• Journal of the Korean Ceramic Society
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• v.29 no.5
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• pp.391-395
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• 1992

In order to improve the compactness and uniformity in ceramic green body, we have developed dynamic CIP(Cold Isostatic Pressing) as a new forming method in which the CIP and the vibratory pressing were combined. In dynamic CIP, bulk density on alumina compacts was linearly increased with higher │Pmax-Pbias│and maximum pressure of dynamic-CIP was decreased over one-third of that of conventional CIP to obtain the same bulk density.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1993.04b
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• pp.49-52
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• 1993

금속의 가공공정에 있어 중요한 인자중의 하나인 재료의 연성은 환경뿐만 아니라 주변압력에 따라 변화한다는 사실이 20세기에 들어 여러 연구자들에 의해 밝혀졌고 1950년대 Birdgman에 의해 최초로 실험적인 방법으로 증면되었다. 재료의 이와같은 현상을 압력유도연성이라 하는데 이는 주변압력이 재료 내부에서의 공동발생 및 그 성장에 관계하기 때문인 것으로 알려졌다. 공동의 합체 및 성장은 연성파괴의 전체조건이 되므로 이를 억제하면 성형성 및 연성이 증가됨을 알 수 있다. 금속의 압력 유도 연성을 이용한 가공방법을 가압금속형형이라 한다. 최근에 가압금속형의 범주는 크게늘고 있 는데 특히, 성형,블랭킹, 분말야금법 등에 널리 이용되고 있다. 정수압의 크기에 다른전단면의 상태 변화 즉, 소성 변형능에 관한 연구는 Fine-Blanking가공이론에 적용, 해석되고 있다.

• Proceedings of the KAIS Fall Conference
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• 2010.05b
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• pp.1137-1140
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• 2010

PP에 용융온도 조절을 위한 첨가제로 ZnO와 ADCA를 첨가하여 발포제의 온도를 약 $165^{\circ}C$로 조절 하였다. 이러한 혼합 분말은 $178{\sim}208^{\circ}C$ 온도범위의 금형에서 약 3분 동안 가압성형 되었다. $198^{\circ}C$, 발포제 1.0wt%에서 비교적 우수한 기공 분포를 나타냈다. 그 보다 낮은 온도에서는 기공형성이 충분치 않았고, 그 이상에서는 기공이 불균일하게 분포하여 측면이나 상부에 밀집되면서 더욱 큰 기공을 형성하는 경향을 보였다. 이렇게 제조된 PP 시트의 밀도는 0.518g/cc이었고, 기공률로 약 47%에 해당하였다.

• Proceedings of the Korean Vacuum Society Conference
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• 2011.02a
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• pp.183-183
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• 2011

리튬 이온 배터리의 cathode 및 electrolyte 재료로 사용되는 LiCoO2을 sputtering이나 pulsed laser deposition을 이용하여 박막으로 증착하기 위해서는 target이 필요하다. Target은 원료 분말을 가압 성형한 후 고온에서 소결하여 제조된다. LiCoO2 target 제조과정에서 고밀도를 얻기 힘들고 Li 성분의 증발이 일어난다. 또한 Li2O 분말은 흡습성이 매우 크다. 본 연구에서는 시간과 온도를 조절하여 최적화된 소결 과정을 통해 target의 밀도가 이론밀도와 근사한 값을 갖도록 하고, LiCoO2 또는 Co3O4 분말에 각각 흡습성이 낮은 Li2CO3 분말을 첨가하여 Li 성분을 조절하였다. Li과 Co의 조성비가 1:1-2:1인 고밀도의 LiCoO2 target을 제조하여 박막 증착 후 Li과 Co의 조성비가 1:1이 되도록 하였다.

