통해 Al-Mg 막의 표면 및 단면 모폴로지가 내식특성에 미치는 영향을 고찰하였다. Al-Mg 막의 모폴로지 관찰결과 Mg 함량 및 열처리 조건에 의해 단면의 주상정 형태는 입상정 또는 무형태로 변화하였고, 표면의 모폴로지는 미세하고 치밀해지는 것으로 나타났다. 결과적으로 무형태의 단면 모폴로지와 미세하고 치밀한 표면 모폴로지를 갖는 막이 우수한 내식성을 나타내었다.