• Title/Summary/Keyword: 반응표면 분석법

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고온, 고압 가수분해반응에 의한 우지 분해공정: 반응표면분석법을 이용한 반응조건의 최적화

  • Kim, Won-Ho;Kim, Yong-Min;Kim, Ho-Jung;Heo, Byeong-Gi
    • 한국생물공학회:학술대회논문집
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    • 2001.11a
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    • pp.303-307
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    • 2001
  • Operation conditions to maximize the hydrolysis of beef tallow was investigated by using the response surface method. In the response surface analysis, reaction temperature, pressure, and ratio of fat to water was considered as independent variables. The concentrations of triglycerides. diglycerides, monoglycerides and free fatty acids were considered as dependent. variables. The optimum conditions for the hydrolysis was as follows' the reaction temperature was $271^{\circ}C$, pressure 86 bar and ratio of fat to water was 106.08g / 133.93 g. The maximum concentration of free fatty acids was 96.49 % at these optimum conditions.

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Application of Response Surface Method for Injection mold Design Optimization (사출금형 설계 최적화를 위한 반응표면 분석법의 적용)

  • 류미라;이권희;김영희;박흥식
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.223-226
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    • 2004
  • It is net easy to predict the shrinkage rate of a plastic injection mold in its design process. The shrinkage rate should be considered as one of the important performances to produce the reliable products. The shrinkage rate can be determined by suing the CAE tools in the design produces. However, since the analysis can take minutes to hours, the high computational costs of performing the analysis limit their use in design optimization. In this study, the surrogate models based on the RSM is used in lien of the original models, facilitating design optimization.

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Optimal Design of FRP Taper Spring Using Response Surface Analysis (반응표면 분석법을 이용한 FRP 테이퍼 판 스프링의 최적설계)

  • 오상진;이윤기;윤희석
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.676-679
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    • 1997
  • The present paper is concerned with the optimal deslgn that the static spring rate of the fiber-reinforcement composite spring is fitted to that of the steel leaf spring. The thickness and w~dth of springs were selected as deslgn variables. And object functions of the regression model were obtained through the analysis with a common analytic program. After regression coefficients were calculated to get functions of the regression model, optimal solutions were calculated with DOT. E-GlassIEpoxy and CarbonIEpoxy were used as fiber reinforcement materials in the design, which were compared and analyzed with the steel leaf spring. It was found that the static spring rate of the optimal model was almost similar to that of the existing spring.

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Robust Design of Mechanisms Using the Response Surface Analysis (반응표면 분석법을 이용한 기구의 강건설계)

  • Han, Hyung-Suk;Park, Tae-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.13 no.10
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    • pp.56-61
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    • 1996
  • In this study a method for a robust design of mechanisms is proposed. The method used in the experimental analysis and quality engineering is applied for mechanisms design. A mathematical model for a mechanism is estimated by the response surface analysis and the estimated model is used in minimization of the variance. Using this result, robust design can be carried out. The method can be applied for general mechansims. Furthermore because the method can be used in the design stage using the computer model, improved quality and lower cost of the product is achieved even in the design stage.

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Fire Power Analysis for Concept Exploration of Combat Vehicle (전투차량체계의 개념탐색을 위한 화력성능분석)

  • Lim, O-Kaung;Choi, Eun-Ho;Ryoo, Jae-Bong
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.22 no.3
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    • pp.251-258
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    • 2009
  • At the stage conceptual design, combat vehicle is classified into three general categories of fire power, mobility and physical properties of system. The present research is restricted to fire power and its optimization. At the stage of conceptual designing of system, it is appropriate to consider major variables affecting fire power - including the weight of bullet, which exerts a direct influence on destroying effect, maximum range which takes long range firing in consideration. To estimate the maximum firing range, a simple interior ballistic and an exterior ballistic model were built by using the lumped parameter method, Le Duc method and point mass trajectory model. Design of experiment and regression analysis was used to derive simulations of fire power. Finally, response surface models were built and design variables were analyzed.

Approximate Multi-Objective Optimization of A Wall-mounted Monitor Bracket Arm Considering Strength Design Conditions (강도조건을 고려한 벽걸이 모니터 브라켓 암의 다중목적 근사최적설계)

  • Doh, Jaehyeok;Lee, Jongsoo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.5
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    • pp.535-541
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    • 2015
  • In this study, an approximate multi-objective optimization of a wall-mounted monitor bracket arm was performed. The rotation angle of the bracket arm was determined considering the inplane degree of freedom. We then formulated an optimization problem on maximum stress and deflection. Analyses of mean and design parameters were conducted for sensitivity regarding performance with orthogonal array and response surface method (RSM). RSM models of objective and constraint functions were generated using central composite (CCD) and D-optimal design. The accuracy of approximate models was evaluated through $R^2$ value. The obtained optimal solutions by non-dominant sorting genetic algorithm (NSGA-II) were validated through the finite element analysis and we compared the obtained optimal solution by CCD and D-optimal design.

