• Journal of the Korean Crystal Growth and Crystal Technology
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• v.13 no.6
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• pp.304-308
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• 2003

By controlling the internal pressure in the cyclone separator, we investigated the separation charateristics of $Al_2O_3$, $Fe_2O_3$ particles with the internal pressure variation. 3-dimensional Langrangian approach was applied for the analysis of the particles separation, and then the minimum cut diameter of the separated particles and the separation rate were calculated through tracking the particle trajectories. The density of the argon gas for transporting particles was decreased corresponding the pressure decrease, consequently, caused the internal pressure drop in the cyclone separator. For that reason the finer particles were separated as the pressure was changed from an atmospheric pressure to an low pressure. Specifically, at 50 torr pressure, $Al_2O_3$ particles of the size of about 4 $\mu\textrm{m}$ and $Fe_2O_3$particles of about 3 $\mu\textrm{m}$ could be separated.

• Korean Chemical Engineering Research
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• v.61 no.1
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• pp.39-44
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• 2023

In this study, the particle size of Si polycrystals was controlled through wet-sedimentation method, and changes in the capacity and cyclic characteristics of the Si anode material according to the particle size were observed. After wet-sedimentation of Si particles pulverized by a vibration mill, the non-uniform particle distribution of Si was uniformly controlled. The d₅₀ of a sample in which Si was sedimented for 24 hours decreased to 0.50 ㎛. As a result of the electrochemical characteristic analysis, the Rct value representing the resistance in the electrode was significantly reduced due to the decrease in particle size. The unclassified Si sample exhibited a discharge capacity of 2,869 mAh/g in the first cycle, and decreased to 85.7 mAh/g after 100 cycles. The sample in which Si was classified for 24 hours showed a capacity of 3,394 mAh/g initially, and maintained a capacity of 1,726 mAh/g after 100 cycles. As the size of the Si particles decreased, the discharge capacity increased and the cycle life was also increased.

• Cement Symposium
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• s.36
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• pp.110-115
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• 2009

2,3,4호 시멘트밀은 기존의 Tube MiIl 단독의 시멘트 분쇄 밀에 예비분쇄기(이하 "Polycom", Polysius 1992년 공급)를 설치, 합리화하여 운영되고 있는 Combi grinding type의 시멘트밀이다. 생산능력은 일 생산성 4,800T/D, Blaine $3,200cm^2/g$ 품질로 설계되었다. 금번 공정개선 부문인 예비분쇄공정의 Polycom 출구 Bucket Elevator(이하 "B/E") 및 Disagglomerator(이하 "DISA")로 위치는 Fig.1과 같다. Polycom 출구 B/E 및 DISA는 Polycom에서 분쇄된 원료를 분급기로 이송 및 cake 상태의 원료를 파쇄하는 설비이다. 상기 설비는 시멘트밀 공정에서 반드시 필요한 설비이나 - 잦은 고장에 따른 설비 가동율 저하 - 순환량 증가시 제한운전에 따른 생산효율저하를 일으키는 주된 설비로써 원단위 절감 및 설비가동효율 향상을 위하여 개선이 불가피한 설비임.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2002.04b
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• pp.45-45
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• 2002

