• Title/Summary/Keyword: 복합 부식시험

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A STUDY ON THE BONDING OF COMPOMER TO DECIDUOUS DENTIN (컴포머와 유치 상아질의 결합에 관한 연구)

  • Kim, Jee-Tae;Kim, Yong-Kee;Kim, Jong-Soo;Kwon, Soon-Won
    • Journal of the korean academy of Pediatric Dentistry
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    • v.29 no.4
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    • pp.509-518
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    • 2002
  • The purpose of this study was to evaluate the bonding of compomer to deciduous dentin which is known to have been developed to improve the weak properties of glass ionomer cement and composite resin. 120 sound primary molars were used for the shear bond strength test and another 24 for the scanning electron microscopic evaluation. Each material was ailed into polyethylene mold attached to exposed dentinal surface($3{\times}4mm$ in diameter) of sample blocks. Shearbond strength was measured using Universal testing machine and data were analyzed statistically with Oneway-ANOVA and Scheffe test. Scanning electron microscopic observation was performed in order to evaluate the pattern of distribution and penetration of resin tags and hybrid layer. Compomer groups(II-V) showed significantly higher bond strength values than glass ionomer group(I)(p<.05). Etching-compomer groups(III, V) showed the significantly higher bond strength than non-etching compomer groups(II, IV)(p<.05), but slightly lower values than composite resin group(VI) with no statistically significant difference(p>.05). No significantly different bond strength was found between compomer groups of different bonding system(p>.05). Scanning electron micrographs showed more irregular distribution of short and thin resin tags in non-etching compomer groups(II, IV) whereas the more regular and intimate distribution of long and thick tags in etching compomer groups(III, V) and composite resin group(VI). The evaluation of hybrid layer also showed more regular formation of thicker layer in etching compomer groups(III, V). Based on the results of present study, the use of compomer as an esthetic restorative material for primary molars might be justified.

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Light fastness of Zinc oxide for aramid fiber via sol-gel deposition (나노 산화아연 처리에 의한 파라 아라미드 섬유의 내광성 증진 연구)

  • Park, S.M.;Kim, M.S.;Kwon, I.J.;Sim, J.H.;Lee, K.N.;Yoon, N.S.
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2012.03a
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    • pp.110-110
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    • 2012
  • 아라미드 섬유소재는 고강도, 고내열성의 소재로 다양한 용도전개가 가능하나, 일광 및 부식에 의한 내광성 및 내후성이 급격하게 저하되는 단점이 있다. 자외선의 광화학적 작용에 의해 변퇴, 경화, 취하, 강도저하가 일어나는 단점을 보완하기 위해 내광성 및 내화학성이 우수한 전이금속산화물 소재와의 복합화를 통해 내광성 및 내화학성 개선에 대하여 연구하였다. zinc acetate 수화물과 수산화리튬을 무수에탄올로 용해시킨 용액을 강하게 교반하여 나노 산화아연 졸을 제조하였다. 제조된 나노크기의 zinc oxide 입자의 형상과 입자분포 등 제조특성을 입도분석기, FE-SEM 및 EDS 분석을 통하여 고찰하였으며, 제조된 나노졸을 아라미드 섬유에 침지시켜 Xenon-arc 내후성시험기에서 80시간 동안 노출시켜 노출시간에 따른 물성변화를 분석하였다. 나노졸을 5~20% 픽업으로 패딩한 후 광에 노출된 아라미드의 인장강도는 나노졸을 처리하지 않은 아라미드 섬유보다 20~30% 개선된 인장강도를 나타내었다.

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Development of Propellant for Turbopump Pyro Starter (터보펌프 시동기용 추진제 개발)

  • Song, Jong-Kwon;Choi, Sung-Han;Hong, Moon-Geun;Lee, Soo-Yong
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.05a
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    • pp.7-10
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    • 2009
  • The development and evaluation of solid propellant were performed for the turbopump pyro starter, which start up the liquid propellant rocket engine for the Space Launch Vehicle (SLV). Requirements for the turbopump pyro starter propellant include the production of low flame temperature, low burning rate and nontoxic gas to protect the mechanical corrosion or air pollution. This study describes the development of the solid propellant composition which is based on PCP binder. DHG (Dihydroxy glyoxime), which has advantages of oxygen balance and ignition, was used as coolant. The mechanical properties and burning rate of the propellants were measured. Finally, static fired test was performed to prove the possibility of development.