광환원법을 이용한 편극 패턴 된 강유전체 표면에 금속 나노입자의 선택적 성장

  • Park, Yeong-Sik;Kim, Jeong-Hun;Chu, Ben-Ben;Min, Chi-Hong;Yang, U-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.445-445
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    • 2011
  • 본 연구에서는 편극 패턴된 강유전체 단결정 $LiNbO_3$ 기판에 광화학적 반응에 의해 금속(Au, Ag, Cu)나노입자를 표면에 선택적으로 성장하였다. 강유전체는 자발편극성의 특성을 지니고 있기 때문에 선택적으로 전압을 가하여 편극성의 역전에 의해 표면의 편극성을 선택적으로 패터닝이 가능하다. 본 연구에서는 주기적으로 양의 편극 영역과 음의 편극 영역이 패턴된 $LiNbO_3$ 기판을 사용하였다. 표면의 편극성은 압전소자반응현미경법(PFM)을 이용하여 확인하였으며, 극성은 R-V curve로 확인하였다. 금속입자는 금속입자를 포함하는 용액에 기판을 넣고 자외선을 조사하여 성장시켰다. 성장된 금속입자의 표면 분포 및 분석은 AFM을 이용하여 측정하였다. Ag 입자를 성장시킨 결과, (-z)편극 영역보다 (+z)편극영역에서 보다 많은 금속 나노입자들이 환원반응을 일으켜 나노입자를 형성하였으며, 경계영역 (inversion domain boundary)에 가장 많은 나노구조체가 형성되었다. Au 입자의 경우, (+z)편극영역이 (-z)편극영역의 표면보다 더 많은 입자가 형성되었지만 Ag입자처럼 편극영역의 경계에서 많이 증착되는 경향성은 보이지 않았다. Cu 입자의 경우 광화학반응을 거의 일으키지 않았으며, 편극영역에 따른 증착 경향성도 보이지 않았다. 이와 같은 결과를 증착된 금속 나노입자의 편극에 따른 표면분포를 강유전체 표면 극성에 따른 표면 밴드구조와, 각 입자가 지닌 환원전위와 전자친화도에 관련된 모델로 설명할 것이다.

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Optimization of LC-MS/MS for the Analysis of Sulfamethoxazole by using Response Surface Analysis (반응표면분석법을 이용한 설파메톡사졸의 액체크로마토그래프-텐덤형 질량분석 최적화)

  • Bae, Hyo-Kwan;Jung, Jin-Young
    • Journal of Korean Society of Environmental Engineers
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    • v.31 no.9
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    • pp.825-830
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    • 2009
  • Pharmaceutical compounds enter the water environment through the diverse pathways. Because their concentration in the water environment was frequently detected in the level of ppt to ppb, the monitoring system should be optimized as much as possible for finding appropriate management policies and technical solutions. One Factor At a Time (OFAT) approach approximating the response with a single variable has been preferred for the optimization of LC-MS/MS operational conditions. However, it is common that variables in analytical instruments are interdependent. Therefore, the best condition could be found by using the statistical optimization method changing multiple variables at a time. In this research, response surface analysis (RSA) was applied to the LC-MS/MS analysis of emerging antibiotic compound, sulfamethoxazole, for the best sensitivity. In the screening test, fragmentation energy and collision voltage were selected as independent variables. They were changed simultaneously for the statistical optimization and a polynomial equation was fit to the data set. The correlation coefficient, $R^2$ valuerepresented 0.9947 and the error between the predicted and observed value showed only 3.41% at the random condition, fragmentation energy of 60 and collision voltage of 17 eV. Therefore, it was concluded that the model derived by RSA successfully predict the response. The optimal conditions identified by the model were fragmentation energy of 116.6 and collision voltage of 10.9 eV. This RSA can be extensively utilized for optimizing conditions of solid-phase extraction and liquid chromatography.

Fabrication of counter electrodes for dye-sensitized solar cells by using surface modified and dispersion controlled multi-walled carbon nanotubes (표면개질 및 분산제어된 다중벽 탄소나노튜브를 이용한 염료감응태양전지 대전극의 제조)

  • Choi, Hee-Jung;Lee, Gi-Won;Park, Nam-Kyu;Kim, Kyung-Kon;Hong, Sung-Chul
    • 한국신재생에너지학회:학술대회논문집
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    • 2008.05a
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    • pp.445-447
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    • 2008
  • 본 연구에서는 다중벽 탄소나노튜브용 표면개질제를 리빙라디칼중합법을 통하여 제조하고, 이를 이용하여 표면개질되고 분산제어된 다중벽탄소나노튜브를 제조하고 염료감응형 태양전지의 대전극 재료로 사용하였다. 우선 리빙라디칼중합법 중 nitroxide mediated polymerization (NMP) 기술을 이용하여 poly(maleic anhydride-co-p-acetoxystyrene)-block-poly(p-acetoxystyrene)를 합성하고, 공중합체중의 maleic anhydride기에 이미드화 반응을 통하여 pyrene기를 도입하였다. 공중합체 중의 p-acetoxystyrene 반복단위들은 가수분해 반응을 통하여 p-hydroxystyrene 반복단위로 변환하였으며, 제조된 공중합체의 구조와 열 특성 등을 GPC, GC, $^1H$-NMR, TGA을 통하여 분석하였다. 제조된 공중합체를 이용하여 다중벽 탄소나노튜브의 표면을 polymer wrapping법으로 처리하였고, 표면개질된 탄소나노튜브의 분산성을 다양한 용매에서 비교분석하였다. 표면이 개질되고 페이스트 내에의 분산성이 향상된 다중벽탄소나노튜브를 염료감응태양전지의 대전극 제조에 응용하였으며, 표면처리 및 분산제어 여부에 따른 제작 특성 및 동작특성 등을 평가하였다.

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