• Korean Journal of Food Science and Technology
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• v.31 no.1
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• pp.257-259
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• 1999

A molding of roasted glutinous rice powder by pressurized steaming was investigated in terms of steaming pressure and powder size. Roasted glutinous rice powders of $80{\sim}115,\;115{\sim}170,\;170{\sim}250$, and 250

• Korean Journal of Materials Research
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• v.6 no.2
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• pp.182-187
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• 1996

물과 에탄올의 혼합용액에 HCI을 촉매로하여 금속알콕사이드의 가수분해로부터 코오디어라이트 분말을 제조하였다. 이때 HCI/precursor 몰비로써 촉매의 양을 조절하였다. 건조분말 중의 용매를 제거하기위해 80$0^{\circ}C$에서 3시간 하소처리하였다. 이들 하소된 분말에 대하여 시차열분석과 X-선회절분석을 행한 결과-92$0^{\circ}C$에서 $\mu$-cordierite, -103$0^{\circ}C$에서 $\alpha$-cordierite 결정상의 생성을 확인하였다. 또한, 하소분말을 가압성형한 후 130$0^{\circ}C$에서 4시간 열처리한 결과 HCI양에 따라 기공율 19.45-25.45%, 부피비중 2.06-1.70g/㎤, 유전상수 1.38-3.38 범위의 소결체를 얻었다. HCI양이 증가할수록 기공율은 증가한 반면에 비유전상수와 부피비중은 감소하였다.

• Journal of Powder Materials
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• v.30 no.1
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• pp.35-40
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• 2023

In this study, a graphite block is fabricated using artificial graphite processing byproduct and phenolic resin as raw materials. Mechanical and electrical property changes are confirmed due to the preforming method. After fabricating preforms at 50, 100, and 150 MPa, CIP molding at 150 MPa is followed by heat treatment to prepare a graphite block. 150UP-CIP shows a 12.9% reduction in porosity compared with the 150 MPa preform. As the porosity is decreased, the bulk density, flexural strength, and shore hardness are increased by 14.9%, 102.4%, and 13.7%, respectively; and the deviation of density and electrical resistivity are decreased by 51.9% and 34.1%, respectively. Therefore, as the preforming pressure increases, the porosity decreases, and the electrical and mechanical properties improve.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.1
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• pp.73-82
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• 1997

High temperature densification behaviors of alumina powder compacts were investigated under hot pressing and hot isostatic pressing. An alumina part of valve-head shape was fabricated under hot pressing and its forming process was simulated by finite element calculation. an alumina powder compact encapsulated by a stainless steel container was also densified under hot isostatic pressing. Inhomogeneous deformations during hot isostatic pressing due to the canning effect were observed experimentally and predicted by finite element analysis.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.5 no.4
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• pp.386-393
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• 1995

A Abstract Producing process of FGM by SHS process has been investigated and $TiB_2$/Cu based FGM was fabricated by the process. When raw material powders were stacked on, Cu substrate, composition profile can be graded. This stacked body was compressed and vacuum­s sealed into the capsule for the synthesis. This sample was ignited and compressed under high h hydro - pressure. By the observation of the crystal phases and microstructures of produced $TiB_2$/Cu FGM samples, the compositional gradient was able to be identified.

• Tunnel and Underground Space
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• v.22 no.1
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• pp.69-76
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• 2012

Theoretical backgrounds on the experimental methods of explosive welding, explosive forming and shock consolidation of powders are introduced. Explosive welding experiments of titanium (Ti) and stainless steel (SUS 304) plate were carried out. It was revealed that a series of waves of metal jet are generated in the contact surface between both materials; and that the optimal collision velocity and collision angle is about 2,100~2,800 m/s and $15{\sim}20^{\circ}$, respectively. Also, explosive forming experiments of Al plate were performed and compared to a conventional press forming method. The results confirmed that the shock-loaded Al plate has a larger curvature deformation than those made using conventional press forming. For shock consolidation of powders, the propagation behaviors of a detonation wave and underwater shock wave generated by explosion of an explosive are investigated by means of numerical calculation. The results revealed that the generation and convergence of reflected waves occur at the wall and center position of water column, and also the peak pressure of the converged reflected waves was 20 GPa which exceeds the detonation pressure. As results from the consolidation experiments of metal/ceramic powders ($Fe_{11.2}La_2O_3Co_{0.7}Si_{1.1}$), shock-consolidated $Fe_{11.2}La_2O_3Co_{0.7}Si_{1.1}$ bulk without cracks was successfully obtained by adapting the suggested water container and strong bonding between powder particles was confirmed through microscopic observations.