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Flexural Behaviors of GFRP Rebars Reinforced Concrete Beam under Accelerated Aging Environments (GFRP Rebar 보강 콘크리트 보의 급속노화환경에서의 휨 거동에 관한 연구)

  • Park, Yeon-Ho;Choi, Yeol
    • Journal of the Korea Concrete Institute
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    • v.25 no.2
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    • pp.137-144
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    • 2013
  • The use of fiber-reinforced polymer (FRP) reinforcing bars in concrete structures has been increased as an alternative of steel reinforcement which has shown greater vulnerability to corrosion problem. However, the long-term performance of concrete members with FRP reinforcement is still questioned in comparison to the used of steel reinforcement. This study presents the results of an experimental study on the long-term behaviors of GFRP (glass fiber reinforced polymer) bar reinforced concrete beams after exposed to accelerated aging in an environmental chamber with temperature of $46^{\circ}C$ ($115^{\circ}F$) and 80% of relative humidity up to 300 days. The objectives of this research was to compare strength degradation and change of ductility between GFRP reinforced concrete beams and steel reinforcement beams after accelerated aging. Two types (wrapped and sand-coated surface) of GFRP bars and steel were reinforced. in concrete beams. Test results show that the failure modes of GFRP bar reinforced concrete beams are very similar with traditional RC beams, and the change of load-carrying capacity of steel reinforcing concrete beam is greater than that of GFRP bar reinforcing concrete beam under the accelerated aging. Test result also shows that the use of GFRP reinforcing in concrete could be introduced more brittle failure than that of steel reinforcing for practical application. The deformability factor up to compression failures indicates no significant variation before and after exposure of accelerated aging.

Electricity Production by Metallic and Carbon Anodes Immersed in an Estuarine Sediment (퇴적토에 담지된 금속 및 탄소전극에 의한 전기 생산 특성)

  • Song, Hyung-Jin;Rhee, In-Hyoung;Kwon, Sung-Hyun;Cho, Dae-Chul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.10 no.12
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    • pp.3731-3739
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    • 2009
  • One-chambered sediment cells with a variety of anodic electrodes were tested for generation of electricity. Material used for anodes was iron, brass, zinc/iron, copper and graphite felt which was used for a common cathode. The estuarine sediment served as supplier of oxidants or electron-producing microbial habitat which evoked electrons via fast metal corrosion reactions or a complicated microbial electron transfer mechanism, respectively. Maximum power density and current density were found to be $6.90\;W/m^2$ (iron/zinc) and $7.76\;A/m^2$ (iron), respectively. Interestingly, copper wrapped with carbon cloth produced better electric performance than copper only, by 60%, possibly because the cloth not only prevented rapid corrosion on the copper surface by some degrees, but also helped growing some electron-emitting microbes on its surface. At anodes oxidation reduction potential(ORP) was kept to be stationary over time except at the very initial period. The pH reduction in the copper and copper/carbon electrodes could be a sign of organic acid production due to a chemical change in the sediment. The simple estimation of interfacial, electrical resistances of electrodes and electrolyte in the sediment cell that a key to the electricity generation should be in how to control corrosion rate or microbial electron transfer activity.

Performance Evaluation of Fiber-Reinforced Concrete Compression Members Transversely Constrained by BFRP (BFRP로 횡구속된 섬유 보강 콘크리트 압축부재의 성능평가)

  • Lee, Gyeong-Bok;Lee, Sang-Moon;Jung, Woo-Young
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.42 no.5
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    • pp.607-616
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    • 2022
  • Corrosion and degradation of reinforced structures due to abnormal climates and natural disasters further accelerate the aging of structures. Coping with the decrease in structure performance, many old structures are being repaired and reinforced with low-weight and high-strength materials such as glass fiber composite material (GFRP). To further contribute, this paper focus on a more economical and eco-friendly material, basalt fiber composite (BFRP), which provide a more effective lateral constraint effect for seismic reinforcement. The main variables considered in this study are the curing temperature during the manufacturing of BFRP and the material characteristics of the target concrete member. The lateral constraint reinforcement effect was investigated through the evaluation of the performance of normal concrete and those with improved durability through fiber reinforcement. The reinforcement effect was 3.15 times for normal concrete and 3.72 times for fiber reinforced concrete, and the difference in reinforcement effect due to the improvement of the durability characteristics of the compression member was not significant. Lastly, the performance of the BFRP was compared with the results of the GFRP reinforcement from the previous study. The effect of the BFRP reinforcement was 1.18 times better than that of the GFRP reinforcement.