나노미터 크기의 결정립을 가지는 나노분말 및 나노복합분말의 제조와 특성에 관한 연구가 매우 활발하다. 나노복합분말의 제조방법에는 기상증발후 응축법, 화학응축법, 기계적합금법 등이 있으나, 고순도 및 균일한 크기분포의 분말과 응집되지 않은 분말의 제조 조건을 가장 잘 만족하는 방법은 화학기상응축법(Chemical Vapor Condensation; CVC)이다. 본 연구그룹 에서는 CVC밤법으로 이용하여 공구/금형재료에 가장 많이 사용되는 WC/Co 합금의 결정립을 n nm크기로 극미세화고자하는 연구을 진행하고 있다. 본 연구에서는 이들 WC/Co합금제조시 가장 중요한 출발분말인 나노크기 WC 분말의 제조와 그 특성에 관하여 연구하고자 하였다. 나노미터 WC분말을 제조하기 의한 전구체는 고상의 금속유기물인Tungstenhexacarbonyl$(W(CO)_6)$ 을 사용하였다. 수평관상로을 반응기로 사용하였으며, 노내의 온도을 500-110$0^{\circ}C$로 변화시 키면서 WC 분말을 합성하였다. 반응기 및 포집기 내부를 대기분위기, 상압의 Ar분위기, 진공 분위기로 변화시켜 압력 및 분위기의 영향을 조사하였다. 포집기는 상온 및 액체질소로 냉각 한 Chiller을 사용하였다. 형성분말의 상분석은 XRD로 조사하였으며, 형태 및 결정립크기는 TEM로 분석하였다. 반응온도 600 -1 OOO$^{\circ}C$의 온도범위에서 검은색의 WC 분말이 제조되었다. XRD 분석의 결과 로 제조된 분말은 상온에서 준안정상인 Hexagonal 구조의 $\gammar-WC_{1-x}$ 상이였으며, TEM 분석결 과 상압하에서는 약 30nm이하의 WC분말이 제조되었으며, 그 형태는 둥근 4각형의 모양을 지녔다. 감압하에서 진행한 경우 결정립의 크기는 8nm이하를 가졌다.곤가스로 산화를 방지하였고, 냉매로는 질소가스를 이용하였다. 제조된 분말을 기ㅖ적 분급법을 이용하여 분급하였고, 냉매로는 질소가스를 이용하였다. 제조된 분말을 기계적 분급ㅂ법을 이용하여 분급하였고, 압출에 이용된 분말은 250$\mu\textrm{m}$이하의 크기를 사용하였다. 또한 분말제조과정 중 형성되는 표면산화층을 제거하기 위하여 36$0^{\circ}C$에서 4시간동안 수소 환원처리를 행하였다. 제조된 분말은 열간 압출을 위하여 Aㅣcan에 넣고 냉간성형체를 만들고, 진공처리를 한 후 밀봉하여 탈가스처리를 하였다. 압출다이는 압출비가 각각 28:1과 16:1인 평다이(9$0^{\circ}C$)를 사용하여 각각 내경이 9, 12cm이고, 길이가 50, 30cm인 압출재를 제조하였다. 열간압출한 후의 미세조직을 광학현미경으로 압출방향에 평행한 방향과 수직방향으로 관찰하였고, 열간 압출재 이방성을 검토하기 위하여 X선 회절분석을 실실하여 결정방위를 확인하였다. 전기 비저항 및 Seebeck 계수 측정을 위하여 각각 2$\times$2$\times$10$mm^3$ 그리고 5$\times$5$\times$10TEX>$mm^3$ 크기의 시편을 준비하였다.준비하였다.전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all low in two aspects, named "the Nonsign

• Resources Recycling
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• v.11 no.1
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• pp.9-18
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• 2002

Printed wiring boards(PWBs) of the obsolete computers are composed of various organic and inorganic compounds as well as metals and alloys. As convinced that the valuable metals obtained from the PWBs are effectively utilized as secondary resources when recovered by economical methods, in this study, an investigation for characterizing the physical separation techniques is conducted. For the recovery of them, the sockets and chips dismantled from PWBs by scraping and residual resin boards are subjected to the appropriate separation processes according to the physical properties of each part. In the case of crushed socket scraps size ranged from -2.36 mm to +1.18 mm, approximately 97 wt% of the product obtained by magnetic separation consists of metallic compounds. In the case of chip scraps, 97% of Fe-Ni alloy and 95% of Cu metal are recovered by the combined process of air classification and dry magnetic separation in the size range from -2.36 mm to +0.15 mm. Ball milling is adopted in order to improve the removal efficiency of the thin-printed metallic materials on the residual resin boards and approximately 77% of Cu metal is recovered by zigzag separation after ball milling.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.11a
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• pp.757-760
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• 2006

This study aims to manufacture ultra fine cement(UFC) with a multi air-classifier of the dry-type. The classifier employed and devised for materials refining was a cyclone type fitted with an air suction device. This study also investigates the basic physical properties and quality of UFC and evaluates its utilizable possibility as a construction material. The basic properties of the UFC containing granulated blast furnace slag were analyzed and examined through recovery ratio, particle size distribution, scanning electron microscopy and compressive strength. Results obtained from the analysis of ultra fine cement have shown that there are possibilities for manufacturing UFC, which could compensate the weak properties of ordinary Portland cement.

• Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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• 2006.11a
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• pp.241-253
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• 2006

• Journal of the Korean earth science society
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• v.37 no.4
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• pp.218-229
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• 2016

The bedform stability diagram indicates the shape and size of bedforms that will occur to a given grain size and flow velocity. The diagram has been constructed from experimental data which have been mostly acquired by flume experiments. Generally, the flume experiments have been performed on well sorted sediments with unimodal grain size distribution, in order to understand relationship between grain size and flow velocity. According to the diagram, a ripple structure initiates to be formed from lower flow regime flat bed, as the flow velocity increases on the surface of fine-sand or medium-sand sediments. This study aims to verify that the experimental result of bedform stability diagram will be reproduced in our flume experimental systems, and also to confirm that the result is consistent not only on well-sorted sand sediments but also on poorly-sorted sand sediments with bimodal grain size distribution. The experimental results in this study show that initiation of 2D or 3D ripple structure on poorly-sorted sand sediments requires higher flow velocity and shear stress than those for initiation of the structure on well-sorted sand sediments. In general, carbonate sediments are characterized by poor sorting due to inactive hydraulic sorting and bimodal grain size distribution with allochems and matrices. The results suggest that the carbonate depositional system possibly need a higher flow velocity for initial formation of 2D or 3D bedform structures. The reason might be the fact that pulling off and lifting of a grain in poorly sorted sediments require more energy due to sorting, friction, stabilization, armour effects, and their complex interaction. This preliminary study warrants additional experiments under various conditions and more accurate analysis on the relationship between formation of bedforms and grain size distribution.

• Journal of the Mineralogical Society of Korea
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• v.18 no.1
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• pp.19-31
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• 2005

A study on the beneficiation of illite occurring in Youngdong province is performed with applying selective grinding and air classification techniques. Quartz and illite are occurred as major components, and sulfide minerals such as pyrite, chalcopyrite are associated as minor components. The result of sieving test shows that contents of Al₂O₃, K₂O and ignition loss are increased, whereas SiO₂ is decreased with particle size decrease. Fe₂O₃ content is almost same in all the particle size range but slightly lower at coarse particles. The yield of fine particles is increased with increasing rotor speed in both grinding stage and air classification stage. When the selective grinding and air classification are carried out at optimal condition, yield of the concentrate is 76.16 wt.%. The chemical compositions of the concentrate are SiO₂70.13%, Al₂O₃ 19.40%, Fe₂O₃ 1.62%, K₂O 5.20%, and ignition loss 2.77%. The beneficiation process developed in the current study is very effective method which purification and particle size control can be achieved simultaneously.

• Resources Recycling
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• v.31 no.6
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• pp.66-72
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• 2022

The circularity and particle size distribution of products obtained from dry classification after circularity tests using a high-intensity mixer were investigated to evaluate the use of domestic graphite concentrate as a lithium-ion battery material. At a rotor speed of 3,000 rpm, the particle size and circularity of the concentrated sample and product were unchanged. The circularity increased and particle size decreased when the rotor speeds were increased to 6,000 rpm, 10,000 rpm, and 12,000 rpm and the operating time was increased. For instance, the circularity increased from 0.870 to 0.936 when the rotor speed was increased from 3,000 rpm to 12,000 rpm for an operating time of 10 min. After the circularity test, dry classification was performed, wherein the circularity of the coarse particles was found to have increased to 0.947. Round particles were observed in the SEM images, indicating that high circularity was successfully achieved.