Evaluation of the Cytotoxicity and Mechanical Strength of Dental Duplex Stainless Steel Orthodontic Wire (치과 교정용 듀플렉스 스테인리스 스틸 와이어의 기계적 강도 및 세포독성 평가)

  • Lee, Myung-Kon;Kim, Chi-Young
    • The Journal of the Korea Contents Association
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    • v.10 no.9
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    • pp.309-317
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    • 2010
  • The stainless steel wire is extensively used for the orthodontic treatment. But, the stainless steel wire that has commonly superior corrosion resistance has caused hypersensitive reaction or allergy as side effects because of corrosion in the oral environment. For improving the problem of corrosion, we was evaluated the suitability of the duplex stainless steel(DSS) as orthodontic wire through this study. The DSS wire was evaluated the mechanical strength and bio-stability for suitability and bio-compatibility as orthodontic wire. In this work, the DSS and stainless steel(SS) as common use of medical grade were prepared for the tensile strength test. The DSS wire were treated by heat. and Temperature conditions of the heat treatment were $28^{\circ}C$, $500^{\circ}C$, $600^{\circ}C$, $700^{\circ}C$, $800^{\circ}C$, $900^{\circ}C$, respectively. And the DSS wires that treated by heat on the optimum temperature condition were conducted the bending moment test and calculated the S-Max value and the modulus of elasticity. For evaluating the bio stability, each materials were conducted in vitro test for measuring the cell survival rate. The most interesting results was that the tensile strength test of SS wire($8.17\times10^4\;N/mm^2$) and DSS wire($8.05\times10^4\;N/mm^2$) that treated at $500^{\circ}C$ by heat were similar in mechanical strength. In the bio-stability study, the DSS has no cytotoxicity (p=0.05) Thus, we could make a conclusion that the duplex stainless steel wire has vastly superior corrosion resistance was suitable as orthodontic wire.

EFFECT OF THE ADDITIONAL ETCHING PROCEDURE ON PUSH-OUT BOND STRENGTH OF ONE-STEP RESIN CEMENT (부가적 부식 과정이 단일 접착 과정 레진 시멘트의 접착 강도에 미치는 영향)

  • Kang, Soon-Il;Park, Jeong-Kil;Hur, Bock;Kim, Hyeon-Cheol
    • Restorative Dentistry and Endodontics
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    • v.33 no.5
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    • pp.443-451
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    • 2008
  • The purpose of this study was to evaluate the effect of additional etching procedure prior to Maxcem resin cement application in indirect restoration cementation using push-out bonding strength. One hundred and two extracted human molars were used to make indirect resin restorations of gold inlay and Synfony. These restorations were cemented using Maxcem and Variolink II. Additional etching procedures were done for one group with Maxcem. Three groups have 17 specimens in both restoration types. Push-out bond strength was measured using multi-purpose tester and calculated for bonding strength per sqaure-millimeter area. The mean bonding strength values were compared using SPSS 12.0K program for one-way ANOVA and Scheffe's Test with 95% significance. Under the condition of this study, the additional etching procedure prior to usage of Maxcem resulted in reduced bond strength for both of restoration types.

An Experimental Study on Bond Characteristics of FRP Reinforcements with Various Surface-type (다양한 표면형상에 따른 FRP 보강재의 부착특성 실험연구)

  • Jung, Woo Tai;Park, Young Hwan;Park, Jong Sup
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.31 no.4A
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    • pp.279-286
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    • 2011
  • FRP (Fiber Reinforced Polymer) tendons can be used as an alternative to solve the corrosion problem of steel tendons. Material properties of FRP tendons-bond strength, transfer length, development length-must be determined in order to apply to concrete structures. First of all, in case of application for pretension concrete members with CFRP tendons, transfer length is an important characteristic. The bond of the material characteristics should be demanded clearly to apply to PSC structures prestressed with FRP tendons. This paper investigated on the bond characteristics of FRP reinforcements with various surface-type. To determine the bond characteristics of FRP materials used in place of steel reinforcement or prestressing tendon in concrete, pull-out testing suggested by CAN/CSA S806-02 was performed. A total of 40 specimens were made of concrete cube with steel strands, deformed steel bar and 6 different surface shape FRP materials like carbon or E-glass. Results of the bonding tests presented that each specimen showed various behaviors as the bond stress-slip curve and compared with the bond characteristic of CFRP tendon developed in Korea.

A study on fatigue properties of GFRP in synthetic sea water (인공해수중 GFRP의 피로특성에 관한 연구)

  • 김연직;임재규
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.6
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    • pp.1351-1360
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    • 1993
  • The fatigue behavior of GFRP composites is affected by environmental parameters. Therefore, we have to study on effect of sea water on fatigue behavior of GFRP composites as to maintain the safety and confidence in design of ocean structure of GFRP. In this paper, we investigated the fatigue properties of chopped strand glass mat/polyester composite in synthetic sea water. (pH 8.2) In case of the glass fiber (CSM type) reinforced polyester composite materials, the fatigue crack in the both dry and wet specimens tested in air or synthetic sea water occurred at the initial of cycle. Thereafter, it was divided with two regions that one decreased with the crack extension and the other increased with the crack extension. The transition point occurred during the crack propagation shifted to high ${\Delta}K$ value as load increase but its point is not changed regardless of immersion or test environment under a constant load. The synthetic sea water degrades the bond strength between fiber and matrix, thereby the tendency of rapid deceleration and acceleration of the crack growth was appeared.